CN102525859B - Carboxymethyl yeast glucan emulsion as well as preparation method and application thereof - Google Patents
Carboxymethyl yeast glucan emulsion as well as preparation method and application thereof Download PDFInfo
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- CN102525859B CN102525859B CN 201210024007 CN201210024007A CN102525859B CN 102525859 B CN102525859 B CN 102525859B CN 201210024007 CN201210024007 CN 201210024007 CN 201210024007 A CN201210024007 A CN 201210024007A CN 102525859 B CN102525859 B CN 102525859B
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Abstract
The invention discloses carboxymethyl yeast glucan emulsion as well as a preparation method and application of the carboxymethyl yeast glucan emulsion. The carboxymethyl yeast glucan emulsion comprises water, cetostearyl alcohol or C12 to C20 alkyl glucoside or mixtures (emulsifying agents) of cetostearyl alcohol and C12 to C20 alkyl glucoside, octanoic acid/capric acid triglyceride, cyclopentasiloxane, dimethyl silicone polymer, one weight percent of carboxymethyl yeast glucan emulsion pure water solution, propylene glycol, glycerol, algae extracts, panthenol, carbomer, hydroxy methyl, disodium ethylene diamine tetraacetate (EDTA), triethanolamine, essence and phenoxyethanol, wherein the octanoic acid/capric acid triglyceride, the cyclopentasiloxane and the dimethyl silicone polymer are used as emollients, and the carboxymethyl yeast glucan emulsion pure water solution, the propylene glycol, the glycerol, the algae extracts and the panthenol are used as skin conditioners. The preparation method comprises the steps that the emulsifying agents and the emollients are mixed and heated to be 80 DEG C, the mixture is stirred for dissolution, then, the mixture is added into water solution of the skin conditioners, the mixture is subjected to continuous stirring dissolution and high-speed homogenizing under the condition of 85 DEG C, then, the heat insulation, the deforming and the temperature reduction are carried out, the triethanolamine is added, other raw materials are added after the temperature is continuously lowered to 45 DEG C, the still standing is carried out for 12 hours after the temperature is lowered to 39 DEG C, and products are obtained through 200-mesh filtering. The carboxymethyl yeast glucan emulsion disclosed by the invention has the efficacies of moisture preservation, skin moisturizing, aging resistance and the like and can be used for daily skin care products.
Description
Technical field
The present invention relates to the cosmetics technical field, be specifically related to a kind of carboxymethyl yeast dextran emulsion and its preparation method and application.
Background technology
Yeast dextran is a kind ofly to be connected to the master with the 1-3 glycosidic bond, contain the branch that a small amount of 1-6 glycosidic bond connects, macromolecule polysaccharide with triple helix tight structure, yeast from discarded beer yeast cells wall separation, glucosan has been realized industrialization, and product is applied to the immunoactivator of body-care food and animal feed.Research is discovery also, and yeast dextran can accelerate skin wound healing, and good skin moisture-keeping performance and crease-resistant, anti-senescence function are arranged simultaneously, and good application prospect is arranged aspect skin care item.
Though the insoluble yeast dextran energy of alkali water absorption and swelling, but be insoluble in water, also be insoluble to the common solvent such as ethanol, thereby limited application aspect skin care item, method by chemical modification is introduced special chemical group, be the conventional means that increases the slightly water-soluble high molecular polymer, as Sulfation, Phosphation, carboxy methylation etc., wherein comparatively the human safety of maturation and product is high for the carboxy methylation technology of polysaccharide always.
Summary of the invention
The object of the present invention is to provide a kind of skin care item that contain water-soluble glucan, i.e. a kind of carboxymethyl yeast dextran emulsion.
Another object of the present invention is to provide the preparation method of above-mentioned carboxymethyl yeast dextran emulsion.
Another purpose of the present invention is to provide the application of above-mentioned carboxymethyl yeast dextran emulsion.
