CN102423286B - Natural hair dye prepared by using phytochrome curcumin and hair dyeing method of natural hair dye - Google Patents
Natural hair dye prepared by using phytochrome curcumin and hair dyeing method of natural hair dye Download PDFInfo
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- CN102423286B CN102423286B CN 201110376414 CN201110376414A CN102423286B CN 102423286 B CN102423286 B CN 102423286B CN 201110376414 CN201110376414 CN 201110376414 CN 201110376414 A CN201110376414 A CN 201110376414A CN 102423286 B CN102423286 B CN 102423286B
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Abstract
The invention relates to a hair dye, in particular to a natural hair dye prepared by using phytochrome curcumin and a hair dyeing method of the natural hair dye. The hair dye comprises an agent A and an agent B, and is characterized in that: the agent A contains 0.1 to 10 weight percent of curcumin, 20 to 50 weight percent of polyol, 1 to 5 weight percent of thickening agent, 1 to 10 weight percent of surfactant and the balance of water, and the pH value is regulated to be 3 to 7; and the agent B contains 1 to 10 weight percent of metal ion mordant, 1 to 5 weight percent of thickening agent, 1 to 10 weight percent of surfactant, 0.1 to 0.3 weight percent of natural essence and the balance of water, and the pH value is regulated to be 3 to 7. The hair dyeing method comprises the following steps of: uniformly spreading the agent A on the hair when the hair is dyed, and dyeing the hair for 10 to 40min at the temperature of between normal temperature and 60 DEG C; and uniformly spreading the agent B on the hair, mordanting for 10 to 20min, cleaning the hair and blow-drying. The curcumin has a good dyeing effect and also has the effects of resisting bacteria and protecting skin. Reagents which are toxic to human bodies are not used in the hair dye, and substances which are toxic to the human bodies are also not generated in the hair dyeing process, so the hair dye is high in safety. The adopted curcumin is insoluble in water and cannot fall off easily in the washing process, so the hair dye has a good dyeing effect, and the color of the dyed hair can be kept for a long time.
Description
Technical field
The present invention relates to a kind of hair dye, particularly a kind of oil-soluble curcumin that adopts is natural hair dye and the hair colouring methods thereof of one-component plant pigment.
Background technology
The hair dye of selling in the market mostly contains p-phenylenediamine (PPD), para-aminophenol, hydroquinone etc., and life-time service causes various diseases, such as alopecia, and skin allergy, skin carcinoma, malignant tumor etc.Along with progressively improving and the continuous progress of the science of improve looks of health of people consciousness, the hair dye that natural plant pigment prepares becomes the development trend in following hair dye market day by day.In the existing patent, the main pigment of botanical hair dye comprises Quercetin, hematoxylin, catechin etc.Having the botanical hair dye Main Problems now is, the dye-uptake of hair dye is lower, and color fastness is relatively poor.
Curcumin is a kind of chemical composition of extracting from the rhizome of zingiberaceous plant as natural pigment, and wherein, Rhizoma Curcumae Longae approximately contains 3%～6%, is the very rare pigment with diketone of plant kingdom, is cyclohexadione compounds.Curcumin is orange-yellow crystalline powder, and flavor is slightly bitter, water insoluble.Curcumin has the effects such as blood fat reducing, antitumor, antiinflammatory, function of gallbladder promoting, antioxidation.Using in hair dye of curcumin has patent report now, and Chinese patent 201010225971.8 discloses a kind of preparation method, using method that comprises the hair dye of Rhizoma Curcumae Longae and tannic acid material, and commercial packing.Chinese patent application 201110008881.8 discloses a kind of take the main effect component of Stigma Croci extract as colored hair dyeing, dyes the colour hair dyeing frost that the color matching composition combines with the plant coloured silk.Wherein said plant coloured silk dyes the color matching composition and is comprised of Fructus Rosae Laevigatae extract, acorn cup extract, Rhizoma Curcumae Longae extract, perhaps is comprised of Madder extract, Fructus Lycopersici esculenti extract and Fructus Gardeniae extract.But these all be curcumin as the color adjusting agent, and do not consider the water-fast characteristic of curcumin.
Summary of the invention
The object of the invention is to adopt oil-soluble natural pigment curcumin is the main pigment composition of hair dye, prepares a kind of new type natural botanical hair dye.This hair dye forms by two doses, and agent A contains the plant pigment curcumin, and agent B contains metal salt mordant.
