CN102527066A - Multifunctional hot reflux extracting and concentrating unit - Google Patents

Multifunctional hot reflux extracting and concentrating unit Download PDF

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Publication number
CN102527066A
CN102527066A CN2012100419872A CN201210041987A CN102527066A CN 102527066 A CN102527066 A CN 102527066A CN 2012100419872 A CN2012100419872 A CN 2012100419872A CN 201210041987 A CN201210041987 A CN 201210041987A CN 102527066 A CN102527066 A CN 102527066A
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concentration
hot reflux
extractor
reflux extracting
tank
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CN2012100419872A
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CN102527066B (en
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李晓云
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Abstract

The invention discloses a multifunctional hot reflux extracting and concentrating unit which comprises an extracting tank, a concentrating tank, an alcohol recycling tank and a condensing unit, wherein a gas outlet on the top of the extracting tank and a gas outlet on the top of the concentrating tank are respectively communicated with fluid at a to-be-condensed gas inlet of the condensing unit, a condensate outlet of the condensing device is communicated with fluid at a fluid inlet of the alcohol recycling tank, and a liquid medicine outlet at the bottom of the extracting tank is communicated with fluid at a liquid medicine inlet at the top of the condensing tank through a liquid medicine transmission pipeline. The multifunctional hot reflux extracting and concentrating unit provided by the invention has the advantages that extraction, condensation and recycle are integrated to reach the purposes of time saving, labor saving and cost reducing; and meanwhile, the extraction purity is high and the concentration ratio is large.

