CN102429135A - Feed used in later laying peak period of SPF (specific pathogen free) breeding hens and preparation method thereof - Google Patents

Feed used in later laying peak period of SPF (specific pathogen free) breeding hens and preparation method thereof Download PDF

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CN102429135A
CN102429135A CN2011104330882A CN201110433088A CN102429135A CN 102429135 A CN102429135 A CN 102429135A CN 2011104330882 A CN2011104330882 A CN 2011104330882A CN 201110433088 A CN201110433088 A CN 201110433088A CN 102429135 A CN102429135 A CN 102429135A
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parts
feed
spf
sterilization
irradiation
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CN102429135B (en
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冯艳忠
李凤兰
姜宇
郭志波
陈振宇
陈晶宇
赵辉
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HARBIN PHARMACEUTICAL GROUP BIOLOGICAL VACCINE CO Ltd
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Abstract

The invention discloses a feed used in the later laying peak period of SPF (specific pathogen free) breeding hens and a preparation method thereof. The feed is characterized by comprising the following raw materials in parts by weight: 620-640 parts of corn meal, 200-220 parts of bean pulp, 25-35 parts of wheat bran, 15-25 parts of fish meal, 1-2 parts of 98% of methionine, 70-90 parts of limestone meal, 10-14 parts of calcium hydrophosphate, 2.5-3.5 parts of salt and 10 parts of premix. Compared with the traditional sterilization method, the preparation method is characterized by adopting a Co60 ray source for radiation sterilization and strictly limiting the radiation dose rate and radiation time. The feed subjected to radiation sterilization of the Co60 ray source has low nutrient losses, good sterilization effect and low cost and is suitable for industrial production.