According to technical scheme provided by the invention, adopt oil-soluble plant pigment curcumin to prepare a kind of novel natural hair dye and comprise agent A and agent B, it is characterized in that, agent A comprises plant pigment curcumin 0.1%-10%, polyhydric alcohol 20-50%, surfactant 1-10%, thickening agent 1-5%, all the other are water, regulate pH to 5-7; Agent B comprises and comprises metal salt mordant 1-5%, thickening agent 1-5%, and surfactant 1-10%, natural essence 0.1-0.3%, all the other are water, regulate pH to 5-7.Unit is percetage by weight.
Polyhydric alcohol among the agent A is one or more in wetting agent glycerol, butanediol, the isopropyl alcohol.
Metal salt mordant is the salt that allows any metal ion of use in the cosmetics among the agent B, includes but not limited to ferrous sulfate, ferrous chloride, iron chloride, zinc sulfate, aluminum chloride, copper nitrate.Natural essence can adopt a kind of in Flos Rosae Rugosae essence, jasmine flower essence, the lavandula angustifolia essence.
The pH of agent A mediating recipe B regulates with phosphoric acid, acetic acid, lactic acid, tartaric acid or citric acid.
Described thickening agent includes but not limited to the one or more combination in Radix Acaciae senegalis, carboxymethyl cellulose, hydroxyethyl-cellulose, guar gum, the propylene glycol stearate.
Surfactant comprises anion, cation, both sexes or the non-ionic surface active agents such as stearyl alcohol, glyceryl stearate, sodium lauryl sulfate, OPEO.
Agent A and agent B are solution or any degree thickening or the liquid that adds glue, Emulsion or cream frost form.
The hair colouring methods of the oil-soluble natural hair dye of described employing curcumin one-component plant pigment is characterized in that, during hair dyeing, at first agent B evenly is applied in hair, at room temperature to 60 ℃ lower hair dyeing 10-40min; Then agent C evenly is applied in hair, behind the mordant dyeing 10-20min, hair cleaned dries up.
The curcumin that the present invention adopts is a kind of natural pigment that extracts from the rhizome of Zingiberaceae Curcuma (Curcuma L) plant Rhizoma Curcumae Longae, Rhizoma Curcumae, Radix Curcumae etc., can cooperate with the different metal ion to form various chromatic colours.And Color is good, color fastness is stronger, has again the effects such as antibiotic skin-care.The present invention has solved the oil-soluble curcumin and has added the easily problem of floating of common hair dye to by adding polyhydric alcohol, realizes the good stability of product, thereby so that the hair dyeing of one-component plant pigment curcumin become a reality.Because the oil-soluble plant pigment is water insoluble, its wash resistant ability is obviously strengthened in addition.Therefore, this hair dye has safe and reliable, and Color is stablized lasting advantage.
The specific embodiment
Below in conjunction with embodiment technical scheme of the present invention is further described, but protection scope of the present invention is not limited to this.
Embodiment 1
Agent A: curcumin 0.7%, isopropyl alcohol 26%, carboxymethyl cellulose 1%, propylene glycol stearate 1%, glyceryl stearate 1%,, the deionized water surplus is transferred pH to 5 with phosphoric acid.
Agent B: ferrous sulfate 2%, reduced iron powder 0.2%, Polyethylene Glycol 10%, carboxymethyl cellulose 2%, stearyl alcohol 2%, the deionized water surplus, lavandula angustifolia essence 0.1% is transferred pH to 5 with phosphoric acid.
Hair colouring methods: agent A evenly is applied in hair, and then the 40min that has hair dyed at normal temperatures evenly is applied in hair with agent B, behind the mordant dyeing 10min hair is cleaned to dry up, and hair is the more shallow brownish black of nature.
Embodiment 2
Agent A: curcumin 5%, butanediol 10%, isopropyl alcohol 25%, hydroxyethyl-cellulose 1%, propylene glycol stearate 2%, ceteareth-20 1%, the deionized water surplus is transferred pH to 6 with phosphoric acid.
Agent B: ferrous sulfate 8%, reduced iron powder 0.2%, guar gum 2%, jasmine flower essence 0.3%, the deionized water surplus is transferred pH to 5 with acetic acid.
Hair colouring methods: agent A evenly is applied in hair, at 40 ℃ of lower hair dyeing 30min, then agent B evenly is applied in hair, behind the mordant dyeing 20min hair cleaned and dry up, hair is the dark brown black of nature.