Description

Multi-functional hot reflux extracting-concentration machine group
Technical field
The present invention relates to the extraction enrichment facility of chemical and field of medicaments, particularly a kind of multi-functional hot reflux extracting-concentration machine group.
Background technology
In chemical and field of medicaments, often need to extract some specific materials, and after concentrating, obtain the higher mixture of content.But in the prior art, extraction equipment and concentrator normally work alone respectively, and consuming time, consumption power and cost are high; And the extraction effect that extracts equipment in the prior art is poor, and dna purity is low; The concentrating capacity of concentrator is relatively poor, causes cocnentration factor less.
Summary of the invention
To the deficiency that exists in the prior art, the object of the present invention is to provide a kind of extraction, concentrate and reclaim the multi-functional hot reflux extracting-concentration machine group of integrated work, reach save time, the laborsaving and purpose of practicing thrift cost, and dna purity is high, cocnentration factor is big.
Technical scheme of the present invention is achieved in that multi-functional hot reflux extracting-concentration machine group; Comprise extractor, concentration tank, alcohol recycling can and condensing unit; The gas vent at the gas vent at said extractor top and said concentration tank top respectively with said condensing unit treat the conducting of condensed gas inlet fluid; The liquid inlet fluid communication of the condensate outlet of said condensing unit and said alcohol recycling can, the medicine liquid outlet of said extractor bottom is through the soup inlet fluid conducting at soup conveyance conduit and said concentration tank top.
Above-mentioned multi-functional hot reflux extracting-concentration machine group is equipped with the liquor piping pump on the said soup conveyance conduit.
Above-mentioned multi-functional hot reflux extracting-concentration machine group all has heat-insulation layer on the lateral wall of said extractor and said concentration tank.
Above-mentioned multi-functional hot reflux extracting-concentration machine group has conduction oil between said extractor inwall and the said heat-insulation layer and between said concentration tank inwall and the said heat-insulation layer, in the said conduction oil electric heater is arranged.
Above-mentioned multi-functional hot reflux extracting-concentration machine group is equipped with stirring motor on the said extractor.
Above-mentioned multi-functional hot reflux extracting-concentration machine group all is equipped with Pressure gauge, oil level pipe and heat conductive oil inlet on said extractor and the said concentration tank.
Above-mentioned multi-functional hot reflux extracting-concentration machine group, said alcohol recycling can are connected with vavuum pump through vacuum tube, and said alcohol recycling can and said concentration tank pass through the suction tube fluid communication, on the said suction tube valve are installed.
The invention has the beneficial effects as follows: multi-functional hot reflux extracting-concentration machine group advantage of the present invention is to extract, concentrates and reclaims integrated work, can reach save time, the laborsaving and purpose of practicing thrift cost, and dna purity is high, cocnentration factor is big.
Description of drawings
Fig. 1 is the structural representation of the multi-functional hot reflux extracting-concentration machine group of the present invention.
Among the figure: 1-extractor, 2-concentration tank, 3-alcohol recycling can, 4-condensing unit, 5-soup conveyance conduit; The 6-vacuum tube, 7-liquor piping pump, 8-heat-insulation layer, 9-conduction oil, 10-electric heater; The 11-stirring motor, 12-Pressure gauge, 13-oil level pipe, 14-heat conductive oil inlet; The 15-water inlet, 16-delivery port, 17-suction tube, 18-valve.
The specific embodiment
In conjunction with accompanying drawing the present invention is done further explanation:
The multi-functional hot reflux extracting-concentration machine group of present embodiment; Comprise extractor 1, concentration tank 2, alcohol recycling can 3 and condensing unit 4; The gas vent at said extractor 1 top and the gas vent at said concentration tank 2 tops respectively with said condensing unit 4 treat the conducting of condensed gas inlet fluid, the liquid inlet fluid communication of the condensate outlet of said condensing unit 1 and said alcohol recycling can 3.After the gas that said extractor 1 and said concentration tank 2 volatilizes away cools off through said condensing unit 4, becoming liquid flows in the said alcohol recycling can 3 and collects and can utilize once more; Realize practicing thrift the purpose of cost.
The medicine liquid outlet of said extractor 1 bottom is through the soup inlet fluid conducting of soup conveyance conduit 5 with said concentration tank 2 tops; Like this can be so that the extract that obtains after extracting is delivered directly in the said concentration tank 2 to be concentrated, thus realized extracting and concentration integrated operation.Said alcohol recycling can 3 is connected with vavuum pump through vacuum tube 6, so that said alcohol recycling can 3 is vacuumized; And said alcohol recycling can 3 passes through suction tube 17 fluid communication with said concentration tank 2; On the said suction tube 17 valve 18 is installed; Like this can be so that the gas pumping that produces in the said concentration tank 2 inherent concentration process arrives said alcohol recycling can 3; Can solve that gases in the said concentration tank 2 can not in time enter into said condensing unit 1 and influence concentrates the problem of speed [alcohol gas that concentration process produces is stranded in and can not in time discharges in the said concentration tank 2; A part becomes liquid again, thereby influence concentrates speed], make the gas that produces in the concentration process be divided to rapidly in said condensing unit 4 and the said alcohol recycling can 3; Quicken the process that concentrates, shorten concentration time.On the said soup conveyance conduit 5 liquor piping pump 7 is installed, can realizes the smooth delivery of power of extract.All have heat-insulation layer 8 on the lateral wall of said extractor 1 and said concentration tank 2, between said extractor 1 inwall and the said heat-insulation layer 8 and between said concentration tank 2 inwalls and the said heat-insulation layer 8 conduction oil 9 is arranged, in the said conduction oil 9 electric heater 10 is arranged; Can heat through 10 pairs of said conduction oils 9 of said electric heater, thereby realize extract in the said extractor 1 and the concentrate in the said concentration tank 2 are heated, help the carrying out of extracting and concentrating.On the said extractor 1 stirring motor 11 is installed, carries out through the material in 11 pairs of said extractors 1 of stirring motor, make extraction rate faster, dna purity is higher.On said extractor 1 and the said concentration tank 2 Pressure gauge 12, oil level pipe 13 and heat conductive oil inlet 14 are installed all, can observe the pressure in said extractor 1 and the said concentration tank 2 easily, guarantee to extract and concentrate and carry out smoothly through said Pressure gauge 12; Through the amount that said oil level pipe 13 can be observed conduction oil, add conduction oils so that in time pass through said heat conductive oil inlet 14.
The multi-functional hot reflux extracting-concentration machine group of present embodiment is particularly useful in the production of heart disease curing drop pill the active ingredient of the Ligusticum wallichii and the red sage root being extracted, and dna purity is high, and cocnentration factor is big.
The multi-functional hot reflux extracting-concentration machine group of the present invention is applicable to the extraction of heat sensitive material, concentrated and receipts cream, and is applicable to that volatile oil extracts and reclaims.Technology is advanced, extracts, concentrates and reclaim and can carry out simultaneously, saves time, laborsaving, saving cost.Dna purity is high, and cocnentration factor is big.
The foregoing description only be for explain clearly that the invention does for example, and be not qualification to the invention specific embodiment.For the those of ordinary skill in affiliated field, on the basis of above-mentioned explanation, can also make other multi-form variation or change.Here need not also can't give exhaustive to all embodiments.And conspicuous variation of being extended out thus or change still are among the protection domain of the invention claim.

