CN201304262Y - Continuous extracting concentration device - Google Patents
Continuous extracting concentration device Download PDFInfo
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- CN201304262Y CN201304262Y CNU2008202015904U CN200820201590U CN201304262Y CN 201304262 Y CN201304262 Y CN 201304262Y CN U2008202015904 U CNU2008202015904 U CN U2008202015904U CN 200820201590 U CN200820201590 U CN 200820201590U CN 201304262 Y CN201304262 Y CN 201304262Y
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- constant temperature
- condensation chamber
- temperature sleeve
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- extraction
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Abstract
The utility model provides a continuous extracting concentration device. The continuous extracting concentration device is characterized in that the concentration device is divided into a reflow extractor 1, a filter 2 and a concentrator 3 from left to right, the filter 2 at the middle part is respectively connected with the reflow extractor 1 on the left and the concentrator 3 on the right, and the upper end of the concentrator 3 is connected with the reflow extractor 1 to form a loop. The upper end of the concentrator 3 is connected with the reflow extractor 1 to form the loop. The reflow extractor 1 comprises a constant-temperature sleeve 11, an extraction container 12, a control panel 13, a steam pipe 14, a condensation chamber 15 and a condensation pipe 16. The concentrator 3 comprises a constant-temperature sleeve 31, a concentration container 32, a control panel 33, a steam chamber 34, a steam chamber cover 35 and a steam lead pipe 36. The continuous extracting concentration device has the advantage that multiple extractions can be continuously and repeatedly carried out when solvent is added once; the extracting time is short, the extraction and concentration are finished in one time, the efficiency is high, energy and solvent are saved, the operation is simple, and the cost is low.
Description
Technical field
The utility model relates to material extractive technique field, is specifically related to a kind of continuous extraction enrichment facility.
Background technology
Contain the number of chemical material in the plant, character according to active component in the plant, people adopt different solvents to extract separation, from plant, extract and isolate active ingredient, for the active ingredient in the plant is come out completely, often repeatedly extract, promptly extract first with certain amount of solvent earlier, filter then extracting liquid filtering is isolated filtrate, filter residue adds certain amount of solvent again and carries out the extraction second time, refilter separation, so repeat for the third time, or the 4th time ... wait repeatedly to extract and separate, collect all filtrate at last, concentrate, obtain containing the concentrate or the thickened solid of effective ingredients in plant, this traditional extraction separation method is in daily use in the extraction of effective ingredients in plant, however this method complicated operation not only, time is long, and the quantity of solvent of using is big, both wastes energy, and wastes solvent again, cost height, effect are also bad.Therefore need improve this method, this must design a kind of device, a certain amount of vegetable solid and certain amount of solvent are extracted continuously, make it once add the extraction that solvent carries out repeated multiple times, improve extraction efficiency, simultaneously also carry out concentration, after extraction is finished, can obtain extracting concentrate.Do not see at present the report that this type of device is arranged.
The utility model content
At the problems referred to above, the purpose of this utility model is to provide a kind of continuous extraction enrichment facility, in the extraction of effective ingredients in plant, add certain amount of solvent, can carry out continuous repeated multiple times extracts, improve extraction efficiency, when extracting, also can carry out concentration, can obtain extracting concentrate at last.
For achieving the above object, the utility model adopts following technical scheme:
Extract enrichment facility continuously, from left to right be divided into refluxing extraction device 1, filter 2 and inspissator 3 three parts, the filter 2 of mid portion is connected with the refluxing extraction device 1 on the left side and the inspissator 3 on the right respectively, and the upper end of inspissator 3 is connected with refluxing extraction device 1, forms a loop.
Above-mentioned refluxing extraction device 1 comprises constant temperature sleeve 11, extraction vessel 12, control panel 13, steam pipe 14, condensation chamber 15 and condenser pipe 16, constant temperature sleeve 11 is a column type, interior having heaters, and be connected with temp sensing controller, around bottom heating tube is uniformly distributed in and the side, to keep temperature constant, constant temperature sleeve 11 also has a upper port, extraction vessel 12 is cylindrical, be used to load plant and the solvent that extracts usefulness, can freely pick and place by the upper port of constant temperature sleeve 11 in constant temperature sleeve 11, the lower end of the suitable for reading and condensation chamber 15 of extraction vessel 12 links to each other, and there is an outlet that exceeds the bottom slightly extraction vessel 12 lower ends, and barrier film is arranged in the outlet, the plant filter residue of isolating extraction vessel 12, this outlet is connected with filter 2, and control panel 13 is in the side below the constant temperature sleeve 11, is provided with thermoregulator and timer, can regulate temperature and extraction time according to the plant extract condition, but jingle bell prompting after extraction is finished.
