CN102503429B - 常压烧结碳化硼陶瓷的制备方法 - Google Patents
常压烧结碳化硼陶瓷的制备方法 Download PDFInfo
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- CN102503429B CN102503429B CN201110312450.0A CN201110312450A CN102503429B CN 102503429 B CN102503429 B CN 102503429B CN 201110312450 A CN201110312450 A CN 201110312450A CN 102503429 B CN102503429 B CN 102503429B
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- boron carbide
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- 229910052580 B4C Inorganic materials 0.000 title claims abstract description 49
- INAHAJYZKVIDIZ-UHFFFAOYSA-N boron carbide Chemical compound B12B3B4C32B41 INAHAJYZKVIDIZ-UHFFFAOYSA-N 0.000 title claims abstract description 49
- 239000000919 ceramic Substances 0.000 title claims abstract description 38
- 238000005245 sintering Methods 0.000 title claims abstract description 30
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- 239000000843 powder Substances 0.000 claims abstract description 27
- 239000000463 material Substances 0.000 claims abstract description 26
- 239000002002 slurry Substances 0.000 claims abstract description 23
- 238000000498 ball milling Methods 0.000 claims abstract description 17
- 238000001694 spray drying Methods 0.000 claims abstract description 16
- 235000015895 biscuits Nutrition 0.000 claims abstract description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000008367 deionised water Substances 0.000 claims abstract description 6
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 6
- 238000003825 pressing Methods 0.000 claims abstract description 5
- 238000005469 granulation Methods 0.000 claims description 28
- 230000003179 granulation Effects 0.000 claims description 28
- 229910010271 silicon carbide Inorganic materials 0.000 claims description 18
- 239000003795 chemical substances by application Substances 0.000 claims description 14
- 239000002994 raw material Substances 0.000 claims description 12
- 239000006185 dispersion Substances 0.000 claims description 9
- 239000003595 mist Substances 0.000 claims description 9
- 238000002156 mixing Methods 0.000 claims description 8
- WGTYBPLFGIVFAS-UHFFFAOYSA-M tetramethylammonium hydroxide Chemical compound [OH-].C[N+](C)(C)C WGTYBPLFGIVFAS-UHFFFAOYSA-M 0.000 claims description 8
- 239000000571 coke Substances 0.000 claims description 6
- 238000000227 grinding Methods 0.000 claims description 6
- 238000001816 cooling Methods 0.000 claims description 4
- 229920001353 Dextrin Polymers 0.000 claims description 3
- 239000004375 Dextrin Substances 0.000 claims description 3
- 235000019425 dextrin Nutrition 0.000 claims description 3
- -1 40 grams Substances 0.000 claims description 2
- 238000000034 method Methods 0.000 abstract description 23
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract description 15
- 239000007787 solid Substances 0.000 abstract description 6
- 238000004519 manufacturing process Methods 0.000 abstract description 5
- 238000005516 engineering process Methods 0.000 abstract description 4
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 abstract description 4
- 230000001681 protective effect Effects 0.000 abstract description 2
- 238000009694 cold isostatic pressing Methods 0.000 abstract 1