Embodiment 3:
Agent A: bisdemethoxycurcumin %, glycerol 5%, isopropyl alcohol 30%, carboxyethyl cellulose 0.5%, stearyl alcohol 2%, the deionized water surplus is transferred pH to 5 with acetic acid.
Agent B: iron chloride 5%, guar gum 2%, the deionized water surplus, jasmine flower essence 0.1% is transferred pH to 3 with lactic acid.
Hair colouring methods: agent A evenly is applied in hair, and then the 40min that has hair dyed at normal temperatures evenly is applied in hair with agent B, behind the mordant dyeing 20min hair is cleaned to dry up, and hair is the hestnut color of nature.
Embodiment 4
Agent A: curcumin 2%, butanediol 10%, isopropyl alcohol 15%, carboxymethyl cellulose 1%, propylene glycol stearyl alcohol 1%, the deionization surplus is transferred pH to 6 with lactic acid.
Agent B: zinc sulfate 3.5%, Polyethylene Glycol 5%, hydroxypropyl cellulose 1.5%, rose essence 0.1%, the deionized water surplus is transferred pH to 6.5 with lactic acid.
Hair colouring methods: agent A evenly is applied in hair, at 50 ℃ of lower hair dyeing 20min, then agent B evenly is applied in hair, behind the mordant dyeing 15min hair cleaned and dry up, hair is the brown color of nature.
Embodiment 5
Agent A: curcumin 8%, isopropyl alcohol 20%, butanediol 25%, carboxymethyl cellulose 1%, stearyl alcohol 2%, the deionized water surplus is transferred pH to 5.5 with phosphoric acid.
Agent B: aluminum chloride 7%, guar gum 2%, rose essence 0.05%, the deionized water surplus is transferred pH to 3 with citric acid.
Hair colouring methods: agent A evenly is applied in hair, at 40 ℃ of lower hair dyeing 20min, then agent B evenly is applied in hair, behind the mordant dyeing 15min hair cleaned and dry up, hair is the brownish black of nature.
Claims (2)
1. adopt a kind of natural hair dye of plant pigment curcumin preparation, comprise agent A and agent B, it is characterized in that, agent A comprises curcumin 0.1%-10%, polyhydric alcohol 20-50%, and thickening agent 1-5%, surfactant 1-10% regulates pH to 3-7, Yu Weishui; Agent B comprises metal salt mordant 1-10%, thickening agent 1-5%, and surfactant 1-10%, natural essence 0.1-0.3% regulates pH to 3-7, Yu Weishui; Unit is percetage by weight;
Polyhydric alcohol among the agent A is one or both in wetting agent glycerol, the butanediol;
Metal salt mordant is one or more in the ferrous sulfate that allow to use in the cosmetics, ferrous chloride, iron chloride, zinc sulfate, aluminum chloride, the copper nitrate among the agent B;
Natural essence among the agent B is a kind of in Flos Rosae Rugosae essence, jasmine flower essence, the lavandula angustifolia essence;
The pH of agent A mediating recipe B regulates with phosphoric acid, acetic acid, lactic acid, tartaric acid or citric acid;
Thickening agent among the agent A mediating recipe B is the one or more combination in Radix Acaciae senegalis, carboxymethyl cellulose, hydroxyethyl-cellulose, guar gum, the propylene glycol stearate;
The surfactant of agent A mediating recipe B comprises stearyl alcohol, glyceryl stearate, sodium lauryl sulfate, OPEO.
