CN201073563Y - High-efficiency energy-saving device integrating and concentrating - Google Patents

High-efficiency energy-saving device integrating and concentrating Download PDF

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Publication number
CN201073563Y
CN201073563Y CNU200720104854XU CN200720104854U CN201073563Y CN 201073563 Y CN201073563 Y CN 201073563Y CN U200720104854X U CNU200720104854X U CN U200720104854XU CN 200720104854 U CN200720104854 U CN 200720104854U CN 201073563 Y CN201073563 Y CN 201073563Y
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China
Prior art keywords
concentration
extractor
heater
condenser
extraction
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Expired - Fee Related
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CNU200720104854XU
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Chinese (zh)
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覃日宝
覃强
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TAN RIBAO TAN QIANG
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TAN RIBAO TAN QIANG
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Abstract

The utility model relates to an extraction and concentration equipment for pharmacy, food, chemical engineering and such industries, which comprises an extraction pot, a condenser, a filter and a heater. The utility model integrates the extraction pot and a concentration vaporizing tank together. The concentration vaporizing tank is sleeved at the outside of the extraction pot. A feeding opening is arranged at the upper part of the extraction pot. A liquid discharge hole and a slag discharge door are arranged at the lower part of the extraction pot. The concentration vaporizing tank outer layer is provided with a liquid inlet at the upper part, a viewing lens and the heater at the central section, and the condenser on the top part. The outlet of the condenser is connected with a cooler which is provided with a valve and a tee pipe at the bottom. One end of the tee pipe is connected with the upper part of the concentration vaporizing tank, one end is connected with extraction pot and one end acts as solvent outlet for reclamation. The liquid discharge hole at the lower part of the extraction pot is connected with the filter. The extracted liquid is transmitted to the liquid inlet of the concentration vaporizing tank by a liquid pump. The utility model has the advantages of energy-efficient, high efficiency and small size, which can complete the extraction, reflow, concentration and reclamation at the same time.

Description

Energy-efficient extraction concentrates equipment integrating
Technical field
The utility model relates to extraction, the concentrator of industries such as a kind of pharmacy, food, chemical industry.
Background technology
Nowadays continuous development along with pharmacy, food, chemical industry has entered the energy-efficient epoch.In industries such as pharmacy, food to extract, the requirement of aspects such as the refining of concentrator, practicality, efficient, energy-saving and environmental protection, small investment is more and more higher.In the device fabrication industry, improve on also constantly for device structure.But do not change traditional discrete extractor and discrete concentration tank all the time.Or the thermal cycle that proposes in the present device fabrication industry is extracted, is concentrated in and has done very big change on the pipeline mounting process, but finally still single device is installed on each discrete platform, still the equipment that can't resolve is installed and is taken the place greatly, pipeline connects many and grows, and it is many to operate not convenient administrative staff.Because traditional discrete extractor need be thrown solvent and the water yield is many, general all in (8-10) of the total raw material amount about doubly, so the solution that draws is many especially, adds and extract several times that elapsed time is long to be influenced production efficiency and waste energy.And discrete concentration tank, in concentration process, needing powerful vacuum system and replenish a large amount of cooling waters, the indirect steam that comes comprehensive evaporator to be evaporated so just can reach the condensation demand of traditional discrete evaporator.So traditional discrete extraction, evaporation and concentration jar are relatively to waste energy and water resource.
At wasting energy and the water resource shortcoming that the extraction of industries such as present pharmacy, food, chemical industry, concentrator exist, people have carried out some improvement to these equipment, what have has increased insulation outside equipment, the measure of passing through recovery hot water or bled steam tail gas that has cuts down the consumption of energy, open source literature has also been reported the structure of some improved extractions, concentrator, for example:
1, Chinese patent: application (patent) number: 00223536.6 applying date: 2000.06.30 title: continous way circulation extraction-concentrator application (patent right) people: Kexin Electromechanical Equipment Co., Ltd. Shifang, the address: two crossing, Shifang City, Sichuan Province town, summary: a concentrator is extracted in a kind of continous way circulation.Mainly comprise extractor, concentration heater, concentration evaporator, condenser etc., it is characterized by concentration evaporator is communicated with extractor, condenser respectively, steam in the extractor enters condenser behind vapour liquid separator, the solvent of separation or condensation flows back to extractor, the extractor bottom is communicated with concentration heater, concentration heater is communicated with concentration evaporator again up and down, and extraction one concentration process is constantly circulated.Characteristics such as extraction, a concentrated shared cover condensation, cooling device are equipped with the forced circulation propeller in evaporation concentrator, the utlity model has simple and compact device, and be efficient, energy-conservation.
2, Chinese patent, application (patent) number: 200510010625.7 applyings date: 2005.01.28 title: a kind of Chinese medicine preparation technology and complete set of equipments application (patent right) people thereof: Yunnan Kunming Shipbuilding Design ﹠ Research Institute address: technical foundation portion of No. 6 elder brother's ships of Kunming, Yunnan Province Renmin Zhonglu mansion Yunnan Kunming Shipbuilding Design ﹠ Research Institute, summary: a kind of Chinese medicine preparation technology and complete set of equipments thereof, its technology comprise that extraction, Separation of Solid and Liquid, pasteurization and the vacuum of carrying out successively concentrate.Its complete set of equipments includes extraction equipment, solid-liquid separating equipment, sterilizing unit and the vacuum concentration equipment that is linked in sequence by feed liquid pipeline.The present invention can disposablely finish separate impurities, the sterilization of soup and the concentration process of soup in the extraction, soup of Chinese medicine material active ingredient continuously, and produce respectively as required and obtain dry powder or thick paste, the automation degree of equipment height, the production efficiency height, energy consumption is low, it is convenient to clean, and it is low to produce the product bacteria containing amount that obtains, steady quality.
3, Chinese patent, application (patent) number: the 98230191.X applying date: 1998.02.19 title: high-efficiency multi-function Chinese medicine extracts enrichment facility application (patent right) people continuously: skin Jie minister address: hengyang, hunan province city pharmacy apparatus factory, summary: the disclosed high-efficiency multi-function Chinese medicine of the utility model extract continuously enrichment facility by extractor, tube still heater, preparation tank, lead rotary separator, condenser, vacuum collecting device, cartridge filter, delivery pump, steam-water separator, dispensing cartridge, filter and be connected by pipeline, valve, interpenetrating forms.Compare with the technology of pharmaceutically active ingredient during existing traditional Chinese medicine extraction jar extracts, have extraction time short, recovery rate is high, 95%, advantage such as cocnentration factor is big, energy-conservation, and can realize full-automation production.It is good that the herb liquid that adopts the utility model to extract has quality, qualities such as strong fragrance.
4, Chinese patent, application (patent) number: 200420041514.3 applyings date: 2004.02.10 title: circulating multi-functional extraction concentrates unit application (patent right) people: Fu builds prosperous address: Yangling District science and education street, Shaanxi Province autumn garden 5-131, summary: the utility model discloses a kind of circulating multi-functional extraction and concentrate unit, it is to be connected to form with pipeline by siphon type multifunctional extractor, receiver, vavuum pump, fluid flowmeter, triple valve and triple valve, thin film evaporator, vapour liquid separator, economic benefits and social benefits condenser, surge tank etc.Circulating multi-functional extraction of the present utility model concentrates unit, can be widely used in the extraction of all kinds of materials in medicine, chemical industry and the food industry and concentrates; Extracting, remove the silt precipitation, filtering, concentrate and solvent recovery is once finished, saved the man power and material, shortened the production cycle, reduced production cost.Adopt economic benefits and social benefits condenser and reflux operation etc., realized the extraction that repeatedly circulates of a solubilizer, improved extraction ratio of effective constituents and solvent recovering rate; Adopt the siphon type multifunctional extractor to realize automatic fitration and automatic infusion; Whole operation all is to carry out under closed state, helps safety in production and environmental requirement.
Above-mentioned open source literature has solved that a part wastes energy and the problem of water resource, but can't can reach high-quality extraction process simultaneously on an equipment, can finish concentrated technological requirement again.
Summary of the invention
The purpose of this utility model provides a kind of can combining extractor and concentration tank together, unites two into one, and has occupation of land less, when economizing material, efficient, characteristics of energy saving, finish extractions, reflux, and concentrates, recovery, and multiple function is the equipment of one.
The utility model is achieved in that energy-efficient extraction concentrates equipment integrating and comprises extractor, condenser, filter, heater, be characterized in: extractor and concentration and evaporation jar are made of one, the concentration and evaporation jar is enclosed within the extractor outside, extractor top is provided with dog-house, the bottom is provided with liquid outlet and ash gate, outer field concentration and evaporation jar top is provided with inlet, and heater and visor are installed in the middle part, and condenser is installed at the top; Condensator outlet connects cooler, and the cooler bottom is connected to valve and three-way pipe, and one crosses the top that U type pipe is received the concentration and evaporation jar all, two logical tops of receiving extractor by straight tube, and three connect solvent solvent outlet recovery tube.
The liquid outlet of extractor bottom is received filter, and the liquid after will being extracted by liquid-feeding pump then is to the top inlet of concentration and evaporation jar.
Above-described condenser is in-line arrangement or coil condenser, can adopt the cooling of water or organic liquid.
Above-described heater is a steam heater, and perhaps electric heater also can adopt the hot gas heater.
Installation method of the present utility model is: earlier the extractor of internal layer is made according to technology, then outer concentration tank and the combination of internal layer extractor are made, again the heater of outer concentration tank and internal layer extractor is pressed mounting process and installs, at last inside and outside layer extract concentration tank evaporation tube, overhead condenser, connect and carry accessories such as hot-water line, cooler and install and just can form the concentrated integrated tank of energy-efficient extraction.
Compared with prior art, the utility model has the advantages that:
1, with existing extraction, concentrate and to separate two-part equipment and be integrated, change traditional discrete extraction, concentration tank, be implemented on the equipment and promptly can finish the extraction process requirement, can finish the concentration technology requirement again, a kind of energy-efficient integrated tank equipment simultaneously.
2, compact conformation, occupation of land less, utilization rate of equipment and installations height, low cost of manufacture, small investment less manpower simple to operate.Adopt inside and outside layer structure and the circulation of indirect steam condensation heat to extract, the indirect steam that can make full use of outer waste heat and concentration and evaporation extracts the efficiency of utilization height, can save a large amount of heat energy.
3, this equipment is owing to the heating process of outer layered heating in the process internal layer extraction just of heating evaporation.Add the hot water that condenses that outer indirect steam condensation of evaporating is got off, energy is gradient stripping extract fully, so extraction time shortens greatly.Next is to extract, concentrate and carry out the utilization rate of equipment and installations height synchronously, reduces a large amount of transitional links such as storage liquid, and the operating time reduces, and can reduce a large amount of thermal energy consumptions.
4, this equipment is because of adopting the disposable solvent that adds, and inside and outside layer extracts continuously, concentrates, condensation cycle is carried out.Can guarantee periodic duty in the structure of the inside and outside layer of a set of equipment to extracting, concentrating, make like this extract more abundant, receive cream rate height, effective component content is also high.Can guarantee color and pure.
5, this equipment is the equipment that extractor and concentration tank are combined together, pollutes so reduce a lot of transition, can protect the Cheng quality, if use and traditional Chinese medicine extraction, more can meet the requirement of GMP.In addition, this equipment is combined into extraction, is concentrated integrated tank by the outer evaporation and concentration jar of internal layer extractor.Changed extraction, concentration integrated technology in the industries such as food, pharmacy, chemical industry, significant to cutting down the consumption of energy.
Description of drawings
Fig. 1 is the structural representation that energy-efficient extraction of the present utility model concentrates equipment integrating.
The specific embodiment
As shown in Figure 1, extractor and concentration and evaporation jar are made of one, concentration and evaporation jar 8 is enclosed within extractor 1 outside, extractor 1 top is provided with dog-house 2, the bottom is provided with liquid outlet 4 and ash gate 3, outer field concentration and evaporation jar 8 tops are provided with inlet 9, heater 10 and visor 11 are installed in the middle part, heater 10 is a steam heater, and perhaps electric heater also can adopt the hot gas heater, concentration and evaporation jar 8 tops are evaporation tubes 12, condenser 13 is installed in evaporation tube 12 tops, and condenser 13 adopts in-line arrangement or coil condenser, adopts water cooling; Condensator outlet connects cooler 15, the cooler bottom is connected to valve and three-way pipe, the cooler bottom is connected to valve and three-way pipe, one crosses the top that U type pipe 17 is received concentration and evaporation jar 8 all, two logical tops of receiving extractor 1 by straight tube 14, three connect solvent solvent outlet recovery tube 18, reclaim purposes as the solvent solvent outlet.
The liquid outlet 4 of extractor 1 bottom is received filter 5, and the liquid after will being extracted by drawing liquid pump 6 then is transported to the top inlet 9 of concentration and evaporation jar 8 by last liquid pipe 7.
Method of operating
1, uses the tightness and the reliability of the energy-efficient extraction of pre-operational check, concentrated each parts of integrated tank.
2, medicine material is dropped into the extractor dog-house 2 of internal layer; Add solvent in proportion, closed feeding door 2; Liquid in-out mouth 4 adding steam from internal layer extractor 1 can add to boiling back steam off then.Open filter 5; Starting drawing liquid pump 6; Deliver to the inlet 9 of outer field concentration and evaporation jar 8 from last liquid pipe 7; Account for (1/3) back closing liquid filter 5 of total throwing liquid measure; Close drawing liquid pump 6; Close extractor feed liquor, steam ports 4; Open the heater 10 of outer field concentration and evaporation jar simultaneously; Start vaporizer concentrates, and produces indirect steam simultaneously and rises to evaporation tube 12; Open condenser 13; Indirect steam enters condenser 13; Forming a large amount of condensate water or solvent flows to connect and carries hot-water line 14; Enter the extractor 1 of internal layer; Form a working cycles.Multiple operation is returned in this circulation finished, open extractor ash gate 3 until the content of material effective ingredient is extracted fully; Whether drain slag thing in the internal layer extractor from the new material of new input, inspecting outer field liquid material proportion simultaneously by random samples can be from outer field evaporation and concentration jar liquid outlet 16 after up to specification; Emit.Simultaneously can be with indirect steam condensed water or solvent from cooler 15; Flow into the extractor 1 of basin or internal layer; As using liquid next time.Also can carry out the reflux technique operation, evaporate after evaporation tube 12 by outer solvent with skin; Flow into condenser 13; Through U type pipeline section 17; Flow back to outer evaporator or through reclaiming pipeline section 18; Be recovered to the extractor of receiver or internal layer.Return with such operation sequence multiple carry out just can being extracted, reflux, reclaim, concentrate, efficient, energy-conservation, convenient, good effect.

