CN102388926B - Raw material composition and preparation method of anti-retroviral, freeze-proofing and refreshing biomembrane preparation - Google Patents
Raw material composition and preparation method of anti-retroviral, freeze-proofing and refreshing biomembrane preparation Download PDFInfo
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- YYRMJZQKEFZXMX-UHFFFAOYSA-N calcium;phosphoric acid Chemical compound [Ca+2].OP(O)(O)=O.OP(O)(O)=O YYRMJZQKEFZXMX-UHFFFAOYSA-N 0.000 description 1
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Abstract
The invention relates to the raw material composition and a preparation method of an anti-retroviral, freeze-proofing and refreshing biomembrane preparation. The anti-retroviral, freeze-proofing and refreshing biomembrane preparation comprises the following raw materials in part by weight: 30 to 50 parts of oligosaccharide, 15 to 30 parts of tissuemat E, 15 to 20 parts of cellulose preparation, and 20 to 30 parts of bacteriacide, adhesive and synergist. The prepared anti-retroviral, freeze-proofing and refreshing biomembrane preparation is safe and non-toxic, and pollution-free, and has the characteristics that the preparation can prevent fruits and vegetables from being frozen and protect fruits and vegetables from retroviral, disinfect and nourish the fruits and vegetables, improve fruit setting, and protect plant to grow through the winter safely. The preparation is particularly suitable for retroviral and frostbite prevention of plants such as fruit trees, vegetables, flowers, grain, cotton, medicinal materials and the like and has durability and controllability in the aspects of preventing plants from being frozen and supplying nutrients to the plants.
Description
One, technical field:
The raw material that the present invention relates to a kind of degeneration-resistant antifreeze fresh-keeping biomembrane preparation is formed and preparation method thereof.
Two, background technology:
After China's reform and opening-up, implement the agricultural structure adjustment, greatly develop rural economy, fruits and vegetables industry, cereal crops, economic crops have become the pillar industry of China's developing agricultural.But artificial environmental influence and natural calamity take place frequently, it is the most serious to the harm of crops particularly to arrive cold spell in spring, cold in the late spring disaster phenomenon causes economic crops and the cereal crops underproduction more than 50%, has seriously influenced the enthusiasm of peasant's farming, and agricultural production is constituted deathblow.China's rare manufacturing enterprise scale and product variety all are in explores the starting stage, and does not form brand mostly, and kind is single, and product quality also is difficult to guarantee.Multi-functional, compoundization, high-quality to have antifreeze, a degeneration-resistant product of nutrition in great shortage especially, be difficult to satisfy market demand.In the information age of global technology economic integration, people advocate Green Product, but are subjected to influence and China's system present situation of economic interests, seldom have enterprise emitting bigger economic risk to participate in this industry.So product does not form scale at present.My company relies on the scientific and technological advantage of Xibei Univ. of Agricultural ﹠ Forest Science ﹠ Technology, and through Yang Ling demonstration area expert development test for many years, technology, technology, product quality are mature and stable.Assessment of result shows that this product belongs to the plant protection product of environment-friendly type.The huge market demand has a extensive future.To provide strong technical guarantee for China's agricultural safety in production.
Three, summary of the invention:
The present invention is in order to solve the weak point in the above-mentioned background technology; provide a kind of raw material of degeneration-resistant antifreeze fresh-keeping biomembrane preparation to form and preparation method thereof; its safety non-toxic, pollution-free has the characteristics of antifreeze, degeneration-resistant, sterilization, nutrition, raising percentage of fertile fruit, cover crop safety to fruits and vegetables.
For achieving the above object, the technical solution used in the present invention is: a kind of degeneration-resistant antifreeze fresh-keeping biomembrane preparation is characterized in that: described degeneration-resistant antifreeze fresh-keeping biomembrane preparation is made up of the raw material of following weight portion: oligosaccharide 30～50 weight portions, Tissuemat E 15～30 weight portions, cellulose preparation 15～20 weight portions, bactericide, adhesive and synergist 20～30 weight portions.