Description

A kind of SPF of being used for kind chicken feed in peak later stage and preparation method thereof of laying eggs
Technical field
The present invention relates to a kind of chicken feed and preparation method thereof, the particularly a kind of SPF of being used for kind chicken feed in peak later stage and preparation method thereof of laying eggs belongs to field of feed processing.
Background technology
The whole world has millions of agri-scientific researches and technology popularization personnel to be engaged in the research and the production of making the required SPF egg of animal vaccine source, can't find reasonable effective technology to stop the predicament that SPF chicken group support is grown the failure generation but face.
Produce SPF kind egg adopt conventional method for breeding cannot, we know that the breed of SPF chicken needs specific room, equipment and feed; SPF chicken feed is several special processed before feeding, and purpose is exactly the special pathogen of killing in the SPF chicken feed, and then are transported to SPF chicken breed house through specific channel; Not only the SPF chicken comprises all apparatus and poultry raiser etc., all can not bring any special pathogen into the SPF chicken and culture house; The purpose of all these loaded down with trivial details links has only a high-quality and safety of be exactly making international endorsement, does not carry the animal vaccine product of specific pathogen microorganism; Then, according to antibody test level and immunology principle in the animal body, and the vaccine characteristic is in rational time, carry out immunity to animal according to rational vaccine method for using, dosage targetedly; And the quality of vaccine is particularly important; Raw material-SPF egg quality of making the vaccine use is more crucial, and is domestic when paying close attention to the animal vaccine quality, more pays close attention to the nutrition and the processing technology of SPF chicken feed; Particularly determine SPF chicken group support to grow the process of killing and the technology of specific pathogen microorganism in the feed that success or failure play a crucial role; Our country puts into effect Policy Conditions separately for this reason, and the egg of making biovaccine must use international SPF egg, and this also is one of China's biovaccine goods key technology point in line with international standards at first; When the animal vaccine of only in this way producing can really reach the specific aim immunity; Be unlikely to take other specific pathogen microorganisms in the animal vaccine to,, spread the specific pathogen microorganism of carrying because of vaccine to such an extent as to cause in this zoonotic while of immunity; Cause the propagation and the diffusion of other infectious diseases, with the happy life of protection human health and happiness.
At present both at home and abroad the trend of research is to kill the specific pathogen microorganism in the SPF chicken feed with processing technology efficiently; In this processing procedure, avoid destroying the nutritive index in the feed as much as possible; Particularly do not destroy the protein in the feed, the composition of vitamin as far as possible; But this is a vision, and the way in the actual production is when the design feed formula; Add excessive nutriment; The nutriment that particularly in the processed process, is easy to processed operation destruction wants excess to add, and to ensure that feed is easy to the nutritional need that ruined nutriment can satisfy SPF chicken crowd in the pathogenic microbe killing process, brings into play SPF chicken crowd's production performance as far as possible;
Adopting at present the more method of killing special pathogen employing in the SPF kind chicken feed in the world is greatly the high-pressure water vapor sterilization; Pack handy specific Polypropylence Sheet to the good finished feed of production exactly and pack, in the high-pressure chamber of packing into, the feeding water vapour makes it pressure and reaches 4.5 standard atmospheric pressures; Temperature reaches more than 120 degrees centigrade; And keep water vapour to flow, and sterilization time reached more than 45 minutes, and sampling detects under special circumstances then; Can use after guaranteeing not contain special pathogen in the feed; The method is time-consuming, effort, waste resource, but also will need the steam boiler fire coal a large amount of with waste, and coal also will produce pollutant such as waste gas such as a large amount of carbon dioxide and dust and environment is caused very big pressure and pollution in combustion process; Simultaneously; Also cause a large amount of losses of nutriment when in utilizing the autoclaved process of water vapour, killing special pathogen, more trouble be and be cause feed humidity and moisture increase and cause the shortening of feed storage time, even cause the growth of mould in the feed and the generation of mycotoxin at high temperature season.
The method that the present invention adopts is the Co that uses atomic energy 60Carry out irradiation; Take certain irradiation dose and exposure time to kill the method for the special pathogen in the feed; The nutritive index of the feed that needs because of SPF kind chicken different life has a long way to go; Feed formula has a long way to go with the feed raw material that need, so kill the needed atomic energy Co of special pathogen in the feed 60Irradiation dose and exposure time gap also very big, so concentrations of nutrient such as multivitamin that in the irradiation process, is easy to lose in the feed and mineral trace element, protein, amino acid, energy and the conventional chicken feed of planting have very big difference.
For this reason, the present invention designs the feed formula that following suitable SPF kind chicken was used in the peak later stage of laying eggs, according to the atomic energy Co that the present invention adopted 60Irradiation dose and exposure time kill the SPF kind chicken of feeding behind the special pathogen in the feed and obtained better effects.
Summary of the invention
