CN107890439B - Extraction method of aesculus hippocastanum seed extract and hair washing composition thereof - Google Patents
Extraction method of aesculus hippocastanum seed extract and hair washing composition thereof Download PDFInfo
- Publication number
- CN107890439B CN107890439B CN201711127147.7A CN201711127147A CN107890439B CN 107890439 B CN107890439 B CN 107890439B CN 201711127147 A CN201711127147 A CN 201711127147A CN 107890439 B CN107890439 B CN 107890439B
- Authority
- CN
- China
- Prior art keywords
- aesculus hippocastanum
- seed
- extract
- seeds
- fermentation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/737—Galactomannans, e.g. guar; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/524—Preservatives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Cosmetics (AREA)
Abstract
The invention relates to the technical field of natural product extraction, in particular to a plant extraction method, and also relates to a shampoo composition containing components extracted by the method. The invention discloses a novel extraction method of effective components of aesculus hippocastanum seeds, which can improve the content of aesculus hippocastanum saponin, simultaneously can recover protein components in plants, improves the anti-inflammatory effect and the effect of removing free radicals of products, and has high utilization rate of raw materials and good repeatability. Meanwhile, the prepared extract has an antiseptic effect, and no preservative is required to be added, so that the safety, efficacy and stability of the product are ensured. The composition capable of improving the carrying efficiency of the effective components disclosed by the invention enables the extract to improve the effect in the optimized formula, and achieves the synergistic purpose of matrix-effect extract.
Description
Technical Field
The invention relates to the technical field of natural product extraction, in particular to a plant extraction method, and also relates to a shampoo composition containing components extracted by the method.
Background
Among the undesirable symptoms of skin and scalp perceived by consumers, skin aging, wrinkles, and itchiness and dandruff of the skin are the most important factors, and there are many factors that cause such a feeling, among which external factors are important factors, external adverse environments stimulate inflammation of the skin surface of a human body, and malassezia on the scalp aggravates dandruff of hair. Meanwhile, with the gradual development of the current science and technology, the artificial inflammation is the main cause of the sub-health problems of the skin or the scalp. Although the problems above individuals may also have internal physical causes, these external adverse environments are also not negligible.
The European aesculus hippocastanum seeds are known to have good free radical removal and inflammation removal capabilities, but most of researches are stopped in the aspect of purified aesculus hippocastanum saponin, while common European aesculus hippocastanum seed extracting solution does not have the aesculus hippocastanum saponin with high concentration, and meanwhile, as the traditional aesculus hippocastanum seed extracting solution mostly adopts direct extraction or purification technology, the mode can cause waste of plant raw materials, and simultaneously, because a large amount of molecular substances exist in the substances extracted from the plants, the substances are difficult to be absorbed by the skin in a short time, and the absorption rate of active substances is low. In addition, in order to ensure that the extracting solution has a certain shelf life, a preservative needs to be added, so that the irritation of the extract is increased, and the application range is low.
Based on the above, if some substances existing in the seeds of aesculus hippocastanum are directly extracted and purified and the extract is directly applied to a personal care product, the active ingredients of the extract are low in absorption rate on the skin and cause a great deal of waste due to the high molecular weight of the active ingredients, and meanwhile, the directly extracted plant extract has a great amount of residual dregs, which also contain a plurality of available ingredients and cause waste of raw materials.
In addition, even though a single extract has been shown to have beneficial effects on the human body, it still does not represent the same effect as the actual addition of the extract to the formulation, and therefore, such an active would have a corresponding requirement for a "matrix" or "carrier" and the need for a corresponding effective delivery of the active ingredients of the extract to the carrier would be sufficient to increase the availability of the active.
Therefore, another effective component capable of fully utilizing the seeds of the European horse chestnut is developed, so that the plant raw materials play a greater role, and the market prospect is good.
Disclosure of Invention
Accordingly, the present invention is directed to overcome the technical defects of the prior art that the extraction of the active ingredients of aesculus hippocastanum seeds is insufficient and the utilization efficiency of the active ingredients by human bodies is not high, to provide a method for extracting the active ingredients of aesculus hippocastanum seeds, and to provide a shampoo composition containing the extract of aesculus hippocastanum seeds. The extraction method disclosed by the invention can improve the content of the aescin, simultaneously can recover protein components in plants, improves the anti-inflammatory effect and the free radical removing effect of products, and has high raw material utilization rate and good repeatability. Meanwhile, the prepared extract has an antiseptic effect, and no preservative is required to be added, so that the safety, efficacy and stability of the product are ensured.