Described bactericide, adhesive and synergist weight ratio are 1:2.5:3.
Described oligosaccharide is raffinose, milk ketose, xylo-oligosaccharide, oligoisomaltose, oligomeric dragon gallbladder sugar or soyabean oligosaccharides.
Described cellulose preparation is cellulose, hemicellulose, polyvinyl resin or pectin.
Described bactericide is Celastrus angulatus.
Adhesive is medical stone or glauconite.
Described synergist is phytic acid.
The preparation method of described a kind of degeneration-resistant antifreeze fresh-keeping biomembrane preparation, may further comprise the steps: 1. oligosaccharide, cellulose preparation and adhesive are ground respectively, put into reactor after the grinding and carry out the heat refining hot melt, then Tissuemat E is mixed with bactericide, add 40 ℃～50 ℃ warm water and be heated to 50 ℃～78 ℃, put into reactor and its reaction 8 hours, the agitator in the described reactor revolution be 300 rev/mins, it mixed to refilter namely get standby raw material; 2. the warm water placing response still reaction that synergist is added 40 ℃～50 ℃ namely got film forming agent in 3 hours ± 13 minutes; 3. the warm water that standby raw material and film forming agent is added 40 ℃～50 ℃ is put into reactor, and reaction temperature is 40 ℃～80 ℃, and the time is to get product through grinding in 3 hours ± 13 minutes again.
Described heat refining hot melting temperature is 85 ℃, and the time is 8.5 hours.
Compared with prior art, the advantage and the effect that have of the present invention is as follows:
1, the present invention sprays about 30 seconds and namely becomes microgrid shape biomembrane naturally according to the fruit-vegetable type shape, 0.01～0.1 millimeter of its controllable thickness, the regulation and control membrane structure term of validity is 10～30 days, fructescence by plant absorbing, the decomposition that comes off naturally, environment is not caused secondary pollution, and can effectively intercept the residual pollution to fruits and vegetables of medicine, safety nuisance free, pollution-free, development green agriculture, environmental protection agricultural and the ecological balance all there are positive role.
2, the present invention has imitative biomembrane function, the moisture of preserving moisture, reduce the blade face evaporation, stop germ to enter and the insect infringement, adding amino acid etc. can be alleviated damage caused by a drought, and the drought resisting hot-dry wind tolerance reduces yellow leaf and fruit phase fallen leaves, add biomembrane and the sugar product of purifying and can play winter protection, freeze proof effect, but the aging of adding phytic acid delayed fruit.
3, product of the present invention can be separated out supply active extract, ice-nucleus, function element; stablize pistil; promote growth of young; eliminate the fruit and vegetable surfaces scab; the control fruit russeting forms; protective plant can improve, activate crop autoimmunity and disease resistance effectively, and diseases such as fruits and vegetables little leaf, yellowtop, rot are had tangible control efficiency.
4, the present invention can urge bud, protect leaf, protect flower, short fruit, precocious volume increase improves quality, the fill light photograph heats fruits and vegetables, promotes evenly paintedly, enlarges stained area, maintenance fruits and vegetables lovely luster is pure, can make the pulp exquisiteness, sugar is moderate, fruity is natural aromatic.
5, the present invention can be used for the plant physiology protection of multiple fruits and vegetables such as multiple fruit such as apple, pears, oranges and tangerines, banana, grape and tomato, cucumber, eggplant and pistil, bud, tender leaf, has vast market prospect.
6, the present invention is particularly useful for crops such as fruit tree, vegetables, flowers, grain, cotton, medicinal material to the protection against cold and freezing conditions of cold in the late spring, plant degeneration-resistant antifreeze and the supply nutrient have persistence and controllability.