The present invention is through lay eggs the peak later stage nutritional need of SPF kind chicken of (421 ages in days-500 eliminate) of analysis-by-synthesis, scientific and reasonable the lay eggs feed in peak later stage of a kind of SPF of being used for kind chicken that made.
The lay eggs feed in peak later stage of a kind of SPF of being used for kind chicken of the present invention; It is characterized in that being made up of each raw material of following weight portion: 620-640 part corn flour, 200-220 part dregs of beans, 25-35 part wheat bran, 15-25 part fish meal, 1-2 part content are methionine, 70-90 part stone flour, 10-14 part calcium monohydrogen phosphate, 2.5-3.5 part salt and 10 parts of premixes of 98%; Contain compound vitamin 20kg, grandidierite dimension 200kg, Choline Chloride 200kg, imported fish meal 400kg and 200 order zeolite powder 180kg in the described premix wherein per ton, said each raw material mixes the back sterilization and promptly gets.
In a preferred embodiment of the invention; The lay eggs feed in peak later stage of the described SPF of being used for kind chicken is made up of each raw material of following weight portion: 634 portions of corn flour, 210 parts of dregs of beans, 30 parts of wheat brans, 20 parts of fish meal, 1.6 parts of content are 98% methionine, 80 parts of stone flours, 12 parts of calcium monohydrogen phosphates, 3 portions of salt and 10 parts of premixes; Contain compound vitamin 20kg, grandidierite dimension 200kg, Choline Chloride 200kg, imported fish meal 400kg and 200 order zeolite powder 180kg in the described premix wherein per ton, said each raw material mixes the back sterilization and promptly gets.
Wherein, preferred, described sterilization is to adopt Co 60Radiographic source irradiation sterilization, irradiation field calibrated error are less than ± 5%, and absorption of sample dosage unevenness is less than 1.2, and radiation dose rate is 25Gy/min, and exposure time is 60 hours.
In a preferred embodiment of the invention, feed formula of the present invention and nutritive index are as shown in table 1:
Table 1 lay eggs peak later stage feed formula and nutritive index (421 ages in days-500 are eliminated)
Figure BDA0000123318850000031
Contain compound vitamin 20kg, grandidierite dimension 200kg, Choline Chloride 200kg, imported fish meal 400kg and 200 order zeolite powder 180kg in the described premix wherein per ton.
The present invention also provides a kind of method for preparing said feed; It is characterized in that described each raw material is mixed according to above arbitrary described weight ratio, adopt nylon-polyethylene compound package material to pack every bag of 40KG; Volume is 80cm*40cm*20cm, uses Co 60Radiographic source irradiation sterilization, irradiation field calibrated error are less than ± 5%, and absorption of sample dosage unevenness is less than 1.2; Sample irradiation is during to a half-value dose; The turn-over continued irradiation in the original place, radiation dose rate is 25Gy/min, exposure time 60 hours; To be stored in 20 ± 5 ℃, relative humidity be the indoor of 40-70% to feed behind the irradiation, finishes using in three weeks.
Compared to prior art, the invention has the advantages that:
1, feed formula is scientific and reasonable, has satisfied SPF kind chicken greatly at the nutritional need in peak later stage of laying eggs, and the SPF kind chicken of edible feed of the present invention is higher than height, average egg weight compared to the SPF kind egg material that adopts normal diet to feed;
2, the present invention adopts atomic energy Co 60Feed is carried out irradiation sterilization, after three weeks, the special pathogen in the feed is detected, testing result is zero;
3, according to atomic energy Co that the present invention adopted 60Irradiation dose and exposure time kill special pathogen in the feed, few to the loss of concentrations of nutrient such as the multivitamin in the feed and mineral trace element, protein, amino acid, energy.
4, the present invention adopts atomic energy Co 60Feed is carried out irradiation sterilization, and simple to operate, convenient, the feed after the sterilization is stored easily, greatly reduces the cost of producing SPF kind chicken feed, can satisfy the demand of large-scale production SPF kind chicken feed.
The specific embodiment
Further describe the present invention below in conjunction with specific embodiment, advantage of the present invention and characteristics will be more clear along with description.But these embodiment only are exemplary, scope of the present invention are not constituted any restriction.It will be understood by those skilled in the art that and down can make amendment with form or replace without departing from the spirit and scope of the present invention, but these modifications and replacing all fall in protection scope of the present invention the details of technical scheme of the present invention.
Raw material: (through diameter is the corn flour after 3 millimeters sieve sheet is pulverized to corn flour.), dregs of beans, wheat bran, fish meal, content be 98% methionine, stone flour, calcium monohydrogen phosphate, salt and premix respectively available from the prosperous biotechnology Co., Ltd of herding in the Heilongjiang Province of herding research institute of Heilongjiang Institute of Agricultural Sciences, premix composition per ton and content are as shown in table 2:
Table 2 premix composition per ton and content:
2 ‰ compound vitamins 2% grandidierite dimension 50% Choline Chloride Imported fish meal 200 order zeolite powders
20kg ?200kg 200kg 400kg ?180kg
Embodiment 1
Take by weighing each raw material respectively by weight portion of the present invention: the content of 634kg corn flour, 210kg dregs of beans, 30kg wheat bran, 20kg fish meal, 1.6kg is 98% methionine, 80kg stone flour, 12kg calcium monohydrogen phosphate, 3kg salt and 10kg premix, wherein contains compound vitamin 20g, grandidierite dimension 200g, Choline Chloride 200g, imported fish meal 400g and 200 order zeolite powder 180g in every kilogram of described premix.