2. a kind of natural hair dye of employing plant pigment curcumin preparation as claimed in claim 1 is characterized in that, described dose of A, agent B are Emulsion or cream frost form.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201110376414 CN102423286B (en) | 2011-11-24 | 2011-11-24 | Natural hair dye prepared by using phytochrome curcumin and hair dyeing method of natural hair dye |
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| CN 201110376414 CN102423286B (en) | 2011-11-24 | 2011-11-24 | Natural hair dye prepared by using phytochrome curcumin and hair dyeing method of natural hair dye |
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| CN102423286A CN102423286A (en) | 2012-04-25 |
| CN102423286B true CN102423286B (en) | 2013-03-06 |
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| CN102824283B (en) * | 2012-09-17 | 2013-07-10 | 山西大学 | Environment-friendly hair-care hair dye and preparation method thereof |
| CN102924966B (en) * | 2012-10-31 | 2014-08-13 | 常州大学 | Date peel red pigment, and preparation and application thereof |
| CN104083307B (en) * | 2014-07-28 | 2016-08-17 | 江南大学 | Use a kind of natural hair dye of preparing of plant pigment carthamin and hair colouring methods thereof |
| CN104398441B (en) * | 2014-12-08 | 2017-05-10 | 上海海洋大学 | Seaweed pigment hair dye and application method thereof |
| CN104825359A (en) * | 2015-05-06 | 2015-08-12 | 江南大学 | Method for preparing natural hair dye from black plum peels |
| CN104825360A (en) * | 2015-05-06 | 2015-08-12 | 江南大学 | Method for preparing natural hair dye from pumpkin |
| CN106309249A (en) * | 2016-10-13 | 2017-01-11 | 江南大学 | Natural hair dye prepared from plant pigment verbena hybrida haematochrome and hair dyeing method of natural hair dye |
| CN106309248A (en) * | 2016-10-13 | 2017-01-11 | 江南大学 | Natural hair dye prepared from plant pigment geranium haematochrome and hair dyeing method of natural hair dye |
| CN106420499A (en) * | 2016-11-28 | 2017-02-22 | 河南工程学院 | Natural hair dye prepared from fructus chebulae pigment and dyeing method thereof |
| JP6963206B2 (en) * | 2017-04-06 | 2021-11-05 | 株式会社ピカソ美化学研究所 | Two-agent hair dye |
| CN107789241B (en) * | 2017-09-22 | 2019-10-25 | 拉芳家化股份有限公司 | Hair film composition and preparation method thereof with hair care colour fixation |
| CN107616925A (en) * | 2017-10-11 | 2018-01-23 | 郭迎庆 | A kind of preparation method of washable hair dye |
| CN107938389A (en) * | 2017-12-28 | 2018-04-20 | 张永成 | A kind of soft solid agent of antibacterial dyed suitable for natural dye to textile |
| CN108403580A (en) * | 2018-03-30 | 2018-08-17 | 王敏 | A kind of natural plant pigment hair dye and preparation method thereof and preparation method thereof |
| CN109925205A (en) * | 2019-01-31 | 2019-06-25 | 西南大学 | Natural botanical hair dye and its application method of the compound common Chinese medicine effective component as dyestuff |
| CN113710222A (en) * | 2019-04-15 | 2021-11-26 | 联合利华知识产权控股有限公司 | Personal care compositions comprising tetramethylcurcumin and methods of making the compositions |
| CN110292536B (en) * | 2019-06-25 | 2022-07-08 | 许雅婷 | Electrochromic keratin fiber dyeing method and device |
| CN111407709A (en) * | 2020-03-27 | 2020-07-14 | 南京益唯森生物科技有限公司 | Natural hair dye adopting plant hair dye powder and preparation method thereof |
| CN112870147A (en) * | 2021-03-17 | 2021-06-01 | 浙江章华保健美发实业有限公司 | Plant type hair dyeing and perming integrated hair beautifying agent |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2838644B1 (en) * | 2002-04-23 | 2005-12-30 | Oreal | USE OF 1,7-BISPHENYL HEPTANE-3,5-DIONE DERIVATIVES AS ACTIVE INHIBITING DEVELOPMENT OF BODY ODORS IN COSMETIC COMPOSITIONS |
| US7749286B2 (en) * | 2006-05-01 | 2010-07-06 | Advanced Cosmetic Technologies, Llc | Composition for dyeing keratin fibers and a method of dyeing hair using same |
| CN101879135B (en) * | 2009-11-12 | 2013-03-06 | 北京世纪博康医药科技有限公司 | Curcuma plant hair dye |
| CN102078276B (en) * | 2011-01-17 | 2012-07-04 | 肖子英 | Saffron series of plant colorful hair dying cream |
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Application publication date: 20120425 Assignee: Yixing Xinyu Chemicals Co., Ltd. Assignor: Jiangnan University Contract record no.: 2013320010177 Denomination of invention: Natural hair dye prepared by using phytochrome curcumin and hair dyeing method of natural hair dye Granted publication date: 20130306 License type: Exclusive License Record date: 20131227 |
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Application publication date: 20120425 Assignee: Yixing Xinyu Chemicals Co., Ltd. Assignor: Jiangnan University Contract record no.: 2013320010177 Denomination of invention: Natural hair dye prepared by using phytochrome curcumin and hair dyeing method of natural hair dye Granted publication date: 20130306 License type: Exclusive License Record date: 20131227 |
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