Four, embodiment:
A kind of degeneration-resistant antifreeze fresh-keeping biomembrane preparation, described degeneration-resistant antifreeze fresh-keeping biomembrane preparation is made up of the raw material of following weight portion: oligosaccharide 30～50 weight portions, Tissuemat E 15～30 weight portions, cellulose preparation 15～20 weight portions, bactericide, adhesive and synergist 20～30 weight portions.
Described bactericide, adhesive and synergist weight ratio are 1:2.5:3.
Described oligosaccharide is raffinose, milk ketose, xylo-oligosaccharide, oligoisomaltose, oligomeric dragon gallbladder sugar or soyabean oligosaccharides.
Described cellulose preparation is cellulose, hemicellulose, polyvinyl resin or pectin.
Described bactericide is Celastrus angulatus.
Adhesive is medical stone or glauconite.
Described synergist is phytic acid.
A kind of preparation method of degeneration-resistant antifreeze fresh-keeping biomembrane preparation, may further comprise the steps: 1. oligosaccharide, cellulose preparation and adhesive are ground respectively, put into reactor after the grinding and carry out the heat refining hot melt, described heat refining hot melting temperature is 85 ℃, time is 8.5 hours, then Tissuemat E is mixed with bactericide, add 40 ℃～50 ℃ warm water and be heated to 50 ℃～78 ℃, put into reactor and its reaction 8 hours, agitator in the described reactor revolution be 300 rev/mins, it mixed to refilter namely get standby raw material; 2. the warm water placing response still reaction that synergist is added 40 ℃～50 ℃ namely got film forming agent in 3 hours ± 13 minutes; 3. the warm water that standby raw material and film forming agent is added 40 ℃～50 ℃ is put into reactor, and reaction temperature is 40 ℃～80 ℃, and the time is to get product through grinding in 3 hours ± 13 minutes again.
Embodiment 1:
A kind of degeneration-resistant antifreeze fresh-keeping biomembrane preparation, described degeneration-resistant antifreeze fresh-keeping biomembrane preparation is made up of the raw material of following weight portion: raffinose 30 weight portions, Tissuemat E 15 weight portions, hemicellulose 15 weight portions, Celastrus angulatus 4 weight portions, medical stone 10 weight portions and phytic acid 12 weight portions;
A kind of preparation method of degeneration-resistant antifreeze fresh-keeping biomembrane preparation, may further comprise the steps: 1. raffinose, hemicellulose and medical stone are ground respectively, put into reactor after the grinding and carry out the heat refining hot melt, described heat refining hot melting temperature is 85 ℃, time is 8.5 hours, then Tissuemat E is mixed with Celastrus angulatus, add 40 ℃ warm water and be heated to 50 ℃, put into reactor and its reaction 8 hours, agitator in the described reactor revolution be 300 rev/mins, it mixed to refilter namely get standby raw material; 2. the warm water placing response still reaction that phytic acid is added 40 ℃～50 ℃ namely got film forming agent in 3 hours ± 13 minutes; 3. the warm water that standby raw material and film forming agent is added 40 ℃～50 ℃ is put into reactor, and reaction temperature is 40 ℃～80 ℃, and the time is to get product through grinding in 3 hours ± 13 minutes again.
Embodiment 2:
A kind of degeneration-resistant antifreeze fresh-keeping biomembrane preparation, described degeneration-resistant antifreeze fresh-keeping biomembrane preparation is made up of the raw material of following weight portion: milk ketose 50 weight portions, Tissuemat E 30 weight portions, polyvinyl resin 20 weight portions, Celastrus angulatus 3.5 weight portions, glauconite 8.75 weight portions and phytic acid 10.5 weight portions.
A kind of preparation method of degeneration-resistant antifreeze fresh-keeping biomembrane preparation, may further comprise the steps: 1. milk ketose, polyvinyl resin and glauconite are ground respectively, put into reactor after the grinding and carry out the heat refining hot melt, described heat refining hot melting temperature is 85 ℃, time is 8.5 hours, then Tissuemat E is mixed with Celastrus angulatus, add 50 ℃ warm water and be heated to 78 ℃, put into reactor and its reaction 8 hours, agitator in the described reactor revolution be 300 rev/mins, it mixed to refilter namely get standby raw material; 2. the warm water placing response still reaction that phytic acid is added 50 ℃ namely got film forming agent in 3 hours ± 13 minutes; 3. the warm water that standby raw material and film forming agent is added 50 ℃ is put into reactor, and reaction temperature is 80 ℃, and the time is to get product through grinding in 3 hours ± 13 minutes again.
Embodiment 3:
A kind of degeneration-resistant antifreeze fresh-keeping biomembrane preparation is characterized in that: described degeneration-resistant antifreeze fresh-keeping biomembrane preparation is made up of the raw material of following weight portion: soyabean oligosaccharides 40 weight portions, Tissuemat E 25 weight portions, pectin 18 weight portions, Celastrus angulatus 4.2 weight portions, glauconite 10.5 weight portions and phytic acid 12.6 weight portions.
A kind of preparation method of degeneration-resistant antifreeze fresh-keeping biomembrane preparation, may further comprise the steps: 1. soyabean oligosaccharides, pectin and glauconite are ground respectively, put into reactor after the grinding and carry out the heat refining hot melt, described heat refining hot melting temperature is 85 ℃, time is 8.5 hours, then Tissuemat E is mixed with Celastrus angulatus, add 45 ℃ warm water and be heated to 68 ℃, put into reactor and its reaction 8 hours, agitator in the described reactor revolution be 300 rev/mins, it mixed to refilter namely get standby raw material; 2. the warm water placing response still reaction that phytic acid is added 46 ℃ namely got film forming agent in 3 hours ± 13 minutes; 3. the warm water that standby raw material and film forming agent is added 48 ℃ is put into reactor, and reaction temperature is 70 ℃, and the time is to get product through grinding in 3 hours ± 13 minutes again.
The test example(according to embodiment 1)
:
1, test objective
According to the field fertilizer efficiency technical regulation that formulate at clay fertilizer station, Shaanxi Province, determine the application effect of degeneration-resistant antifreeze fresh-keeping biomembrane preparation on cucumber that Yang Ling China shafts biotechnology Co., Ltd produces.
2, test material
Cucumber variety is the close thorn in Heilungkiang, and all are handled mu and execute degeneration-resistant antifreeze fresh-keeping biomembrane preparation 2000kg, and test site is in the cucumber ground of Qindu District fishing platform town Ba Li village Zhang Haichuan, handles mu and executes degeneration-resistant antifreeze fresh-keeping biomembrane preparation 150kg.Contrast mu base is executed urea 33kg, superphosphate (16%) 75kg, potassium sulphate 14.3kg, disposable applying after field planting.For trying the main nutrition table with test results of soil such as following table 1:
3, test method
3.2: demonstration test design and application process
Two processing are established in this test, and executing degeneration-resistant antifreeze fresh-keeping biomembrane preparation is the demonstration area, and 5 mu of areas, conventional fertilizer application are the check plot, and 1 mu of area adopts the duplicate rows plant apart from 30cm, wide line-spacing 85cm.Narrow row is apart from 35cm, and plantation density is 3400 strain/mus.
3.3: data determination method and statistical analysis
After the cucumber field planting, observe record in good time.Biology symptoms such as the plant height, stem of investigating cucumber the full bearing period is thick, leaf area, setting number, receipts phase beginning statistics is respectively handled output, the difference of aspects such as analysing output, single fruit weight, measured result is carried out significance test of difference.
4, test results and analysis
4.1: the influence that different disposal is grown to cucumber plant
Degeneration-resistant antifreeze fresh-keeping biomembrane preparation can promote growing of cucumber plant.By table 2 as seen, use degeneration-resistant antifreeze fresh-keeping biomembrane preparation after, plant height, stem are thick, leaf area, percentage of fertile fruit all have raising in various degree, percentage of fertile fruit has increased by 18.4% respectively.This shows that degeneration-resistant antifreeze fresh-keeping biomembrane preparation can improve cucumber rhizosphere nutrition condition and growing environment, increase plant nutrient supply, promoted the absorption of crop to nutritive element, thereby improved the resistance of crop, for the output that improves cucumber is laid a good foundation.
Table 2: the influence that degeneration-resistant antifreeze fresh-keeping biomembrane preparation grows to cucumber plant
| Handle | Plant height cm | The thick cm of stem | Percentage of fertile fruit % | Leaf area (10 strain) cm 2 |
| T | 178.5 | 0.90 | 86.4 | 298.7 |
| CK | 162.3 | 0.73 | 68.0 | 270.4 |
4.2: different disposal is to the influence of cucumber yield
Degeneration-resistant antifreeze fresh-keeping biomembrane preparation can significantly improve cucumber yield, and receipts phase beginning of cucumber has shifted to an earlier date 3 days than contrast, use degeneration-resistant antifreeze fresh-keeping biomembrane preparation after output obviously increase.Increased by 13.7% than contrast, the increase of output mainly is indicated as the increase of single fruit weight.The processing of having used fertilizer compared with the control simultaneously, the quantity of female flower is more, and individual plant melon number also increases to some extent.
Table 3: different disposal is to the influence of cucumber yield and picking time
| Handle | Receipts phase beginning (day/month) | The heavy g of single melon | Individual plant melon number (individual) | Per mu yield kg |
| T | 10//5 | 174 | 14.2 | 7788.3 |
| CK | 15/5 | 166 | 11.8 | 6849.5 |
4.3: different disposal is to the influence of cucumber resistance
As can be seen from Table 4, behind the application of organic fertilizers, diseased fruit rate, the leaf incidence of disease, drought are frozen dead plant rate and are decreased, percentage of fertile fruit then is increase trend, wherein diseased fruit rate reduces by 45.4% than contrast, and this may improve the nutrient environment of root system of plant because degeneration-resistant antifreeze fresh-keeping biomembrane preparation improves soil physical, thereby make plant be easy to absorb nutrient, thereby improved the resistance of crop.
Table 4: degeneration-resistant antifreeze fresh-keeping biomembrane preparation is to the influence of cucumber resistance
| Handle | Change melon rate % | Downy mildew incidence of disease % | Diseased fruit rate % | The cold dead plant rate that freezes |
| T | 15.3 | 7.3 | 9.7 | 2.7 |
| CK | 18.7 | 12.3 | 5.3 | 5.4 |
4.4: the different disposal input-output ratio is analyzed
As can be seen from Table 5, after degeneration-resistant antifreeze fresh-keeping biomembrane preparation is used, can improve utilization rate of fertilizer, balanced nutritious, robust plant, resistance increase, disease reduces, reduced the production cost of cucumber, simultaneously height product rate height, the output height of cucumber, agricultural dish revenue growth.
4.5 use degeneration-resistant antifreeze fresh-keeping biomembrane preparation to the influence of cucumber yield
Table 7 pairing design experiment result statistics
Degree of freedom n-1=5-1=4, table look-up t
0.05=2.776, t
0.01=4.604, because of t=5.37〉t
0.01=4.604 demonstration areas and check plot level error heteropole are remarkable, illustrate that degeneration-resistant antifreeze fresh-keeping biomembrane preparation has effect extremely significantly.
3, result and discussion
Degeneration-resistant antifreeze fresh-keeping biomembrane preparation has the utilization rate of fertilizer of raising, reduces fertilizer amount, increases soil porosity, improves the granular structure of soil, increases income antifreezing adverse-resistant, the transportation of promotion nutrition in the plant body of crop, improves the effect of plant strain growth.