Each raw material pulverizing of above-mentioned weight is mixed, adopt nylon-polyethylene compound package material to pack, every bag of 40KG, volume are 80cm*40cm*20cm, use Co 60Radiographic source irradiation sterilization, irradiation field calibrated error are less than ± 5%, and absorption of sample dosage unevenness is less than 1.2; Sample irradiation is during to a half-value dose; The turn-over continued irradiation in the original place, radiation dose rate is 25Gy/min, exposure time 60 hours; Behind the irradiation feed be stored in 20 ℃, relative humidity be 50% indoor, finish using in three weeks.
Embodiment 2
Take by weighing each raw material respectively by weight portion of the present invention: the content of 630kg corn flour, 205kg dregs of beans, 30kg wheat bran, 20kg fish meal, 2kg is 98% methionine, 90kg stone flour, 10kg calcium monohydrogen phosphate, 3kg salt and 10kg premix, wherein contains compound vitamin 20g, grandidierite dimension 200g, Choline Chloride 200g, imported fish meal 400g and 200 order zeolite powder 180g in every kilogram of described premix.
Each raw material pulverizing of above-mentioned weight is mixed, adopt nylon-polyethylene compound package material to pack, every bag of 40KG, volume are 80cm*40cm*20cm, use Co 60Radiographic source irradiation sterilization, irradiation field calibrated error are less than ± 5%, and absorption of sample dosage unevenness is less than 1.2; Sample irradiation is during to a half-value dose; The turn-over continued irradiation in the original place, radiation dose rate is 25Gy/min, exposure time 60H; Behind the irradiation feed be stored in 20 ℃, relative humidity be 50% indoor, finish using in three weeks.
Embodiment 3
Take by weighing each raw material respectively by weight portion of the present invention: the content of 638kg corn flour, 220kg dregs of beans, 30kg wheat bran, 15kg fish meal, 1kg is 98% methionine, 70kg stone flour, 14kg calcium monohydrogen phosphate, 2.5kg salt and 10kg premix, wherein contains compound vitamin 20g, grandidierite dimension 200g, Choline Chloride 200g, imported fish meal 400g and 200 order zeolite powder 180g in every kilogram of described premix.
Each raw material pulverizing of above-mentioned weight is mixed, adopt nylon-polyethylene compound package material to pack, every bag of 40KG, volume are 80cm*40cm*20cm, use Co 60Radiographic source irradiation sterilization, irradiation field calibrated error are less than ± 5%, and absorption of sample dosage unevenness is less than 1.2; Sample irradiation is during to a half-value dose; The turn-over continued irradiation in the original place, radiation dose rate is 25Gy/min, exposure time 60H; Behind the irradiation feed be stored in 20 ℃, relative humidity be 50% indoor, finish using in three weeks.
Test Example 1
Adopt embodiment 1 described method to prepare 1 batch of feed, be divided into 10 groups, Co 60Week about 10 groups of feeds are carried out the detection of specific pathogen bacterium behind the radiographic source irradiation sterilization respectively, testing result is as shown in table 3.
Table 3Co 60Irradiation sterilization experimental design prescription specific pathogen recall rate
Figure BDA0000123318850000061
Can find out from The above results, adopt the feed after method of the present invention is sterilized, in the 3rd week after sterilization,, the edible safety that sterilizing methods sterilization of the present invention is thorough, effective, guaranteed SPF kind chicken is described still not by detecting any specific pathogen bacterium.
Test Example 2
In order to contrast each changes of Nutritional Components situation behind the feed predose, the content of nutritional labeling in the feed behind the predose is measured, the result is as shown in table 4.
The nutritive index table of comparisons behind the table 4 feed predose
Figure BDA0000123318850000062
Test Example 3
Lay eggs the peak later stage SPF kind chicken of (421 ages in days-500 are eliminated) of the forage feed that adopts embodiment 1 to prepare is added up the adult livability in the peak later stage of laying eggs, and the result is as shown in table 5.
Table 5Co 60The irradiation sterilization experimental design prescription peak later stage adult livability table of comparisons of laying eggs
Figure BDA0000123318850000071
Test Example 4
Being used for autoclaved feed formula is: 600kg corn flour, 240kg dregs of beans, 30kg wheat bran, 20kg fish meal, 1kg content are that 98% lysine, 80kg stone flour, 1.6kg content are 98% methionine, 15kg calcium monohydrogen phosphate, 2.4kg salt and 10kg premix, contain compound vitamin 20kg, grandidierite dimension 200kg, Choline Chloride 200kg, imported fish meal 400kg and 200 order zeolite powder 180kg in the described premix wherein per ton.
High-pressure sterilizing method: pack handy specific Polypropylence Sheet to the good finished feed of production and pack; Pack into then in the high-pressure chamber, the feeding water vapour makes it pressure and reaches 4.5 standard atmospheric pressures, and temperature reaches more than 120 degrees centigrade; And keeping water vapour to flow, sterilization time reached more than 45 minutes.
Adopt autoclaved feed formula and atomic energy irradiation sterilization feed of the present invention to raise 421 ages in days-500 age in days SPF kind chicken respectively; Every group 3000; After feeding 2 months SPF kind chicken is added up at the peak later stage chicken feed conversion rate of laying eggs; The result is as shown in table 6, adopts the average production performance index of the SPF kind chicken that two groups of DIFFERENT FEED feed as shown in table 7:
Table 6 autoclaving feed formula and the experimental design of the atomic energy irradiation sterilization prescription peak later stage chicken feed conversion rate table of comparisons of laying eggs
Figure BDA0000123318850000072
The average production performance index of table 7
Wherein, every of accumulative total goes into to give up laying hen egg yield=full crowd's egg production/go into hen number of house
Test Example 5
Adopt the embodiment of the invention 1 to prepare forage feed SPF kind chicken, parallelly carry out 10 groups, results SPF kind egg carries out the detection of 24 kinds of special pathogens, and testing result is as shown in table 8.
Table 8SPF kind egg 24 special pathogen testing results
Figure BDA0000123318850000082
Figure BDA0000123318850000091

Claims (4)

1. one kind is used for the lay eggs feed in peak later stage of SPF kind chicken; It is characterized in that being made up of each raw material of following weight portion: 620-640 part corn flour, 200-220 part dregs of beans, 25-35 part wheat bran, 15-25 part fish meal, 1-2 part content are methionine, 70-90 part stone flour, 10-14 part calcium monohydrogen phosphate, 2.5-3.5 part salt and 10 parts of premixes of 98%; Contain compound vitamin 20kg, grandidierite dimension 200kg, Choline Chloride 200kg, imported fish meal 400kg and 200 order zeolite powder 180kg in the described premix wherein per ton, said each raw material mixes the back sterilization and promptly gets.
2. the lay eggs feed in peak later stage of the SPF of being used for kind chicken as claimed in claim 1; It is characterized in that being made up of each raw material of following weight portion: 634 portions of corn flour, 210 parts of dregs of beans, 30 parts of wheat brans, 20 parts of fish meal, 1.6 parts of content are 98% methionine, 80 parts of stone flours, 12 parts of calcium monohydrogen phosphates, 3 portions of salt and 10 parts of premixes; Contain compound vitamin 20kg, grandidierite dimension 200kg, Choline Chloride 200kg, imported fish meal 400kg and 200 order zeolite powder 180kg in the described premix wherein per ton, said each raw material mixes the back sterilization and promptly gets.
3. according to claim 1 or claim 2 feed is characterized in that described sterilization is to adopt Co 60Radiographic source irradiation sterilization, irradiation field calibrated error are less than ± 5%, and absorption of sample dosage unevenness is less than 1.2, and radiation dose rate is 25Gy/min, and exposure time is 60 hours.
4. method for preparing each described feed of claim 1-3; It is characterized in that described each raw material is mixed according to claim 1 or 2 described weight ratios, adopt nylon-polyethylene compound package material to pack every bag of 40KG; Volume is 80cm*40cm*20cm, uses Co 60Radiographic source irradiation sterilization, irradiation field calibrated error are less than ± 5%, and absorption of sample dosage unevenness is less than 1.2; Sample irradiation is during to a half-value dose; The turn-over continued irradiation in the original place, radiation dose rate is 25Gy/min, exposure time 60 hours; To be stored in 20 ± 5 ℃, relative humidity be the indoor of 40-70% to feed behind the irradiation, finishes using in three weeks.
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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102987155A (en) * 2012-12-13 2013-03-27 青岛康大食品有限公司 Feed for SPF (Specific Pathogen Free) breeding female rabbits in non-pregnant period and preparation method thereof
CN103027203A (en) * 2012-12-13 2013-04-10 青岛康大食品有限公司 Feed for SPF male rabbit mating period and preparation method thereof
CN106615970A (en) * 2016-12-30 2017-05-10 枞阳县恒祥生态农业有限公司 Feed for promoting later egg laying performance of aged laying hen

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
刘月琴等: "《新编蛋鸡饲料配方600例》", 31 March 2009, 化学工业出版社 *
李北: "产蛋高峰后提高蛋鸡效益的措施", 《河南畜牧兽医》 *
王君华: "SPF试验动物饲料辐照灭菌的研究", 《中国优秀硕士学位论文全文数据库(电子期刊)农业科技辑》 *

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102987155A (en) * 2012-12-13 2013-03-27 青岛康大食品有限公司 Feed for SPF (Specific Pathogen Free) breeding female rabbits in non-pregnant period and preparation method thereof
CN103027203A (en) * 2012-12-13 2013-04-10 青岛康大食品有限公司 Feed for SPF male rabbit mating period and preparation method thereof
CN106615970A (en) * 2016-12-30 2017-05-10 枞阳县恒祥生态农业有限公司 Feed for promoting later egg laying performance of aged laying hen

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