Another object of the present invention is to provide a composition capable of improving the carrying efficiency of effective ingredients, so that the efficacy of the extract in the optimized formula can be improved, and the synergistic purpose of matrix-efficacy extract can be achieved.
The scheme for solving the technical problems is as follows:
a method for extracting a horse chestnut seed extract sequentially comprises the following steps:
s1, washing the seeds of the aesculus hippocastanum, wherein the weight ratio of the seeds is 50-55: adding deionized water according to the mass ratio of 35-50, and coarsely crushing to obtain mixed European horse chestnut seed primary pulp;
s2, respectively activating lactic acid bacteria accounting for 0.5-2wt% of the S1 material and yeast accounting for 0.5-2wt% of the S1 material to respectively obtain a lactic acid bacteria secondary seed liquid and a yeast secondary seed liquid;
s3, inoculating the lactobacillus secondary seed liquid and the microzyme secondary seed liquid obtained in the step S2 into the aesculus hippocastanum seed primary pulp obtained in the step 1, and performing coarse fermentation, wherein 0.5-2wt% of urea is supplemented in the process to obtain aesculus hippocastanum seed fermentation products; the time of the crude fermentation is 6-10 days, the temperature of the crude fermentation is 25-28 ℃, and the pressure of the crude fermentation is 0.08-0.1 Mpa;
s4, stirring, centrifuging and filtering the aesculus hippocastanum seed fermentation product obtained in the step S3, and removing filter residues to obtain a aesculus hippocastanum seed fermentation product filtrate;
s5, processing the filter residue obtained in the step S4 as follows:
a. drying the filter residue at 90-100 ℃ to obtain filter residue cake, shearing at high speed and crushing into powder, and placing in a container;
b. adding 30-45 parts by mass of hot pure water at 85-90 ℃ into 10-20 parts by mass of powder, soaking for 30-60 minutes, filtering to another container, keeping filtrate, and removing filter residues;
c. 0.1-5 parts by mass of flocculating agent Al is added2 (SO4) 3 Precipitating, removing impurities, cooling, and keeping the upper filtrate;
d. c, adding 30-60 parts by mass of 70-95% ethanol solution into the upper filtrate obtained in the step c, soaking and stirring for 2-4 hours, precipitating and filtering;
e. d, circularly decoloring the filtrate flow obtained in the step d in a decoloring device for 18-22 minutes;
f. distilling and concentrating the decolorized solution for 2-8 h, condensing the steam by a condensing device, and recovering an ethanol solution;
g. vacuum drying the crude aesculus hippocastanum seed fermentation product after distillation and concentration to obtain a solid finished product; the yield of the European horse chestnut seed solid finished product prepared by the process is 10-15%, and the purity is 92-96%. And the European horse chestnut seeds can form foams through experiments and have certain efficacy of relieving inflammation.
S6, mixing the fermentation liquid of the aesculus hippocastanum seeds obtained in the S4 and the solid finished products of the aesculus hippocastanum seeds obtained in the S5 according to the ratio of 2: 1-1: 2, adding the polyalcohol to dissolve the aesculus hippocastanum seed extract into a thick slurry solution, wherein the polyalcohol accounts for 10wt% of the thick slurry solution. This solution has been demonstrated to be preserved for long periods of time without the addition of preservatives.
A shampoo composition containing the above Aesculus hippocastanum seed extract comprises the following raw materials by weight percent:
(A) concentrated pulp solution of Aesculus hippocastanum seed extract 0.01-30%;
(B) 0.01-10% of anionic surfactant;
(C) 0.5 to 10 percent of amphoteric surfactant;
(D) 0.05-3% of cationic polysaccharide polymer derivative; wherein the cationic polysaccharide polymer derivative is selected from cationic guar gum derivatives, the charge density of the cationic polysaccharide polymer derivative is 0.5-1.0 meq/g, and the molecular weight of the cationic polysaccharide polymer derivative is 400000-1500000 g/mol;
(E) 0.01-10% of rheology modifier or appearance modifier; and the remainder of
(F) Pure water.