The present invention is achieved through the following technical solutions above-mentioned purpose:
We adopt the carboxymethyl yeast dextran to join in skin-protection product, obtain the cosmetics that compatibility is good, effect is good.
a kind of carboxymethyl yeast dextran emulsion, formed by following raw material, by the quality percentage composition, be respectively: water 65.00 ~ 85.00%, cetearyl alcohol or C12 ~ 20(also can be write as C12 ~ C20, the expression carbon number between 12 ~ 22) alkyl androstanediol or both mixture 0.50 ~ 5.00%, caprylic/capric triglyceride 1.00 ~ 10.00%, encircle five polydimethylsiloxane 0.50 ~ 3.00%, polydimethylsiloxane 0.50 ~ 3.00%, the carboxymethyl yeast dextran pure water solution 0.10 ~ 10.00% of 1wt%, propylene glycol 0.50 ~ 5.00%, glycerol 1.00 ~ 10.00%, carbomer 0.05 ~ 1.00%, algae extract 3.00%, pantothenylol 0.10 ~ 1.00%, methyl hydroxybenzoate 0.01 ~ 0.20%, EDETATE SODIUM 0.01 ~ 0.20%, triethanolamine 0.01 ~ 2.00%, essence 0.01 ~ 0.80%, phenoxyethanol 0.40 ~ 1.00%.
as a kind of preferred version, the formula of above-mentioned carboxymethyl yeast dextran emulsion is as follows: (by the quality percentage composition) water 78.42 ~ 80.50%, the alkyl androstanediol mixture 1.00 ~ 2.00% of the pure and mild C12 ~ C20 of cetearyl alcohol, caprylic/capric triglyceride 2.00 ~ 3.00%, encircle five polydimethylsiloxane 2.00 ~ 3.00%, polydimethylsiloxane 1.50 ~ 3.00%, the carboxymethyl yeast dextran pure water solution 2.00 ~ 3.00% of 1wt%, propylene glycol 3.00 ~ 4.00%, glycerol 3.00 ~ 4.00%, carbomer 0.30 ~ 0.40%, algae extract 0.20 ~ 0.30%, pantothenylol 0.50 ~ 1.00%, methyl hydroxybenzoate 0.10 ~ 0.20%, EDETATE SODIUM 0.05 ~ 0.15, triethanolamine 0.30 ~ 0.40%, essence 0.05 ~ 0.10%, phenoxyethanol 0.40 ~ 0.50%.
In above-mentioned formula, caprylic/capric triglyceride is the mixture of Trivent OCG and tricaprin, and this product I NCI name is called: CAPRYLIC/CAPRIC TRIGLYCERIDE; No. CAS: 65381-09-1; 73398-61-5 can directly buy in the market.Algae extract I NCI name is called ALGAE EXTRACT; No. CAS: 92128-82-0, can directly buy in the market.In the present invention, essence refers to can use in article of everyday use such as food, articles for washing, skin care item or cosmetics, can give the reagent of the certain odor type of article of everyday use, can be natural essence or compound essence.
The alkyl androstanediol of the cetearyl alcohol of this formula or C12 ~ 20 or both mixture play emulsifying agent; Caprylic/capric triglyceride, ring five polydimethylsiloxane and polydimethylsiloxane use mainly as emollient in this product; Carboxymethyl yeast dextran, propylene glycol, glycerol, algae extract and pantothenylol are as skin conditioning agent; Water is solvent, and carbomer mainly plays thick stabilization, and methyl hydroxybenzoate and phenoxyethanol are antiseptic, EDETATE SODIUM is chelating agen, triethanolamine is mainly used to regulate the pH value of product, and the pH value scope of product is between 5.0 ~ 7.0, and essence uses as aromatic.
A kind of preparation method of above-mentioned carboxymethyl yeast dextran emulsion, step is as follows:
(1) all production equipments and apparatus are cleaned, disinfect;
(2) with alkyl androstanediol or both mixture, caprylic/capric triglyceride, ring five polydimethylsiloxane and the polydimethylsiloxane mix and blend of cetearyl alcohol or C12 ~ 20, heat to 80 ℃, obtain mixture after stirring predissolve fully standby;
(3) add respectively propylene glycol, glycerol, carbomer, pantothenylol, methyl hydroxybenzoate and EDETATE SODIUM in 85 ℃ of pure water, stirring and dissolving is complete, with the speed homogenizing of 2000 ~ 5000 rev/mins 5 minutes, is incubated 20 minutes and stirs and obtain mixed liquor;
(4) mixture with step (2) joins in the mixed liquor of step (3), stirs after 3 minutes with the speed homogenizing of 2000 ~ 5000 rev/mins 5 minutes, is incubated 20 minutes, the emulsifying froth breaking;
(5) lower the temperature after froth breaking, add triethanolamine in the time of 70 ℃, rear continuation cooling stirs;
When (6) cooling to 45 ℃, then add respectively 1wt% carboxymethyl yeast dextran pure water solution, algae extract, essence and phenoxyethanol, continue to be cooled to 39 ℃ after stirring and dissolving is complete;
(7) standing 12 hours, 200 orders filtered discharging and obtain semi-finished product.
(8) semi-finished product are after be up to the standards (cosmetic field be correlated with routine inspection), get the packaging material that cleaning and sterilizing crosses and carry out fill under clean environment, and assemble each accessory by product requirement and form product;
(9) product is tested (cosmetics finished product be correlated with routine inspection), warehousing after passing.
Carboxymethyl yeast dextran emulsion of the present invention can be used for preventing skin aging, desalination wrinkle, increases skin elasticity or increase the skin moisture-keeping degree.
Compared with prior art, the present invention has following beneficial effect:
Preparation method of the present invention is simple to operation, preparation condition is gentle, can not destroy the effect of formula components, the carboxymethyl yeast dextran emulsion exquisite quality for preparing, but rapid osmotic skin, have the effect that better prevents skin aging, increases skin vitality than other like products, and high to human safety, have wide market prospect.
The specific embodiment
Embodiment 1
production weight 50kg, each raw material and weight are: water 40.25kg(80.50%), the mixture of the pure and mild C12-20 alkyl androstanediol of cetearyl alcohol (both are roughly 4:6 by mass ratio) 1.00kg(2.00%), caprylic/capric triglyceride 1.00kg(2.00%), encircle five polydimethylsiloxane 1.00kg(2.00%), polydimethylsiloxane 1.00kg(2.00%), mass percentage concentration is 1% carboxymethyl yeast dextran pure water solution 1.00kg(2.00%), propylene glycol 1.75kg(3.50%), glycerol 1.75kg(3.50%), carbomer 0.15(0.30%), algae extract 0.10kg(0.20%), pantothenylol 0.50kg(1.00%), methyl hydroxybenzoate 0.075kg(0.15%), EDETATE SODIUM 0.025kg(0.05%), triethanolamine 0.15kg(0.30%), essence 0.05kg(0.10%), phenoxyethanol 0.20kg(0.40%).
To produce the cleaning and sterilizings such as required utensil, equipment standby.First mixture, caprylic/capric triglyceride, ring five polydimethylsiloxane and the polydimethylsiloxane of the pure and mild C12-20 alkyl androstanediol of cetearyl alcohol stirred in oil cauldron and be warmed up to 80 ℃, stir predissolve fully standby.Water is added main cooker, be warming up to 85 ℃, then with propylene glycol, glycerol, carbomer, pantothenylol, methyl hydroxybenzoate and EDETATE SODIUM, join respectively in main cooker, stirring and dissolving is complete, is aided with the speed high speed homogenization 5 minutes of 3000 rev/mins, insulated and stirred 20 minutes.Slowly join mixture, caprylic/capric triglyceride, ring five polydimethylsiloxane and the polydimethylsiloxanemixture mixture of the pure and mild C12-20 alkyl androstanediol of the cetearyl alcohol in the oil cauldron of handling well in main cooker, stir after 3 minutes, open high speed homogenization 5 minutes (3000 rev/mins), be incubated 20 minutes emulsifying froth breakings.Begin cooling after insulation finishes, in the time of 70 ℃, triethanolamine is joined, rear continuation cooling stirs.Be during 1% carboxymethyl yeast dextran pure water solution, algae extract, essence and phenoxyethanol join main cooker respectively with mass percentage concentration 45 ℃ of left and right, stirring and dissolving continues to be cooled to 39 ℃ after fully.
Then qualified rear standing 12 hours of the said goods self check is crossed 200 orders filtration dischargings and is obtained semi-finished product, the qualified rear fill of the inspection of semifinished product, product inspection warehousing after passing.
Embodiment 2
Production weight 200kg.composition of raw materials: water 158.30kg(79.15%), cetearyl alcohol 2.00kg(1.00%), caprylic/capric triglyceride 6.00kg(3.00%), encircle five polydimethylsiloxane 6.00kg(3.00%), polydimethylsiloxane 3.00kg(1.50%), mass percentage concentration is 1% carboxymethyl yeast dextran pure water solution 6.00kg(3.00%), propylene glycol 6.00kg(3.00%), glycerol 8.00kg(4.00%), carbomer 0.80kg(0.40%), algae extract 0.60kg(0.30%), pantothenylol 1.00kg(0.50%), methyl hydroxybenzoate 0.20kg(0.10%), EDETATE SODIUM 0.20kg(0.10%), triethanolamine 0.80kg(0.40%), essence 0.10kg(0.05%), phenoxyethanol 1.00kg(0.50%).
To produce the cleaning and sterilizings such as required utensil, equipment standby.First mixture, caprylic/capric triglyceride, ring five polydimethylsiloxane and the polydimethylsiloxane of the pure and mild C12-20 alkyl androstanediol of cetearyl alcohol stirred in oil cauldron and be warmed up to 80 ℃, stir predissolve fully standby.Water is added main cooker, be warming up to 85 ℃, then with propylene glycol, glycerol, carbomer, pantothenylol, methyl hydroxybenzoate and EDETATE SODIUM, join respectively in main cooker, stirring and dissolving is complete, be aided with high speed homogenization 5 minutes (4000 rev/mins), insulated and stirred 20 minutes.Slowly join mixture, caprylic/capric triglyceride, ring five polydimethylsiloxane and the polydimethylsiloxanemixture mixture of the pure and mild C12-20 alkyl androstanediol of the cetearyl alcohol in the oil cauldron of handling well in main cooker, stir after 3 minutes, open high speed homogenization 5 minutes (4000 rev/mins), be incubated 20 minutes emulsifying froth breakings.Begin cooling after insulation finishes, in the time of 70 ℃, triethanolamine is joined, rear continuation cooling stirs.Be during 1% carboxymethyl yeast dextran pure water solution, algae extract, essence and phenoxyethanol join main cooker respectively with mass percentage concentration 45 ℃ of left and right, stirring and dissolving continues to be cooled to 39 ℃ after fully.
Then qualified rear standing 12 hours of the said goods self check is crossed 200 orders filtration dischargings and is obtained semi-finished product, the qualified rear fill of the inspection of semifinished product, product inspection warehousing after passing.
Embodiment 3
Production weight 300kg.composition of raw materials: water 235.26kg(78.42%), C12-20 alkyl androstanediol 4.50kg(1.50%), caprylic/capric triglyceride 7.50kg(2.50%), encircle five polydimethylsiloxane 7.50kg(2.50%), polydimethylsiloxane 9.00kg(3.00%), mass percentage concentration is 1% carboxymethyl yeast dextran pure water solution 7.50kg(2.50%), propylene glycol 12.00kg(4.00%), glycerol 9.00kg(3.00%), carbomer 1.05kg(0.35%), algae extract 0.75kg(0.25%), pantothenylol 2.25kg(0.75%), methyl hydroxybenzoate 0.60kg(0.20%), EDETATE SODIUM 0.45kg(0.15%), triethanolamine 1.05kg(0.35%), essence 0.24kg(0.08%), phenoxyethanol 1.35kg(0.45%).
To produce the cleaning and sterilizings such as required utensil, equipment standby.First mixture, caprylic/capric triglyceride, ring five polydimethylsiloxane and the polydimethylsiloxane of the pure and mild C12-20 alkyl androstanediol of cetearyl alcohol stirred in oil cauldron and be warmed up to 80 ℃, stir predissolve fully standby.Water is added main cooker, be warming up to 85 ℃, then with propylene glycol, glycerol, carbomer, pantothenylol, methyl hydroxybenzoate and EDETATE SODIUM, join respectively in main cooker, stirring and dissolving is complete, be aided with high speed homogenization 5 minutes (3500 rev/mins), insulated and stirred 20 minutes.Slowly join mixture, caprylic/capric triglyceride, ring five polydimethylsiloxane and the polydimethylsiloxanemixture mixture of the pure and mild C12-20 alkyl androstanediol of the cetearyl alcohol in the oil cauldron of handling well in main cooker, stir after 3 minutes, open high speed homogenization 5 minutes (3500 rev/mins), be incubated 20 minutes emulsifying froth breakings.Begin cooling after insulation finishes, in the time of 70 ℃, triethanolamine is joined, rear continuation cooling stirs.Be during 1% carboxymethyl yeast dextran pure water solution, algae extract, essence and phenoxyethanol join main cooker respectively with mass percentage concentration 45 ℃ of left and right, stirring and dissolving continues to be cooled to 39 ℃ after fully.
Then qualified rear standing 12 hours of the said goods self check is crossed 200 orders filtration dischargings and is obtained semi-finished product, the qualified rear fill of the inspection of semifinished product, product inspection warehousing after passing.
Embodiment 4
Select the crowd in three groups of all ages and classes stages to try out the carboxymethyl yeast dextran emulsion that embodiment 1 prepares.
First group of number 20 people on probation, age level was observed result on trial at 50 ~ 55 years old after different time on probation under the same conditions, saw Table 1:
Table 1
| One week | Two weeks | One month | Two months | |
| Test result | The skin moisture-keeping performance obviously increases, and wrinkle is without obviously improving (18 people produce effect) | The skin moisture-keeping performance increases obviously, and the eye wrinkle-removing degree of depth can be seen has a little to improve (16 people have a little effect) | The skin moisture-keeping degree is high, microgroove is obviously desalinated in eye wrinkle-removing, (18 people have obvious desalination effect) | The skin moisture-keeping degree is high, microgroove is obviously desalinated in eye wrinkle-removing, and crows-feet is improved phenomenon, and skin elasticity increases.(18 people have obvious desalination effect) |
Second group of number 20 people on probation, age level was observed result on trial at 40 ~ 45 years old after different time on probation under the same conditions, saw Table 2:
Table 2
| One week | Two weeks | One month | Two months | |
| Test result | The skin moisture-keeping performance obviously increases, and wrinkle is without obviously improving (18 people produce effect) | The skin moisture-keeping performance increases obviously, and the eye wrinkle-removing degree of depth can be seen has a little to improve (16 people have a little effect) | The skin moisture-keeping degree is high, microgroove is obviously desalinated in eye wrinkle-removing, (18 people have obvious desalination effect) | The skin moisture-keeping degree is high, microgroove is obviously desalinated in eye wrinkle-removing, and crows-feet is improved phenomenon, and skin elasticity increases.(18 people have obvious desalination effect) |
The 3rd group of number 20 people on probation, age level was observed result on trial at 30 ~ 35 years old after different time on probation under the same conditions, saw Table 3:
Table 3
| One week | Two weeks | One month | Two months | |
| Test result | The skin moisture-keeping performance obviously increases, and observes the microgroove of regeneration without obviously increasing (18 people produce effect) | The skin moisture-keeping performance increases obviously, and the eye microgroove degree of depth can be seen has a little to improve (16 people have a little effect) | The skin moisture-keeping degree is high, microgroove is obviously desalinated in eye wrinkle-removing, (18 people have obvious desalination effect) | The skin moisture-keeping degree is high, microgroove is obviously desalinated in eye wrinkle-removing, and skin elasticity increases obviously.(18 people have obvious desalination effect) |
Claims (1)
1. carboxymethyl yeast dextran emulsion, it is characterized in that being formed by following raw material, by the quality percentage composition, be respectively: water 65.00 ~ 85.00%, the alkyl androstanediol of cetearyl alcohol or C12 ~ 20 or both mixture 0.50 ~ 5.00%, caprylic/capric triglyceride 1.00 ~ 10.00%, encircle five polydimethylsiloxane 0.50 ~ 3.00%, polydimethylsiloxane 0.50 ~ 3.00%, the carboxymethyl yeast dextran pure water solution 0.10 ~ 10.00% of 1wt%, propylene glycol 0.50 ~ 5.00%, glycerol 1.00 ~ 10.00%, carbomer 0.05 ~ 1.00%, algae extract 0.10 ~ 3.00%, pantothenylol 0.10 ~ 1.00%, methyl hydroxybenzoate 0.01 ~ 0.20%, EDETATE SODIUM 0.01 ~ 0.20%, triethanolamine 0.01 ~ 2.00%, essence 0.01 ~ 0.80%, phenoxyethanol 0.40 ~ 1.00%,
The preparation method of described carboxymethyl yeast dextran emulsion is following steps:
(1) all production equipments and apparatus are cleaned, disinfect;
(2) with alkyl androstanediol or both mixture, caprylic/capric triglyceride, ring five polydimethylsiloxane and the polydimethylsiloxane mix and blend of cetearyl alcohol or C12 ~ 20, heat to 80 ℃, obtain mixture after stirring predissolve fully standby;
(3) add respectively propylene glycol, glycerol, carbomer, pantothenylol, methyl hydroxybenzoate and EDETATE SODIUM in 85 ℃ of water, stirring and dissolving is complete, with the speed homogenizing of 2000 ~ 5000 rev/mins 5 minutes, is incubated 20 minutes and stirs and obtain mixed liquor;
(4) mixture with step (2) joins in the mixed liquor of step (3), stirs after 3 minutes with the speed homogenizing of 2000 ~ 5000 rev/mins 5 minutes, is incubated 20 minutes, the emulsifying froth breaking;
(5) lower the temperature after froth breaking, add triethanolamine in the time of 70 ℃, rear continuation cooling stirs;
When (6) cooling to 45 ℃, then add respectively 1wt% carboxymethyl yeast dextran pure water solution, algae extract, essence and phenoxyethanol, continue to be cooled to 39 ℃ after stirring and dissolving is complete;
(7) standing 12 hours, 200 orders filtered discharging and obtain semi-finished product;
(8) semi-finished product are through after the assay was approved, get the packaging material that cleaning and sterilizing crosses and carry out fill under clean environment, and assemble each accessory by product requirement and form product;
(9) product is tested, warehousing after passing.
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| Title |
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| JP特开2007-77093A 2007.03.29 |
| 王庆华等.羧甲基酵母葡聚糖在护肤品中的应用研究.《广东化工》.2010,第37卷(第6期),7-9. |
| 羧甲基酵母葡聚糖在护肤品中的应用研究;王庆华等;《广东化工》;20100630;第37卷(第6期);7-9页 * |
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