- 229910052799 carbon Inorganic materials 0.000 description 12
- 239000000428 dust Substances 0.000 description 8
- 238000004537 pulping Methods 0.000 description 6
- 239000011230 binding agent Substances 0.000 description 4
- 239000007789 gas Substances 0.000 description 4
- 239000002245 particle Substances 0.000 description 4
- 239000004372 Polyvinyl alcohol Substances 0.000 description 3
- 238000005452 bending Methods 0.000 description 3
- 238000007731 hot pressing Methods 0.000 description 3
- 238000005360 mashing Methods 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 239000012071 phase Substances 0.000 description 3
- 229920002037 poly(vinyl butyral) polymer Polymers 0.000 description 3
- 229920002451 polyvinyl alcohol Polymers 0.000 description 3
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 2
- 229910010293 ceramic material Inorganic materials 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000005056 compaction Methods 0.000 description 2
- 239000008103 glucose Substances 0.000 description 2
- 238000011031 large-scale manufacturing process Methods 0.000 description 2
- 239000007791 liquid phase Substances 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- 239000003643 water by type Substances 0.000 description 2
- 229910052582 BN Inorganic materials 0.000 description 1
- PZNSFCLAULLKQX-UHFFFAOYSA-N Boron nitride Chemical compound N#B PZNSFCLAULLKQX-UHFFFAOYSA-N 0.000 description 1
- 239000003082 abrasive agent Substances 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000001133 acceleration Effects 0.000 description 1
- DHKHKXVYLBGOIT-UHFFFAOYSA-N acetaldehyde Diethyl Acetal Natural products CCOC(C)OCC DHKHKXVYLBGOIT-UHFFFAOYSA-N 0.000 description 1
- 125000002777 acetyl group Chemical class [H]C([H])([H])C(*)=O 0.000 description 1
- 235000011114 ammonium hydroxide Nutrition 0.000 description 1
- 229910052786 argon Inorganic materials 0.000 description 1
- 238000000889 atomisation Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000006229 carbon black Substances 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000001186 cumulative effect Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000000280 densification Methods 0.000 description 1
- 229910003460 diamond Inorganic materials 0.000 description 1
- 239000010432 diamond Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000008188 pellet Substances 0.000 description 1
- 238000005498 polishing Methods 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 239000004576 sand Substances 0.000 description 1
- 239000003566 sealing material Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
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- Carbon And Carbon Compounds (AREA)
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Families Citing this family (15)
Publication number | Priority date | Publication date | Assignee | Title |
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CN103073298A (zh) * | 2013-02-25 | 2013-05-01 | 常熟华融太阳能新型材料科技有限公司 | 高纯碳化硼陶瓷的制备方法 |
CN103613389B (zh) * | 2013-11-29 | 2015-11-25 | 宁波伏尔肯机械密封件制造有限公司 | 碳化硼陶瓷烧结制备方法 |
CN104529457B (zh) * | 2014-12-03 | 2017-06-13 | 中国兵器工业第五二研究所烟台分所 | 基于粗颗粒粉体的无压烧结碳化硼陶瓷制备方法 |
CN104628387A (zh) * | 2015-02-07 | 2015-05-20 | 宁波伏尔肯机械密封件制造有限公司 | 一种异型碳化硼陶瓷喷砂嘴的制备方法 |
CN108218432A (zh) * | 2017-12-29 | 2018-06-29 | 安徽应流久源核能新材料科技有限公司 | 一种辐射屏蔽组件用碳化硼烧结块的加工工艺 |
CN108276003A (zh) * | 2018-02-13 | 2018-07-13 | 苏州纳朴材料科技有限公司 | 一种利用蓝宝石研磨废弃料制备碳化硼复相陶瓷的方法 |
CN108516831B (zh) * | 2018-03-22 | 2020-12-29 | 宁波哈泰雷碳化物有限公司 | 一种防弹陶瓷整板的制备方法 |
CN108439988A (zh) * | 2018-05-16 | 2018-08-24 | 苏州汉尼威电子技术有限公司 | 一种高性能水刀陶瓷砂管及其制备方法 |
CN108640687B (zh) * | 2018-05-29 | 2021-02-05 | 北京理工大学 | 一种碳化硼/碳化硅复相陶瓷及其制备方法 |
KR20200019068A (ko) * | 2018-08-13 | 2020-02-21 | 에스케이씨솔믹스 주식회사 | 탄화붕소 소결체 및 이를 포함하는 식각장치 |
CN109704771B (zh) * | 2019-01-17 | 2021-11-19 | 宁波伏尔肯科技股份有限公司 | 一种高温气冷堆核控制棒用碳化硼多孔陶瓷的制备方法 |
CN111348916A (zh) * | 2020-02-17 | 2020-06-30 | 江苏大学 | 一种高性能碳化硼研磨介质、制备方法及其应用 |
CN111807841A (zh) * | 2020-07-02 | 2020-10-23 | 山东国晶新材料有限公司 | 一种碳化硼陶瓷的制备方法 |
CN113620714A (zh) * | 2021-07-22 | 2021-11-09 | 安徽应流久源核能新材料科技有限公司 | 一种碳化硼-石墨屏蔽体的制备方法 |
CN114671689A (zh) * | 2022-02-28 | 2022-06-28 | 宁波伏尔肯科技股份有限公司 | 一种热压液相烧结碳化硼复合陶瓷及其制备方法 |
Citations (2)
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CN101525240A (zh) * | 2009-04-23 | 2009-09-09 | 浙江大学 | 硼化物增强型碳化硅陶瓷及其制备方法 |
CN101555143A (zh) * | 2009-05-12 | 2009-10-14 | 宁波欧翔精细陶瓷技术有限公司 | 常压烧结碳化硅陶瓷的制备方法 |
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CN100528425C (zh) * | 2007-11-22 | 2009-08-19 | 上海交通大学 | 活泼金属钛和碳化硼复合球形热喷涂粉末的制备方法 |
CN101280129B (zh) * | 2008-05-22 | 2010-10-27 | 上海交通大学 | 金属钛、钴和碳化硼混合热喷涂粉末浆料制备方法 |
CN102194532A (zh) * | 2011-04-07 | 2011-09-21 | 清华大学 | 一种碳化硼与炭素复合粉体的制备方法 |
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- 2011-10-17 CN CN201110312450.0A patent/CN102503429B/zh active Active
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101525240A (zh) * | 2009-04-23 | 2009-09-09 | 浙江大学 | 硼化物增强型碳化硅陶瓷及其制备方法 |
CN101555143A (zh) * | 2009-05-12 | 2009-10-14 | 宁波欧翔精细陶瓷技术有限公司 | 常压烧结碳化硅陶瓷的制备方法 |
Non-Patent Citations (4)
Title |
---|
喷雾造粒制备SiC-AlN复合粉体特性及烧结性能;郭兴忠等;《中国有色金属学报》;20081031;第18卷(第10期);第1846-1851页 * |
李海淼等.水基SiC浆料的喷雾造粒特性.《陶瓷学报》.2007,第28卷(第3期),第160-163页. |
水基SiC浆料的喷雾造粒特性;李海淼等;《陶瓷学报》;20070930;第28卷(第3期);第160-163页 * |
郭兴忠等.喷雾造粒制备SiC-AlN复合粉体特性及烧结性能.《中国有色金属学报》.2008,第18卷(第10期),第1846-1851页. |
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Inventor after: Wu Guoping Inventor after: Jiao Yongfeng Inventor after: Xie Fangmin Inventor before: Wu Guoping |
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Free format text: CORRECT: INVENTOR; FROM: WU GUOPING TO: WU GUOPING JIAO YONGFENG XIE FANGMIN |
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Address after: 315104 Jin Yuan Road, Yinzhou investment and business center, Zhejiang, Ningbo, China, No. 666 Patentee after: Ningbo fu'erken Ceramic Technology Co. Ltd. Address before: 315104 Jin Yuan Road, Yinzhou investment and business center, Zhejiang, Ningbo, China, No. 666 Patentee before: Ningbo Vulcan Mechanical Seals Manufacturing Co., Ltd. |
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Address after: 315104 Jin Yuan Road, Yinzhou investment and entrepreneurship center, Ningbo, Zhejiang 666 Patentee after: Ningbo Vulcan Polytron Technologies Inc Address before: 315104 Jin Yuan Road, Yinzhou investment and entrepreneurship center, Ningbo, Zhejiang 666 Patentee before: Ningbo fu'erken Ceramic Technology Co. Ltd. |
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