(A) Concentrated pulp solution of European horse chestnut seed extract
The Aesculus hippocastanum seed contains various proteins, amino acids, aescin and the like, and has the effects of scavenging free radicals, resisting inflammation, improving skin microenvironment and the like.
(B) Anionic surfactants
The anionic surfactant is selected from one or more of alkyl polyoxyethylene ether sulfate, fatty acid monoglyceride sulfate, fatty alcohol ether sulfosuccinate, N-fatty acylamino acid salt, fatty acyl methyl taurate, monoalkyl sulfate, monoalkyl carboxylate and monoalkyl phosphate. Preferably at least one or two of alkyl polyoxyethylene ether sulfate, fatty acid monoglyceride sulfate, fatty alcohol ether sulfosuccinate, N-fatty acylamino acid salt and fatty acyl methyl taurate, and the anionic surfactant has a larger critical stacking parameter, wherein the stacking parameter is expressed by the following formula:
wherein the content of the first and second substances,
the stacking parameter of the surfactant is obtained, V is the volume of a hydrocarbon chain of the surfactant, l is the critical length, and a is the area of an end group; it is desirable to include at least anionic surfactants having critical packing parameters above at least 1/4, optionally with the aid of one or both of monoalkyl sulfates, monoalkyl carboxylates, and monoalkyl phosphates, and it is within the scope of this patent to exclude such low packing parameters.
Experiments show that the surfactant with larger accumulation parameters is beneficial to reducing the irritation of the whole system, and simultaneously, the flocculation strength and the flocculation persistence generated by the anionic surfactant, the amphoteric surfactant and the cationic cellulose derivative can be enhanced, so that the technical effect to be realized in the patent has a gain effect. The addition of the auxiliary anionic surfactant can bring about improved foaming effect and thickening effect, and the addition is selectively positioned according to the final composition.
(C) Amphoteric surfactant
The amphoteric surfactant is selected from one or more of fatty acyl amphoacetate, fatty acyl propyl betaine and fatty amide hydroxypropyl sulfobetaine. One or two of fatty acyl amphoacetate and fatty acyl propyl betaine are preferred, and fatty acyl propyl betaine is particularly preferred. The addition of amphoteric surfactant makes the flocculation strength and the flocculation durability further enhanced, and at the same time, if the anionic surfactant part has the surfactant with high optimized stacking parameter, the amphoteric surfactant is beneficial to increasing the easy adjustment of the viscosity of the composition, and the addition of amphoteric surfactant is known in the art to greatly improve the foam performance, the mild performance and the process realizable performance.
(D) Cationic polysaccharide polymer derivatives
The cationic polysaccharide polymer derivative is selected from cationic guar gum derivatives, and the charge density of the cationic polysaccharide polymer derivative is about 0.5-1.0 meq/g; and the molecular weight is about 400000-1500000 g/mol; preferably, the charge density is about 0.6-0.9 meq/g, and the molecular weight is about 450000-1300000 g/mol; most preferably, the charge density is about 0.7-0.8 meq/g, and the molecular weight is about 450000-1300000 g/mol 500000-1200000 g/mol; the applicant finds that in the system adopting the cationic guar gum derivative and the system compounded with the cationic guar gum derivative, and in the optimized system matched with the cationic guar gum derivative, the diluted floc has good effect of coating protein substances, and meanwhile, the water content of the flocculation phase reaches an ideal state, so that the good deposition effect of the protein substances is realized.
(E) Rheology or appearance modifiers
The rheology modifier or appearance modifier is selected from acyl derivatives and long chain amine oxides. Wherein the acyl derivative includes, but is not limited to, glycol esters of fatty acids containing 16 to 22 carbon atoms, long chain hydrocarbons, long chain esters of long chain fatty acids, long chain esters of long chain alkanolamides. Wherein the long chain amine oxide includes, but is not limited to, dimethylamine oxide of 16 to 22 carbon atoms. Preferably a fatty acid glycol diester having 18 carbon atoms. The applicant has experimentally verified that such a suspending agent has little influence on the degree of flocculation of the system and does not provide sufficient suspending power depending on the yield value.