The lower end of above-mentioned condensation chamber 15 is connected with extraction vessel 12, one aperture is arranged at the bottom, be used for solvent refluxing with condensation to extraction vessel 12, one side of condensation chamber 15 lower ends also is connected with the steam lead 36 of inspissator 3, so that the steam that inspissator 3 produces enters condensation chamber 15, condensation chamber 15 inner steam pipes 14 in addition, steam pipe 14 lower ends directly communicate with the upper end of extraction vessel 12, so that the steam of extraction vessel 12 directly enters cooling in the condensation chamber 15 by steam pipe 14, condensation chamber 15 also is built-in with condenser pipe 16, the steam that is used for cooling condensation chamber 15, the water inlet of condenser pipe 16 is positioned at the lower end of condensation chamber 15, delivery port is positioned at the upper end of condensation chamber 15, and the top of condensation chamber 15 also has an outlet that communicates with atmosphere.
Above-mentioned filter 2 is the column type filter tunnel, the catheter 21 that has switch communicates with the extraction vessel 12 on the left side, when extract reaches a certain amount of, can enter in the concentrate container 32 by the catheter 22 that filters through filter 2 lower ends through catheter 21 inflow filters 2.
Above-mentioned inspissator 3 comprises constant temperature sleeve 31, concentrate container 32, control panel 33, vaporium 34, steam chamber cap 35 and steam guiding tube 36, constant temperature sleeve 31 is a column type, interior having heaters, and be connected with temp sensing controller, around bottom heating tube is uniformly distributed in and the side, to keep temperature constant, constant temperature sleeve 31 also has a upper port, concentrate container 32 is cylindrical, be used to load the extract that flows into by filter, can freely pick and place by the upper port of constant temperature sleeve 31 in constant temperature sleeve 31, suitable for reading and the vaporium 34 of concentrate container 32 links to each other, and there is a steam guiding tube 36 vaporium 34 upper ends, directly is connected with condensation chamber 15 lower ends, steam is fed in the condensation chamber 15, vaporium 34 tops also have a steam chamber cap 35, and control panel 33 is in the side below the constant temperature sleeve 31, is provided with thermoregulator and timer, can regulate temperature and extraction time according to concentrated condition, but jingle bell prompting after concentrated the finishing.
Compared with prior art, the present invention has following beneficial effect:
The utility model provides a kind of continuous extraction enrichment facility, this device is compared with traditional extraction separation method, have and once add solvent and can carry out repeated multiple times continuously and extract advantage, extraction time is short, disposable finishing extracted and concentrated, the efficient height, and save the energy and solvent, simple to operate, cost is low.
Description of drawings
Fig. 1 is a structural representation of the present utility model.
The specific embodiment
Below in conjunction with accompanying drawing the utility model is described further.