Claims (3)

1. an energy-efficient extraction concentrates equipment integrating, comprise extractor, condenser, filter, heater, it is characterized in that: extractor and concentration and evaporation jar are made of one, concentration and evaporation jar (8) is enclosed within extractor (1) outside, extractor (1) top is provided with dog-house (2), the bottom is provided with liquid outlet (4) and ash gate (3), outer field concentration and evaporation jar (8) top is provided with inlet (9), heater (10) and visor (11) are installed in the middle part, concentration and evaporation jar (8) top is evaporation tube (12), condenser (13) is installed in evaporation tube (12) top, condensator outlet connects cooler (15), and the cooler bottom is connected to valve and three-way pipe, and one crosses the top that U type pipe (17) is received concentration and evaporation jar (8) all, two lead to the top of being received extractor (1) by straight tube (14), and three connect solvent solvent outlet recovery tube (18).
2. energy-efficient extraction according to claim 1 concentrates equipment integrating, it is characterized in that: described condenser (13) is in-line arrangement or coil condenser, adopts the cooling of water or organic liquid.
3. energy-efficient extraction according to claim 1 concentrates equipment integrating, it is characterized in that: described heater (10) is steam heater, electric heater, perhaps adopts the hot gas heater.
CNU200720104854XU 2007-07-28 2007-07-28 High-efficiency energy-saving device integrating and concentrating Expired - Fee Related CN201073563Y (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102778044A (en) * 2011-05-11 2012-11-14 黄太清 Heating device for gathering electromagnetic wave energy
CN112494971A (en) * 2020-12-08 2021-03-16 重庆医药高等专科学校 Burn and scald film spraying medicament raw material component dynamic extraction device
CN113509739A (en) * 2021-06-03 2021-10-19 广西锦东自动化设备有限公司 Non-reflux rapid juice discharging method for evaporating pot
CN113637090A (en) * 2021-08-10 2021-11-12 张明勋 Paper mulberry branch and bark material separation, decoction and extraction system and method
CN114455552A (en) * 2022-03-07 2022-05-10 盛隆资源再生(无锡)有限公司 Treatment device and treatment method for high-COD waste acid

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102778044A (en) * 2011-05-11 2012-11-14 黄太清 Heating device for gathering electromagnetic wave energy
CN102778044B (en) * 2011-05-11 2017-02-15 黄太清 Heating device for gathering electromagnetic wave energy
CN112494971A (en) * 2020-12-08 2021-03-16 重庆医药高等专科学校 Burn and scald film spraying medicament raw material component dynamic extraction device
CN113509739A (en) * 2021-06-03 2021-10-19 广西锦东自动化设备有限公司 Non-reflux rapid juice discharging method for evaporating pot
CN113637090A (en) * 2021-08-10 2021-11-12 张明勋 Paper mulberry branch and bark material separation, decoction and extraction system and method
CN113637090B (en) * 2021-08-10 2022-07-12 张明勋 Paper mulberry branch and bark material separation, decoction and extraction system and method
CN114455552A (en) * 2022-03-07 2022-05-10 盛隆资源再生(无锡)有限公司 Treatment device and treatment method for high-COD waste acid
CN114455552B (en) * 2022-03-07 2023-03-31 盛隆资源再生(无锡)有限公司 Treatment device and treatment method for high-COD waste acid

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C14 Grant of patent or utility model
GR01 Patent grant
C17 Cessation of patent right
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20080618

Termination date: 20120728