The personal care composition containing the aesculus hippocastanum seed extract may contain at least one of the following components in addition to the above essential components:
suspending agent: 0.01 to 5 percent;
nonionic surfactant: 0.01 to 5 percent;
non-volatile conditioning agents: 0.01 to 3 percent
Organic conditioning oil: 0.01 to 2 percent
Higher aliphatic alcohol: 0.01 to 5 percent
Preservative: 0.01-1%;
essence: 0.01 to 3 percent;
viscosity modifier: 0.01-4%;
light screening agent: 0.01 to 1.0 percent
Chelating agent: 0.005-0.2%;
ultraviolet absorber: 0.01-2%;
other plant extracts and their derivatives: 0.0001-5%;
the personal care composition of the aesculus hippocastanum seed extract has the advantages that the adding process of the concentrated pulp solution of the aesculus hippocastanum seed extract is carried out according to the conventional surfactant adding method, and the preparation method of the shampoo composition adopts the conventional preparation and mixing technology, and the detailed description is not provided herein.
The invention has the following beneficial effects:
1. according to the invention, the fermentation process and the high-temperature extraction process are combined to carry out fermentation treatment on the European aesculus hippocastanum seed extract, so that the utilization rate of the raw materials of the European aesculus hippocastanum seed extract is improved, the absorption rate of active ingredients on skin is improved, and the waste of the raw materials is avoided.
2. The aesculus hippocastanum seed extract replaces part of chemically synthesized surfactant content, can reduce the irritation of the surfactant of the whole system, and can reduce the burden of scalp nursing. Experiments prove that the aescin in the aesculus hippocastanum seed extract also has foaming performance, is a natural foaming agent, is mild and nontoxic, and can be used for further caring skin and hair by reducing the irritation of the shampoo composition in order to relieve unhealthy symptoms of the skin and scalp.
3. The fermentation product of the European aesculus hippocastanum seeds obtained by fermentation has active substance molecules combined by large and small molecules, is easier to absorb, assists the antioxidation effect of the aesculus hippocastanum, and simultaneously supplements skin nutrient substances, so that the effect of removing free radicals is more obvious.
4. The European horse chestnut seed fermentation product, the aescin, the anionic surfactant and the cationic polysaccharide polymer derivative are used together, so that the skin or scalp state can be relieved from the skin or scalp state and microecological level, the free radicals can be removed, and the unhealthy conditions of the skin and the scalp can be effectively reduced. The stimulation of the surfactant to the scalp and the stimulation of the environment to the scalp are apparent as inflammation phenomena to a large extent, and the aescin can effectively relieve the inflammation phenomena of the scalp.
5. The extraction process of the European horse chestnut seeds disclosed by the invention is low in difficulty, plant raw materials are effectively utilized, the concentration and the absorbability of active ingredients are improved, the compounding synergistic effect between the active ingredients and the personal care composition is obvious, the shampoo composition is low in irritation, and obvious in anti-inflammatory effect and anti-dandruff effect through the synergistic effect between the raw materials, and the unhealthy condition of skin or hair can be relieved from multiple aspects.
Detailed Description
The present invention will be described in detail with reference to examples.
Table 1 below shows 3 preferred examples of the present invention and 3 comparative examples. Wherein, the comparative example 3 uses the common European horse chestnut seed extract on the market, and the comparative example 4 selects the two-in-one shampoo which is good in sales and takes the concept of scalp care on the market.