Structural representation of the present utility model as shown in Figure 1, extract enrichment facility continuously, from left to right be divided into refluxing extraction device 1, filter 2 and inspissator 3 three parts, the filter 2 of mid portion is connected with the refluxing extraction device 1 on the left side and the inspissator 3 on the right respectively, the upper end of inspissator 3 is connected with refluxing extraction device 1, forms a loop.Refluxing extraction device 1 comprises constant temperature sleeve 11, extraction vessel 12, control panel 13, steam pipe 14, condensation chamber 15 and condenser pipe 16, constant temperature sleeve 11 is a column type, interior having heaters, and be connected with temp sensing controller, around bottom heating tube is uniformly distributed in and the side, to keep temperature constant, constant temperature sleeve 11 also has a upper port, extraction vessel 12 is cylindrical, be used to load plant and the solvent that extracts usefulness, can freely pick and place by the upper port of constant temperature sleeve 11 in constant temperature sleeve 11, the lower end of the suitable for reading and condensation chamber 15 of extraction vessel 12 links to each other, and there is an outlet that exceeds the bottom slightly extraction vessel 12 lower ends, and barrier film is arranged in the outlet, the plant filter residue of isolating extraction vessel 12, this outlet is connected with filter 2, and control panel 13 is in the side below the constant temperature sleeve 11, is provided with thermoregulator and timer, can regulate temperature and extraction time according to the plant extract condition, but jingle bell prompting after extraction is finished.The lower end of condensation chamber 15 is connected with extraction vessel 12, one aperture is arranged at the bottom, be used for solvent refluxing with condensation to extraction vessel 12, one side of condensation chamber 15 lower ends also is connected with the steam lead 36 of inspissator 3, so that the steam that inspissator 3 produces enters condensation chamber 15, condensation chamber 15 inner steam pipes 14 in addition, steam pipe 14 lower ends directly communicate with the upper end of extraction vessel 12, so that the steam of extraction vessel 12 directly enters cooling in the condensation chamber 15 by steam pipe 14, condensation chamber 15 also is built-in with condenser pipe 16, the steam that is used for cooling condensation chamber 15, the water inlet of condenser pipe 16 is positioned at the lower end of condensation chamber 15, delivery port is positioned at the upper end of condensation chamber 15, and the top of condensation chamber 15 also has an outlet that communicates with atmosphere.Filter 2 is the column type filter tunnel, the catheter 21 that has switch communicates with the extraction vessel 12 on the left side, when extract reaches a certain amount of, can enter in the concentrate container 32 by the catheter 22 that filters through filter 2 lower ends through catheter 21 inflow filters 2.Inspissator 3 comprises constant temperature sleeve 31, concentrate container 32, control panel 33, vaporium 34, steam chamber cap 35 and steam guiding tube 36, constant temperature sleeve 31 is a column type, interior having heaters, and be connected with temp sensing controller, around bottom heating tube is uniformly distributed in and the side, to keep temperature constant, constant temperature sleeve 31 also has a upper port, concentrate container 32 is cylindrical, be used to load the extract that flows into by filter, can freely pick and place by the upper port of constant temperature sleeve 31 in constant temperature sleeve 31, suitable for reading and the vaporium 34 of concentrate container 32 links to each other, and there is a steam guiding tube 36 vaporium 34 upper ends, directly is connected with condensation chamber 15 lower ends, steam is fed in the condensation chamber 15, vaporium 34 tops also have a steam chamber cap 35, and control panel 33 is in the side below the constant temperature sleeve 31, is provided with thermoregulator and timer, can regulate temperature and extraction time according to concentrated condition, but jingle bell prompting after concentrated the finishing.
Method of operating: during use, take out extraction vessel 12, the plant that will extract and solvent are packed in the container, then extraction vessel 12 is put into the constant temperature sleeve 11 of refluxing extraction device 1, again condensation chamber 15 is packed on the extraction vessel 12, connect, check refluxing extraction device 1, whether filter 2 and inspissator 3 three parts connect fully, regulate by control panel 13 at last and extract temperature and time, open switch, extract, this moment is because the solvent that adds surpasses the outlet of extraction vessel 12 lower ends, earlier the switch of catheter 21 cuts out, behind the certain hour to be extracted, again catheter 21 switch opens, extract will enter filter 2 through catheter 21 by the barrier film of extraction vessel 12 lower ends outlet this moment, by filtering, enter in the concentrate container 32 through catheter 22, when extract reaches a certain amount of, open the switch of inspissator 3, regulate thickening temperature and time, beginning heating concentrates, the steam that concentrate this moment will enter condensation chamber 15 by vaporium 34 and steam guiding tube 36, be back to after the cooling in the extraction vessel 12, extract again, circulation so repeatedly, until extracting fully, the switch and catheter 21 switches of closing volume extractor 1 concentrate separately at this moment, till concentrated finishing, take off condensation chamber 15, take out extraction vessel 12, pour out the filter residue after the extraction, the cleaning back is standby, in addition, take off vaporium 34, take out concentrate container 32, pour out concentrate, the extraction of carrying out again after the cleaning next time concentrates.
Claims (5)
1, extract enrichment facility continuously, it is characterized in that extracting continuously enrichment facility and from left to right be divided into refluxing extraction device (1), filter (2) and inspissator (3) three parts, the upper end of inspissator (3) is connected with refluxing extraction device (1), forms a loop.