Degeneration-resistant antifreeze fresh-keeping biomembrane preparation has the cucumber of raising percentage of fertile fruit, improves the cucumber single fruit weight, increases output, improves the effect of the commodity rate of cucumber, thereby reaches the purpose of increasing both production and income.
Claims (7)
1. degeneration-resistant antifreeze fresh-keeping biomembrane preparation, it is characterized in that: described degeneration-resistant antifreeze fresh-keeping biomembrane preparation is made up of the raw material of following weight portion: oligosaccharide 30～50 weight portions, Tissuemat E 15～30 weight portions, cellulose preparation 15～20 weight portions, bactericide, adhesive and synergist 20～30 weight portions;
Described bactericide is Celastrus angulatus;
Described synergist is phytic acid.
2. a kind of degeneration-resistant antifreeze fresh-keeping biomembrane preparation according to claim 1, it is characterized in that: described bactericide, adhesive and synergist weight ratio are 1:2.5:3.
3. a kind of degeneration-resistant antifreeze fresh-keeping biomembrane preparation according to claim 1, it is characterized in that: described oligosaccharide is raffinose, milk ketose, xylo-oligosaccharide, oligoisomaltose, oligomeric dragon gallbladder sugar or soyabean oligosaccharides.
4. a kind of degeneration-resistant antifreeze fresh-keeping biomembrane preparation according to claim 1, it is characterized in that: described cellulose preparation is cellulose, hemicellulose, polyvinyl resin or pectin.
5. a kind of degeneration-resistant antifreeze fresh-keeping biomembrane preparation according to claim 1, it is characterized in that: adhesive is medical stone or glauconite.
6. the preparation method of a kind of degeneration-resistant antifreeze fresh-keeping biomembrane preparation according to claim 1, its special being: may further comprise the steps: 1. oligosaccharide, cellulose preparation and adhesive are ground respectively, put into reactor after the grinding and carry out the heat refining hot melt, then Tissuemat E is mixed with bactericide, add 40 ℃～50 ℃ warm water and be heated to 50 ℃～78 ℃, put into reactor and its reaction 8 hours, agitator in the described reactor revolution be 300 rev/mins, it mixed to refilter namely get standby raw material; 2. the warm water placing response still reaction that synergist is added 40 ℃～50 ℃ namely got film forming agent in 3 hours ± 13 minutes; 3. the warm water that standby raw material and film forming agent is added 40 ℃～50 ℃ is put into reactor, and reaction temperature is 40 ℃～80 ℃, and the time is to get product through grinding in 3 hours ± 13 minutes again.
7. the preparation method of a kind of degeneration-resistant antifreeze fresh-keeping biomembrane preparation according to claim 6, its special being: described heat refining hot melting temperature is 85 ℃, the time is 8.5 hours.
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| CN105340893B (en) * | 2015-12-10 | 2017-07-14 | 沈阳化工研究院有限公司 | A kind of agricultural degeneration-resistant composition and its preparation method and application |
| CN105325466B (en) * | 2015-12-10 | 2018-02-06 | 沈阳化工研究院有限公司 | A kind of composition for inducing plant disease-resistant and coordinate plant growth, and its preparation method and application |
| CN106614821A (en) * | 2016-12-16 | 2017-05-10 | 四川金牌农业发展有限公司 | Anti-freezing agent for crops |
| CN107410462A (en) * | 2017-04-09 | 2017-12-01 | 湖南易科生物工程有限公司 | A kind of compound method of leaf vegetables antistaling agent |
| CN107467035A (en) * | 2017-07-13 | 2017-12-15 | 句容市龙山茶场（普通合伙） | A kind of tea tree antifreezing agent and preparation method thereof |
| CN115886005B (en) * | 2023-01-04 | 2024-05-14 | 青岛农业大学 | Plant antifreeze agent containing quercetin and raffinose as well as preparation method and application thereof |
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