Wherein, the concentrated slurry solution of the aesculus hippocastanum seed extract used in examples 1 to 3 and comparative example 2 is obtained by the following extraction method:
s1, washing the seeds of the aesculus hippocastanum, wherein the weight ratio of the seeds is 50-55: adding deionized water according to the mass ratio of 35-50, and coarsely crushing to obtain mixed European horse chestnut seed primary pulp;
s2, respectively activating lactic acid bacteria accounting for 0.5-2wt% of the S1 material and yeast accounting for 0.5-2wt% of the S1 material to respectively obtain a lactic acid bacteria secondary seed liquid and a yeast secondary seed liquid;
s3, inoculating the lactobacillus secondary seed liquid and the microzyme secondary seed liquid obtained in the step S2 into the aesculus hippocastanum seed primary pulp obtained in the step 1, and performing coarse fermentation, wherein 0.5-2wt% of urea is supplemented in the process to obtain aesculus hippocastanum seed fermentation products; the time of the crude fermentation is 6-10 days, the temperature of the crude fermentation is 25-28 ℃, and the pressure of the crude fermentation is 0.08-0.1 Mpa;
s4, stirring, centrifuging and filtering the aesculus hippocastanum seed fermentation product obtained in the step S3, and removing filter residues to obtain a aesculus hippocastanum seed fermentation product filtrate;
s5, processing the filter residue obtained in the step S4 as follows:
a. drying the filter residue at 90-100 ℃ to obtain filter residue cake, shearing at high speed and crushing into powder, and placing in a container;
b. adding 30-45 parts by mass of hot pure water at 85-90 ℃ into 10-20 parts by mass of powder, soaking for 30-60 minutes, filtering to another container, keeping filtrate, and removing filter residues;
c. 0.1-5 parts by mass of flocculating agent Al is added2 (SO4) 3 Precipitating, removing impurities, cooling, and keeping the upper filtrate;
d. c, adding 30-60 parts by mass of 70-95% ethanol solution into the upper filtrate obtained in the step c, soaking and stirring for 2-4 hours, precipitating and filtering;
e. d, circularly decoloring the filtrate flow obtained in the step d in a decoloring device for 18-22 minutes;
f. distilling and concentrating the decolorized solution for 2-8 h, condensing the steam by a condensing device, and recovering an ethanol solution;
g. vacuum drying the crude aesculus hippocastanum seed fermentation product after distillation and concentration to obtain a solid finished product;
s6, mixing the fermentation liquid of the aesculus hippocastanum seeds obtained in the S4 and the solid finished products of the aesculus hippocastanum seeds obtained in the S5 according to the ratio of 2: 1-1: 2, adding the polyalcohol to dissolve the aesculus hippocastanum seed extract into a thick slurry solution, wherein the polyalcohol accounts for 10wt% of the thick slurry solution.
The test data for each example and comparative example are as follows:
as can be seen from the comparison of examples and comparative examples, the aesculus hippocastanum seed extract obtained by the extraction method of the present invention has a better effect on the microenvironment of the scalp and has a lower residual amount of surfactant, and thus it can be said that the extract obtained by the extraction method has a higher aesculus hippocastanum seed extract than a general aesculus hippocastanum seed extract. In addition, the example 1 and the comparative example 2 show that if the matrix disclosed by the invention is not selected, the bacteriostatic efficiency of the matrix does not reach a more ideal state, and therefore, the synergistic matching of the matrix is also important to fully exert the efficacy of the extract.
Claims (2)
1. A shampoo composition containing an extract of aesculus hippocastanum seeds is characterized by comprising the following raw materials in percentage by weight:
(A) concentrated pulp solution of Aesculus hippocastanum seed extract 0.01-30%;
(B) 0.01-10% of anionic surfactant;
(C) 0.5 to 10 percent of amphoteric surfactant;
(D) 0.05-3% of cationic polysaccharide polymer; the cationic polysaccharide polymer is cationic guar gum, the charge density of the cationic guar gum is 0.6-0.9 meq/g, and the molecular weight is 450000-1300000 g/mol;
(E) 0.01-10% of rheology modifier or appearance modifier; and the remainder of
(F) Pure water;
the anionic surfactant is sodium laureth sulfate, sodium laureth sulfate and coconut oil agent monoethanolamide;