Claims (7)

1. multi-functional hot reflux extracting-concentration machine group; It is characterized in that; Comprise extractor (1), concentration tank (2), alcohol recycling can (3) and condensing unit (4); The gas vent at the gas vent at said extractor (1) top and said concentration tank (2) top respectively with said condensing unit (4) treat the conducting of condensed gas inlet fluid; The liquid inlet fluid communication of the condensate outlet of said condensing unit (4) and said alcohol recycling can (3), the medicine liquid outlet of said extractor (1) bottom is through the soup inlet fluid conducting of soup conveyance conduit (5) with said concentration tank (2) top.
2. multi-functional hot reflux extracting-concentration machine group according to claim 1 is characterized in that, liquor piping pump (7) is installed on the said soup conveyance conduit (5).
3. multi-functional hot reflux extracting-concentration machine group according to claim 1 is characterized in that, all has heat-insulation layer (8) on the lateral wall of said extractor (1) and said concentration tank (2).
4. multi-functional hot reflux extracting-concentration machine group according to claim 3; It is characterized in that; Between said extractor (1) inwall and the said heat-insulation layer (8) and between said concentration tank (2) inwall and the said heat-insulation layer (8) conduction oil (9) is arranged, electric heater (10) is arranged in the said conduction oil (9).
5. multi-functional hot reflux extracting-concentration machine group according to claim 1 is characterized in that, stirring motor (11) is installed on the said extractor (1).
6. according to claim 1-5 arbitrary one described multi-functional hot reflux extracting-concentration machine group, it is characterized in that, Pressure gauge (12), oil level pipe (13) and heat conductive oil inlet (14) all are installed on said extractor (1) and the said concentration tank (2).
7. according to the arbitrary described multi-functional hot reflux extracting-concentration machine group of claim 1-5; It is characterized in that; Said alcohol recycling can (3) is connected with vavuum pump through vacuum tube (6); And said alcohol recycling can (3) passes through suction tube (17) fluid communication with said concentration tank (2), and valve (18) is installed on the said suction tube (17).
CN201210041987.2A 2012-02-23 2012-02-23 Multifunctional hot reflux extracting and concentrating unit Expired - Fee Related CN102527066B (en)

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CN201210041987.2A CN102527066B (en) 2012-02-23 2012-02-23 Multifunctional hot reflux extracting and concentrating unit

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Application Number Priority Date Filing Date Title
CN201210041987.2A CN102527066B (en) 2012-02-23 2012-02-23 Multifunctional hot reflux extracting and concentrating unit

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CN102527066B CN102527066B (en) 2014-09-17

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103007571A (en) * 2012-12-19 2013-04-03 温州市天龙轻工设备有限公司 Alcohol-recyclable medicine extracting device and process thereof
CN105998126A (en) * 2016-05-18 2016-10-12 安徽瑞思威尔科技有限公司 Method for preparing Bozhou chrysanthemum general flavone extracting solution and concentrated solution by extraction and concentration machine

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2329428Y (en) * 1998-02-13 1999-07-21 石家庄市星烁实业公司 Reactor for preparing liquid crystal high polymer
CN2596984Y (en) * 2003-01-18 2004-01-07 刘燕湫 Chinese medicine extraction and concentration machine
WO2007042542A1 (en) * 2005-10-12 2007-04-19 Boehringer Ingelheim Pharma Gmbh & Co. Kg Improved method for the production of betulinic acid
CN102342304A (en) * 2011-08-10 2012-02-08 河南华泰粮油机械工程有限公司 Production method for extracting pyrethrin from pyrethrum

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2329428Y (en) * 1998-02-13 1999-07-21 石家庄市星烁实业公司 Reactor for preparing liquid crystal high polymer
CN2596984Y (en) * 2003-01-18 2004-01-07 刘燕湫 Chinese medicine extraction and concentration machine
WO2007042542A1 (en) * 2005-10-12 2007-04-19 Boehringer Ingelheim Pharma Gmbh & Co. Kg Improved method for the production of betulinic acid
CN102342304A (en) * 2011-08-10 2012-02-08 河南华泰粮油机械工程有限公司 Production method for extracting pyrethrin from pyrethrum

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103007571A (en) * 2012-12-19 2013-04-03 温州市天龙轻工设备有限公司 Alcohol-recyclable medicine extracting device and process thereof
CN103007571B (en) * 2012-12-19 2014-09-10 汪振朴 Alcohol-recyclable medicine extracting device and process thereof
CN105998126A (en) * 2016-05-18 2016-10-12 安徽瑞思威尔科技有限公司 Method for preparing Bozhou chrysanthemum general flavone extracting solution and concentrated solution by extraction and concentration machine

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Granted publication date: 20140917