CN105709456A - Ultrasonic hot reflux extraction condensation set - Google Patents
Ultrasonic hot reflux extraction condensation set Download PDFInfo
- Publication number
- CN105709456A CN105709456A CN201610253770.6A CN201610253770A CN105709456A CN 105709456 A CN105709456 A CN 105709456A CN 201610253770 A CN201610253770 A CN 201610253770A CN 105709456 A CN105709456 A CN 105709456A
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- pipeline
- unicom
- extraction
- valve
- pot
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0207—Control systems
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0215—Solid material in other stationary receptacles
- B01D11/0223—Moving bed of solid material
- B01D11/0234—Moving bed of solid material using other slow rotating arms or elements, whereby the general transport direction of the solids is not parallel to the rotation axis, e.g. perpendicular
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0261—Solvent extraction of solids comprising vibrating mechanisms, e.g. mechanical, acoustical
- B01D11/0265—Applying ultrasound
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0292—Treatment of the solvent
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0292—Treatment of the solvent
- B01D11/0296—Condensation of solvent vapours
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Physics & Mathematics (AREA)
- Acoustics & Sound (AREA)
- Automation & Control Theory (AREA)
- Mechanical Engineering (AREA)
- Extraction Or Liquid Replacement (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention discloses an ultrasonic hot reflux extraction condensation set. The ultrasonic hot reflux extraction condensation set comprises an electric control device, and a vacuum concentration device, an extraction device and a solvent recycling device which are mounted on an integrated rack in sequence, wherein a vacuum concentration tank in the vacuum concentration device is internally provided with a concentration stirrer; an extraction tank in the extraction device is internally provided with a stirrer and an ultrasonic generator and is used for forcedly extracting materials; the solvent recycling device and the extraction device form a communicated pipeline through a pipeline; a solvent is used for circularly extracting the materials in the set; and an oil-water separation can also be used for separating aromatic oil. The ultrasonic hot reflux extraction condensation set disclosed by the technical scheme has the advantages of shortening extraction and concentration time, improving the extraction effect, and saving the solvent, and is high in concentration efficiency.
Description
Technical field
The present invention relates to the extraction abstraction technique field of material, particularly relate to a kind of ultrasonic heat backflow extraction concentration group.
Background technology
Existing plant, animality material effective ingredient extraction, the main mode adopting solvent dissolution to separate concentration again is extracted, namely according to certain solid-to-liquid ratio, material to be extracted is put into and puts in extraction element together with solvent such as water or other organic solvents, at a certain temperature the effective ingredient of material is extracted.Also there is the report adopting ultrasonic technology strengthening extraction effect, but there is also structure complexity, the material away from supersonic generator is extracted strengthening effect bad, it is impossible to carrying out the extraction concentration of aromatic oil composition, solvent makes the problem that consumption is big.
Summary of the invention
In view of the deficiency of prior art existence, the purpose of the present invention aims to provide a kind of simple in construction, and it is effective that material is extracted strengthening by supersonic generator, it is possible to carry out the ultrasonic heat backflow extraction concentration group that extraction concentrates and solvent makes consumption few of aromatic oil composition.For reaching object above, the present invention realizes by the following technical solutions, a kind of ultrasonic heat backflow extraction concentration group, including electric control gear 4 and the vacuum concentrating apparatus 1 being sequentially arranged in integral type frame 19, extraction element 2, solvent recovery unit 3, described vacuum concentrating apparatus 1 includes vacuum concentration pot 16, it is installed on the concentration agitator 11 in vacuum concentration pot 16, described vacuum concentration pot 16 top is provided with the first pipeline 12 and is terminated with the first valve 13 outside, described vacuum concentration pot 16 upper end be provided with second pipe 14 by the second valve 15 respectively with the 6th pipeline 213 and the 9th pipeline 313 UNICOM, described vacuum concentration pot 16 lower end is provided with the 3rd valve 17, described 3rd valve 17 is arranged below sealing and receives cream cylinder 18, described extraction element 2 includes extraction pot 21 upper end described in extraction pot 21 and is provided with a charging aperture 214, described extraction pot 21 upper end is additionally provided with the 6th pipeline 213, described extraction pot 21 top is provided with the 5th pipeline 211 by the 4th valve 212 and threeway 111 and the first valve 13 and the 4th pipeline 29 UNICOM, described extraction pot 21 top is additionally provided with the 5th valve 34, described extraction pot 21 is internal is provided with extraction agitator 22 and supersonic generator 23, described extraction pot 21 lower end is provided with slag notch filter screen 24, described slag notch filter screen 24 lower end couples the 3rd pipeline 25, described 3rd pipeline 25 port of export and delivery pump 26 entrance point UNICOM, described delivery pump 26 port of export and extracting solution filter 28 entrance point UNICOM, described extracting solution filter 28 port of export the 4th pipeline 29 UNICOM, described extracting solution filter 28 entrance point is also linked with sewage draining valve 27, described solvent recovery unit 3 includes solvent recovery tank 31, described solvent recovery tank 31 top is provided with solvent recovery import and the 6th valve 35 UNICOM, described 6th valve 35 and the 7th pipeline 36 UNICOM, UNICOM bottom described 7th pipeline 36 and oil water separator 38, described oil water separator 38 lower end is additionally provided with draining valve 37, described oil water separator 38 upper end is linked with vacuum buffer tank 39, described vacuum buffer tank 39 upper end is linked with vacuum line 32, middle part is by the 8th pipeline 310 and cooler 311 UNICOM, described cooler 311 and condenser 312 UNICOM, described condenser 312 and the 9th pipeline UNICOM 313, described vacuum line 32 and vacuum pump 314 UNICOM.
The present invention is further set to, and described 7th pipeline 36 is serpentine bend pipe, and described 6th valve 35 and the 7th pipeline 36 UNICOM position are the bottom that on the 7th pipeline 36, U-bend is bent.
The invention have the benefit that employing the technical program can realize Effect of Alcohol Extracting Procedureto Total on the one hand, especially by agitator and supersonic generator mating reaction in extraction pot, material is stirred continuously near supersonic generator and enhances extraction effect；On the other hand, once reinforced rear solvent uses at airtight equipment internal recycle, and the effective ingredient in raw material can constantly extract, so with doses conservation more than 30% under identical extracted amount, reducing and extract concentration time, improves thickening efficiency, saves solvent；Thirdly through condenser and oil water separator mating reaction not only can reclaim organic solvent, it is also possible to the aromatic oil in separation and Extraction material.
Accompanying drawing explanation
Fig. 1 is present configuration schematic diagram.
Detailed description of the invention
As shown in Figure 1, a kind of ultrasonic heat backflow extraction concentration group, including electric control gear 4 and the vacuum concentrating apparatus 1 being sequentially arranged in integral type frame 19, extraction element 2, solvent recovery unit 3, vacuum concentrating apparatus 1 includes vacuum concentration pot 16, it is installed on the concentration agitator 11 in vacuum concentration pot 16, it is provided with the first pipeline 12 on vacuum concentration pot 16 top and is terminated with the first valve 13 outside, be additionally provided with in vacuum concentration pot 16 upper end second pipe 14 by the second valve 15 respectively with the 6th pipeline 213 and the 9th pipeline 313 UNICOM, it is provided with the 3rd valve 17 in vacuum concentration pot 16 lower end, 3rd valve 17 is arranged below sealing and receives cream cylinder 18；Extraction element 2 includes extraction pot 21, extraction pot 21 upper end is provided with a charging aperture 214, extraction pot 21 upper end is additionally provided with the 6th pipeline 213, extraction pot 21 top is provided with the 5th pipeline 211 by the 4th valve 212 and threeway 111 and the first valve 13 and the 4th pipeline 29 UNICOM, extraction pot 21 top is additionally provided with the 5th valve 34, extraction pot 21 is internal is provided with extraction agitator 22 and supersonic generator 23, extraction pot 21 lower end is provided with slag notch filter screen 24, slag notch filter screen 24 lower end couples the 3rd pipeline 25, 3rd pipeline 25 port of export and delivery pump 26 entrance point UNICOM, delivery pump 26 port of export and extracting solution filter 28 entrance point UNICOM, extracting solution filter 28 port of export the 4th pipeline 29 UNICOM, extracting solution filter 28 entrance point is also linked with sewage draining valve 27, solvent recovery unit 3 includes solvent recovery tank 31, solvent recovery tank 31 top is provided with solvent recovery import and the 6th valve 35 UNICOM, 6th valve 35 and the 7th pipeline 36 UNICOM, UNICOM bottom 7th pipeline 36 and oil water separator 38, oil water separator 38 lower end is additionally provided with draining valve 37, oil water separator 38 upper end is linked with vacuum buffer tank 39, vacuum buffer tank 39 upper end is linked with vacuum line 32, middle part is by the 8th pipeline 310 and cooler 311 UNICOM, cooler 311 and condenser 312 UNICOM, condenser 312 and the 9th pipeline UNICOM 313, vacuum line 32 and vacuum pump 314 UNICOM.
The present invention is further set to, and the 7th pipeline 36 is serpentine bend pipe, and the 6th valve 35 and the 7th pipeline 36 UNICOM position are the bottom that on the 7th pipeline 36, U-bend is bent.
The technical program operation principle: put into quantitative thing to be extracted by dog-house 214 when extracting work and be mixed in extraction pot 21 with solvent, under the control of electric control gear 4, carrying out temperature control heating and regulate temperature, agitator 22 and supersonic generator 23 are opened simultaneously, carry out mixed liquor forcing to extract；Open the first valve 13, close the 4th valve 212, under delivery pump 26 acts on, the solvent containing leachable is passed sequentially through slag notch filter screen 24, 3rd pipeline 25, extracting solution filter 28, 4th pipeline 29, threeway 111, first valve 13, first pipeline 12 enters vacuum concentration pot 16, after vacuum pump 314 evacuation, solvent evaporates, and through second pipe 14 second valve 15, 9th pipeline 313 enters condenser 312, meet cold post liquefaction and enter cooler 311, vacuum buffer tank 39 is entered again through the 8th pipeline 310, subsequently flow into oil water separator 38 and carry out oil-water separation, solvent reenters in extraction pot 21 by the 7th pipeline 36 and adjusting valve door 34, material is extracted by circulation.Effective ingredient leads to the 3rd valve 17 of its lower end and enters in sealing receipts cream cylinder 18 after concentrating accumulation in vacuum concentration pot 16.Extract complete, close the 5th valve 34, open the 6th valve 35, make solvent flow in solvent recovery tank 31, use again in order to next time.The aromatic oil extracted can be discharged by the oil extraction valve 37 of oil water separator 38.
Claims (2)
1. a ultrasonic heat backflow extraction concentration group, including electric control gear (4) and the vacuum concentrating apparatus (1) that is sequentially arranged in integral type frame (19), extraction element (2), solvent recovery unit (3), it is characterized in that: described vacuum concentrating apparatus (1) includes vacuum concentration pot (16), it is installed on the concentration agitator (11) in vacuum concentration pot (16), described vacuum concentration pot (16) top is provided with the first pipeline (12) and is terminated with the first valve (13) outside, described vacuum concentration pot (16) upper end be provided with second pipe (14) by the second valve (15) respectively with the 6th pipeline (213) and the 9th pipeline (313) UNICOM, described vacuum concentration pot (16) lower end is provided with the 3rd valve (17), described 3rd valve (17) is arranged below sealing and receives cream cylinder (18), described extraction element (2) includes extraction pot (21) described extraction pot (21) upper end and is provided with a charging aperture (214), described extraction pot (21) upper end is additionally provided with the 6th pipeline (213), described extraction pot (21) top is provided with the 5th pipeline (211) by the 4th valve (212) and threeway (111) and the first valve (13) and the 4th pipeline (29) UNICOM, described extraction pot (21) top is additionally provided with the 5th valve (34), described extraction pot (21) is internal is provided with extraction agitator (22) and supersonic generator (23), described extraction pot (21) lower end is provided with slag notch filter screen (24), described slag notch filter screen (24) lower end couples the 3rd pipeline (25), described 3rd pipeline (25) port of export and delivery pump (26) entrance point UNICOM, described delivery pump (26) port of export and extracting solution filter (28) entrance point UNICOM, described extracting solution filter (28) port of export the 4th pipeline (29) UNICOM, described extracting solution filter (28) entrance point is also linked with sewage draining valve (27), described solvent recovery unit (3) includes solvent recovery tank (31), described solvent recovery tank (31) top is provided with solvent recovery import and the 6th valve (35) UNICOM, described 6th valve (35) and the 7th pipeline (36) UNICOM, described 7th pipeline (36) and oil water separator (38) bottom UNICOM, described oil water separator (38) lower end is additionally provided with draining valve (37), described oil water separator (38) upper end is linked with vacuum buffer tank (39), described vacuum buffer tank (39) upper end is linked with vacuum line (32), middle part is by the 8th pipeline (310) and cooler (311) UNICOM, described cooler (311) and condenser (312) UNICOM, described condenser (312) and the 9th pipeline UNICOM (313), described vacuum line (32) and vacuum pump (314) UNICOM.
2. a kind of ultrasonic heat backflow extraction concentration group according to claim 1, it is characterized in that: described 7th pipeline (36) is serpentine bend pipe, described 6th valve (35) and the 7th pipeline (36) UNICOM position are the bottom that the upper U-bend of the 7th pipeline (36) is bent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610253770.6A CN105709456A (en) | 2016-04-22 | 2016-04-22 | Ultrasonic hot reflux extraction condensation set |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610253770.6A CN105709456A (en) | 2016-04-22 | 2016-04-22 | Ultrasonic hot reflux extraction condensation set |
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| CN105709456A true CN105709456A (en) | 2016-06-29 |
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| CN201610253770.6A Pending CN105709456A (en) | 2016-04-22 | 2016-04-22 | Ultrasonic hot reflux extraction condensation set |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109011692A (en) * | 2018-08-21 | 2018-12-18 | 宁夏医科大学 | Use for laboratory traditional Chinese medicine effective ingredient extraction system and extracting method |
| CN112619199A (en) * | 2020-11-04 | 2021-04-09 | 福建智罗科技有限公司 | Ultrasonic reflux extraction and concentration equipment |
| CN115430185A (en) * | 2022-10-14 | 2022-12-06 | 甘肃中医药大学 | Extraction, filtration and concentration device for polysaccharide components for processing traditional Chinese medicine health products |
Citations (5)
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| WO1995022387A1 (en) * | 1992-10-26 | 1995-08-24 | Chemical Industry Consultants, Inc. | Method of gelatin recovery and purification from encapsulation process |
| CN101234264A (en) * | 2007-11-20 | 2008-08-06 | 黄宗玉 | Miniaturization extracting concentrating machine group and high-efficiency type preparation production technique thereof |
| CN101612487A (en) * | 2009-06-16 | 2009-12-30 | 江苏七○七天然制药有限公司 | The extraction of effective components of Chinese medicinal and concentrator and extraction and method for concentration |
| CN201592000U (en) * | 2010-01-11 | 2010-09-29 | 徐子亮 | Ultrasonic Chinese traditional medicine extracting tank |
| CN205549674U (en) * | 2016-04-22 | 2016-09-07 | 瑞安市新莱流体设备有限公司 | Concentration machine set is drawed in ultrasonic wave hot reflux |
-
2016
- 2016-04-22 CN CN201610253770.6A patent/CN105709456A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1995022387A1 (en) * | 1992-10-26 | 1995-08-24 | Chemical Industry Consultants, Inc. | Method of gelatin recovery and purification from encapsulation process |
| CN101234264A (en) * | 2007-11-20 | 2008-08-06 | 黄宗玉 | Miniaturization extracting concentrating machine group and high-efficiency type preparation production technique thereof |
| CN101612487A (en) * | 2009-06-16 | 2009-12-30 | 江苏七○七天然制药有限公司 | The extraction of effective components of Chinese medicinal and concentrator and extraction and method for concentration |
| CN201592000U (en) * | 2010-01-11 | 2010-09-29 | 徐子亮 | Ultrasonic Chinese traditional medicine extracting tank |
| CN205549674U (en) * | 2016-04-22 | 2016-09-07 | 瑞安市新莱流体设备有限公司 | Concentration machine set is drawed in ultrasonic wave hot reflux |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109011692A (en) * | 2018-08-21 | 2018-12-18 | 宁夏医科大学 | Use for laboratory traditional Chinese medicine effective ingredient extraction system and extracting method |
| CN112619199A (en) * | 2020-11-04 | 2021-04-09 | 福建智罗科技有限公司 | Ultrasonic reflux extraction and concentration equipment |
| CN115430185A (en) * | 2022-10-14 | 2022-12-06 | 甘肃中医药大学 | Extraction, filtration and concentration device for polysaccharide components for processing traditional Chinese medicine health products |
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Application publication date: 20160629 |
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