the amphoteric surfactant is cocamidopropyl betaine;
the rheological modifier or the appearance modifier is polydimethylsiloxane or ethylene glycol distearate;
the extraction method of the concentrated pulp solution of the aesculus hippocastanum seed extract sequentially comprises the following steps:
s1, washing the seeds of the aesculus hippocastanum, wherein the weight ratio of the seeds is 50-55: adding deionized water according to the mass ratio of 35-50, and coarsely crushing to obtain mixed European horse chestnut seed primary pulp;
s2, respectively activating lactic acid bacteria accounting for 0.5-2wt% of the S1 material and yeast accounting for 0.5-2wt% of the S1 material to respectively obtain a lactic acid bacteria secondary seed liquid and a yeast secondary seed liquid;
s3, inoculating the secondary seed liquid of the lactic acid bacteria and the secondary seed liquid of the microzyme obtained in the step S2 into the primary pulp of the European horse chestnut seeds obtained in the step S1, and performing coarse fermentation, wherein 0.5-2wt% of urea is supplemented in the process to obtain the European horse chestnut seed fermentation product; the time of the crude fermentation is 6-10 days, the temperature of the crude fermentation is 25-28 ℃, and the pressure of the crude fermentation is 0.08-0.1 Mpa;
s4, stirring, centrifuging and filtering the aesculus hippocastanum seed fermentation product obtained in the step S3, and removing filter residues to obtain a aesculus hippocastanum seed fermentation product filtrate;
s5, processing the filter residue obtained in the step S4 as follows:
a. drying the filter residue at 90-100 ℃ to obtain filter residue cake, shearing at high speed and crushing into powder, and placing in a container;
b. adding 30-45 parts by mass of hot pure water at 85-90 ℃ into 10-20 parts by mass of powder, soaking for 30-60 minutes, filtering to another container, keeping filtrate, and removing filter residues;
c. 0.1-5 parts by mass of flocculating agent Al is added2 (SO4) 3 Precipitating, removing impurities, cooling, and keeping the upper filtrate;
d. c, adding 30-60 parts by mass of 70-95% ethanol solution into the upper filtrate obtained in the step c, soaking and stirring for 2-4 hours, precipitating and filtering;
e. d, circularly decoloring the filtrate flow obtained in the step d in a decoloring device for 18-22 minutes;
f. distilling and concentrating the decolorized solution for 2-8 h, condensing the steam by a condensing device, and recovering an ethanol solution;
g. vacuum drying the crude aesculus hippocastanum seed fermentation product after distillation and concentration to obtain a solid finished product;
s6, mixing the fermentation liquid of the aesculus hippocastanum seeds obtained in the S4 and the solid finished products of the aesculus hippocastanum seeds obtained in the S5 according to the ratio of 2: 1-1: 2, adding the polyalcohol to dissolve the aesculus hippocastanum seed extract into a thick slurry solution, wherein the polyalcohol accounts for 10wt% of the thick slurry solution.
2. A shampoo composition according to claim 1, characterised in that: also contains at least one of the following components:
suspending agent: 0.01 to 5 percent;
nonionic surfactant: 0.01 to 5 percent;
non-volatile conditioning agents: 0.01 to 3 percent;
organic conditioning oil: 0.01-2%;
preservative: 0.01-1%;
essence: 0.01 to 3 percent;
viscosity modifier: 0.01-4%;
light screening agent: 0.01 to 1.0 percent
Chelating agent: 0.005-0.2%;
ultraviolet absorber: 0.01-2%;
other plant extracts: 0.0001-5%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711127147.7A CN107890439B (en) | 2017-11-15 | 2017-11-15 | Extraction method of aesculus hippocastanum seed extract and hair washing composition thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711127147.7A CN107890439B (en) | 2017-11-15 | 2017-11-15 | Extraction method of aesculus hippocastanum seed extract and hair washing composition thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN107890439A CN107890439A (en) | 2018-04-10 |
| CN107890439B true CN107890439B (en) | 2021-04-27 |
Family
ID=61805253
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711127147.7A Active CN107890439B (en) | 2017-11-15 | 2017-11-15 | Extraction method of aesculus hippocastanum seed extract and hair washing composition thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107890439B (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110693927A (en) * | 2019-11-27 | 2020-01-17 | 深圳市星银医药有限公司 | Preparation method of horse chestnut extract |