2, continuous extraction enrichment facility according to claim 1, it is characterized in that refluxing extraction device (1) comprises constant temperature sleeve (11), extraction vessel (12), control panel (13), steam pipe (14), condensation chamber (15) and condenser pipe (16), constant temperature sleeve (11) is a column type, interior having heaters, and be connected with temp sensing controller, constant temperature sleeve (11) also has a upper port, extraction vessel (12) is cylindrical, can freely pick and place by the upper port of constant temperature sleeve (11) in constant temperature sleeve (11), the lower end of the suitable for reading and condensation chamber (15) of extraction vessel (12) links to each other, there is an outlet that exceeds the bottom slightly extraction vessel (12) lower end, barrier film is arranged in the outlet, this outlet is connected with filter 2, and control panel (13) is in the side below the constant temperature sleeve (11), is provided with thermoregulator and timer.
3, continuous extraction enrichment facility according to claim 2, the lower end that it is characterized in that condensation chamber (15) is connected with extraction vessel (12), one aperture is arranged at the bottom, one side of condensation chamber (15) lower end also is connected with the steam lead (36) of inspissator (3), the inner steam pipe (14) in addition of condensation chamber (15), steam pipe (14) lower end directly communicates with the upper end of extraction vessel (12), condensation chamber (15) is built-in with condenser pipe (16), the water inlet of condenser pipe (16) is positioned at the lower end of condensation chamber (15), delivery port is positioned at the upper end of condensation chamber (15), and the top of condensation chamber (15) also has an outlet that communicates with atmosphere.
4, continuous extraction enrichment facility according to claim 1, it is characterized in that filter (2) is the column type filter tunnel, the catheter (21) that the upper end has switch communicates with the extraction vessel (12) on the left side, and the catheter (22) of filter (2) lower end communicates with concentrate container (32).
5, continuous extraction enrichment facility according to claim 1, it is characterized in that inspissator (3) comprises constant temperature sleeve (31), concentrate container (32), control panel (33), vaporium (34), steam chamber cap (35) and steam guiding tube (36), constant temperature sleeve (31) is a column type, interior having heaters, constant temperature sleeve (31) also has a upper port, concentrate container (32) is cylindrical, can freely pick and place by the upper port of constant temperature sleeve (31) in constant temperature sleeve (31), suitable for reading and the vaporium (34) of concentrate container (32) links to each other, there is a steam guiding tube (36) vaporium (34) upper end, directly be connected with condensation chamber (15) lower end, steam is fed in the condensation chamber (15), vaporium (34) top also has a steam chamber cap (35), and control panel (33) is in the side below the constant temperature sleeve (31), is provided with thermoregulator and timer.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNU2008202015904U CN201304262Y (en) | 2008-10-09 | 2008-10-09 | Continuous extracting concentration device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNU2008202015904U CN201304262Y (en) | 2008-10-09 | 2008-10-09 | Continuous extracting concentration device |
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| Publication Number | Publication Date |
|---|---|
| CN201304262Y true CN201304262Y (en) | 2009-09-09 |
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| Application Number | Title | Priority Date | Filing Date |
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| CNU2008202015904U Expired - Fee Related CN201304262Y (en) | 2008-10-09 | 2008-10-09 | Continuous extracting concentration device |
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| CN (1) | CN201304262Y (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103877741A (en) * | 2012-12-19 | 2014-06-25 | 江苏飞亚化学工业有限责任公司 | Condensing reflux distributor |
| CN110465109A (en) * | 2019-09-12 | 2019-11-19 | 中国人民解放军陆军特色医学中心 | A kind of drug distillation circulator |
| CN114618186A (en) * | 2022-03-19 | 2022-06-14 | 莆田市农汇食品有限公司 | Natural food aromatic extraction device |
-
2008
- 2008-10-09 CN CNU2008202015904U patent/CN201304262Y/en not_active Expired - Fee Related
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103877741A (en) * | 2012-12-19 | 2014-06-25 | 江苏飞亚化学工业有限责任公司 | Condensing reflux distributor |
| CN110465109A (en) * | 2019-09-12 | 2019-11-19 | 中国人民解放军陆军特色医学中心 | A kind of drug distillation circulator |
| CN114618186A (en) * | 2022-03-19 | 2022-06-14 | 莆田市农汇食品有限公司 | Natural food aromatic extraction device |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C17 | Cessation of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20090909 Termination date: 20101009 |