| CN115581653B (en) * | 2022-09-30 | 2023-08-04 | 广州市博之越精细化工有限公司 | Shumin repair agent and application thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105132491A (en) * | 2015-10-23 | 2015-12-09 | 山东迅达康兽药有限公司 | Pachymaran extracting method |
| CN106309278A (en) * | 2016-08-31 | 2017-01-11 | 澳宝化妆品（惠州）有限公司 | Maguey leavening for anti-aging cosmetics and preparation method and application of maguey leavening |
| CN106333881A (en) * | 2016-10-26 | 2017-01-18 | 澳宝化妆品（惠州）有限公司 | Moistening, bubbly and stable cream bath combination |
| CN106619237A (en) * | 2016-12-16 | 2017-05-10 | 广东芭薇生物科技股份有限公司 | Plant compound extract-containing skin care composition |
-
2017
- 2017-11-15 CN CN201711127147.7A patent/CN107890439B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105132491A (en) * | 2015-10-23 | 2015-12-09 | 山东迅达康兽药有限公司 | Pachymaran extracting method |
| CN106309278A (en) * | 2016-08-31 | 2017-01-11 | 澳宝化妆品（惠州）有限公司 | Maguey leavening for anti-aging cosmetics and preparation method and application of maguey leavening |
| CN106333881A (en) * | 2016-10-26 | 2017-01-18 | 澳宝化妆品（惠州）有限公司 | Moistening, bubbly and stable cream bath combination |
| CN106619237A (en) * | 2016-12-16 | 2017-05-10 | 广东芭薇生物科技股份有限公司 | Plant compound extract-containing skin care composition |
Non-Patent Citations (1)
| Title |
|---|
| "欧洲七叶树的化学、药理作用和临床";刘湘;《国外医药 植物药分册》;19990415;第14卷(第2期);47-52 * |
Also Published As
| Publication number | Publication date |
|---|---|
| CN107890439A (en) | 2018-04-10 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN107438427B (en) | Shampoo | |
| CN102796205B (en) | Preparation method of high-transparency scleroglucan | |
| CN110478305A (en) | A kind of preparation process and its application of sheep placenta extract | |
| CN107890439B (en) | Extraction method of aesculus hippocastanum seed extract and hair washing composition thereof | |
| CN105687040B (en) | A kind of multi-functional lotion and preparation method thereof of zymolyte containing seaweed and collagen | |
| CN106798656B (en) | Deep hair nourishing essence containing yak bone small molecule peptide and preparation method thereof | |
| CN112263537A (en) | Whitening and antioxidant toning lotion rich in ergothioneine and preparation method thereof | |
| CN111840172A (en) | Skin-beautifying firming cream and preparation method thereof | |
| CN108635275B (en) | Antioxidant composition and application thereof in essence | |
| CN109276502A (en) | Water storage facial mask | |
| CN110882172B (en) | Multi-effect hair care shampoo containing paeonol and preparation method thereof | |
| CN107468560B (en) | Shampoo composition containing tea extract | |
| CN106727255B (en) | Shampoo containing natural surfactant and preparation method thereof | |
| KR101675916B1 (en) | Cosmetic Composition Comprising Ribonucleic acid and Extract of Magnolia sieboldii as active ingredient | |
| KR100868929B1 (en) | Cleansing composition comprising red-dog extract and preparation method thereof | |
| CN103599054B (en) | Containing the facial film and preparation method thereof of peanut protein polypeptide | |
| JP2002284632A (en) | Extinction substance for superoxide anion extracted from sake lees as effective component | |
| CN112442466B (en) | Rice washing water fermentation product with scalp aging resisting function and preparation method thereof | |
| KR101908476B1 (en) | Cosmetic composition comprising rx complex | |
| CN114939092A (en) | Natural hot spring shampoo and preparation method thereof | |
| KR20150081892A (en) | Cosmetic composition comprising the extract of Helianthus Tuberosus Root | |
| CN106377458A (en) | Shampoo composition containing tea seed cake extracts and preparation method thereof | |
| CN112852549A (en) | Method for extracting plant hydrolat by using double auxiliary agents | |
| CN109908061A (en) | A kind of fizzy dandruff control shampoo containing and preparation method thereof | |
| CN117752562A (en) | Alfalfa extract and application thereof in shampoo composition |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| CB02 | Change of applicant information |
Address after: 516000 Licheng industrial area, Shuikou Town, Huicheng District, Huizhou, Guangdong, China Applicant after: Huizhou Zhaoting Cosmetic Co., Ltd. Address before: 516000 Licheng industrial area, Shuikou Town, Huicheng District, Huizhou, Guangdong, China Applicant before: Huizhou Zhao Qi Gift Co. Ltd. |
|
| CB02 | Change of applicant information | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |