CN102329165B - Preparation method of biological fertilizer additive - Google Patents
Preparation method of biological fertilizer additive Download PDFInfo
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- CN102329165B CN102329165B CN 201110179941 CN201110179941A CN102329165B CN 102329165 B CN102329165 B CN 102329165B CN 201110179941 CN201110179941 CN 201110179941 CN 201110179941 A CN201110179941 A CN 201110179941A CN 102329165 B CN102329165 B CN 102329165B
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Abstract
The invention discloses a preparation method of a biological fertilizer additive, relating to the technical fields of biomedicine and nano material application. The preparation method comprises the following process flow steps: A, preparing raw materials; B, preparing natural saccharide nano microspheres; C, preparing an antimicrobial active solution; and D, preparing the biological fertilizer additive. The biological fertilizer additive has the characteristics of high efficiency and low toxicity, is beneficial to improvement of a surrounding environment of a plant, is capable of timely supplying nutrients required by plant growth, and the like. The biological fertilizer additive coordinated with other fertilizers can be used for rice, fruit and economic crop, can be used as a basic fertilizer, an additional fertilizer and a leaf surface fertilizer.
Description
Technical field
The present invention relates to biological medicine and technical field of nano material application, particularly a kind of preparation method of bio-feritlizer additive.
Background technology
Agriculture production is as the source of food, and in growing process, the incorrect use of material is dropped in the outside, and the food-safety problem that causes is serious day by day and outstanding, the health and lives of its direct harm humans.Only from provand chain source, agricultural-food are subjected to agricultural chemicals, pollution by chemical fertilizer to some extent in planting process.China is large agricultural country, and more than 20 hundred million mu of crop seeding areas, the rate of fertilizer in per hectare soil are 2 times, 2.4 times of the U.S. of Japan, and 1.4 hundred million tons of year chemical fertilizer applications occupy first place in the world.Excessive use chemical fertilizer and agricultural chemicals cause soil compaction, soil fertility to descend, and utilization rate of fertilizer is low, simultaneously, make disease and pest aggravate, and cause objectionable impurities to deposit in plant.Human body is by the long-term edible vegetables that are subjected to agricultural chemicals, pollution by chemical fertilizer, residual objectionable impurities is accumulated certain limit by food in human body after, can cause some chronic diseases to take place, as cancer, arteriosclerosis, cardiovascular diseases, fetal anomaly, stillborn foetus, early die young, disease such as early ageing.Chinese patent (application number is 02117548.9) " multifunctional additive of fertilizer " mainly is made up of microbial biomass nitrogen, humic acids, poly aspartic acid, xylogen and mineral clay; This additive mixes the back by a certain percentage to be used with chemical fertilizer of simple substance, compound fertilizer, organic fertilizer, microbial fertilizer, organic and inorganic fertilizer, can improve chemical fertilizer utilization ratio, increases fertilizer efficiency, prolongs the fertile phase, and can improve the quick-acting of organic fertilizer microbial fertilizer.And for example Chinese patent (application number is 01118050.1) " multifunctional additive of fertilizer " mainly is made up of microbial biomass nitrogen, humic acids, sepiolite, attapulgite, zeolite.This additive by a certain percentage with compound fertilizer, fertilizer or bio-fertilizer mixing granulation, not only can reduce fertilizer amount, reduce production costs, but also can improve nitrogen utilization efficiency and fertilizer efficiency.
Summary of the invention
Technical problem to be solved by this invention provides a kind of high-effect, hypotoxicity, is conducive to improve the plant surrounding enviroment, and in time supplies with the preparation method of the bio-feritlizer additive of the required nutrient of plant-growth.
The technical solution used in the present invention is the preparation method of a kind of bio-feritlizer additive of invention, and its technological process is as follows:
A, weight share take by weighing antibacterial substance 10-25 part, organic fertilizer 3-8 part, tensio-active agent 1-5 part and micro-1-3 part, and be standby;
B, with the natural sugar hydrolysis of 1.5 parts of weight quota in the distilled water of 60 parts of weight quota, treat that hydrolyzed solution is chilled to room temperature after, add the linking agent Aum-35 of 0.03 part of weight quota, with the rotating speed stirring reaction of 800r/min 2 hours, make the natural sugar Nano microsphere, as carrier, standby;
C, above-mentioned standby antibacterial substance is dissolved in the solvent that 3-5 doubly measures, adds standby natural sugar Nano microsphere again, add standby tensio-active agent simultaneously, stirred at normal temperatures 2-8 hour, make anti-microbial activity solution, standby;
D, in standby anti-microbial activity solution, add standby organic fertilizer and trace element, namely get the bio-feritlizer additive;
The technological process of its optimisation technique scheme one is as follows:
A, weight share take by weighing antibacterial substance 15-21 part, organic fertilizer 4-6 part, tensio-active agent 2-3.75 part and micro-1.5-2 part, and be standby;
B, with the natural sugar hydrolysis of 1.5 parts of weight quota in the distilled water of 60 parts of weight quota, treat that hydrolyzed solution is chilled to room temperature after, add the linking agent Aum-35 of 0.03 part of weight quota, with the rotating speed stirring reaction of 800r/min 2 hours, make the natural sugar Nano microsphere, as carrier, standby;
C, above-mentioned standby antibacterial substance is dissolved in the solvent that 3-5 doubly measures, adds standby natural sugar Nano microsphere again, add standby tensio-active agent simultaneously, stirred at normal temperatures 2-8 hour, make anti-microbial activity solution, standby;
D, in standby anti-microbial activity solution, add standby organic fertilizer and trace element, namely get the bio-feritlizer additive.
The technological process of its optimisation technique scheme two is as follows:
A, weight share take by weighing 1.5 parts of 15 parts of antibacterial substances, 6 parts in organic fertilizer, 3.75 parts in tensio-active agent and trace elements, and be standby;
B, with the natural sugar hydrolysis of 1.5 parts of weight quota in the distilled water of 60 parts of weight quota, treat that hydrolyzed solution is chilled to room temperature after, add the linking agent Aum-35 of 0.03 part of weight quota, with the rotating speed stirring reaction of 800r/min 2 hours, make the natural sugar Nano microsphere, as carrier, standby;
C, above-mentioned standby antibacterial substance is dissolved in the solvent that 3-5 doubly measures, adds standby natural sugar Nano microsphere again, add standby tensio-active agent simultaneously, stirred at normal temperatures 2-8 hour, make anti-microbial activity solution, standby;
D, in standby anti-microbial activity solution, add standby organic fertilizer and trace element, namely get the bio-feritlizer additive.
The technological process of its optimisation technique scheme three is as follows:
A, weight share take by weighing 1.5 parts of 15 parts of antibacterial substances, 4 parts in organic fertilizer, 2 parts in tensio-active agent and trace elements, and be standby;
B, with the natural sugar hydrolysis of 1.5 parts of weight quota in the distilled water of 60 parts of weight quota, treat that hydrolyzed solution is chilled to room temperature after, add the linking agent Aum-35 of 0.03 part of weight quota, with the rotating speed stirring reaction of 800r/min 2 hours, make the natural sugar Nano microsphere, as carrier, standby;
C, above-mentioned standby antibacterial substance is dissolved in the solvent that 3-5 doubly measures, adds standby natural sugar Nano microsphere again, add standby tensio-active agent simultaneously, stirred at normal temperatures 2-8 hour, make anti-microbial activity solution, standby;
D, in standby anti-microbial activity solution, add standby organic fertilizer and trace element, namely get the bio-feritlizer additive.
The technological process of its optimisation technique scheme four is as follows:
A, weight share take by weighing 2 parts of 21 parts of antibacterial substances, 6 parts in organic fertilizer, 3 parts in tensio-active agent and trace elements, and be standby;
B, with the natural sugar hydrolysis of 1.5 parts of weight quota in the distilled water of 60 parts of weight quota, treat that hydrolyzed solution is chilled to room temperature after, add the linking agent Aum-35 of 0.03 part of weight quota, with the rotating speed stirring reaction of 800r/min 2 hours, make the natural sugar Nano microsphere, as carrier, standby;
C, above-mentioned standby antibacterial substance is dissolved in the solvent that 3-5 doubly measures, adds standby natural sugar Nano microsphere again, add standby tensio-active agent simultaneously, stirred at normal temperatures 2-8 hour, make anti-microbial activity solution, standby;
D, in standby anti-microbial activity solution, add standby organic fertilizer and trace element, namely get the bio-feritlizer additive.
Antibacterial substance described in above-mentioned each scheme is one or both in tea saponin, the bamfolin; When being two kinds, the ratio of tea saponin and bamfolin is 2-4: 1;
Organic fertilizer described in above-mentioned each scheme is that to contain N, P, K total amount be 90% organic fertilizer, and wherein: the ratio of N, P, K is 1: 1.5: 1.5;
Tensio-active agent described in above-mentioned each scheme is that in alkylphenol polyoxyethylene series, gum arabic, sulfonate series, vitriol series, the series of phosphate one or both are multiple or whole, and when being two kinds and when two or more, its consumption is equal portions;
Trace element described in above-mentioned each scheme is the vitriol that contains Fe, Zn, Ca ion, and three's consumption is equal portions;
Natural sugar described in above-mentioned each scheme is glucose, also can adopt fructose or sucrose or other carbohydrate;
Solvent described in above-mentioned each scheme is water or organic solvent (as: methyl alcohol, ethanol, ethyl acetate etc.).
In above-mentioned each scheme, used weight quota unit can be gram or kilogram or ton, also can be other weight metering unit.
The preparation method of bio-feritlizer additive of the present invention, the main nanometer technology of preparing that adopts, natural antibacterial active substance tea saponin and bamfolin are converted into the material that is beneficial to plant absorbing, utilization, and be equipped with other nutritive ingredient, thereby, can not only improve plant growth environment, can also supply with the required nutrient of plant-growth in time, effectively, promote plant to other nutrient absorbing, improve the usefulness of fertilizer.Simultaneously, N, P, the K fertilizer of institute's adapted are organic fertilizer, so toxicity is lower.
Use the bio-feritlizer additive that the present invention produces, its effect is very remarkable, showed in ground such as Hunan Province's Yongzhou City Dongan County, Lengshuitan District, Jiang Hua county tests in 2010, the bio-feritlizer additive that uses the present invention to produce, good absorption, instant effect, the growing way of various farm crop is vigorous, fruit quality is good, and resistibility obviously increases.As tobacco on average increase production 20%, oranges and tangerines on average increase production 10%, vegetables on average increase production 12%, other crops are also on average increased production between 20%, and the crop disease-resistant ability obviously improves.
Embodiment
Below in conjunction with embodiment, the preparation method of bio-feritlizer additive of the present invention is further described.Following explanation is the mode that exemplifies, but protection scope of the present invention is not limited thereto.
Embodiment one:
The preparation method of the bio-feritlizer additive of present embodiment, its technological process is as follows:
A, take by weighing tea saponin 15 gram, organic fertilizer 6 grams, sodium alkyl benzene sulfonate 3.75 grams and trace element 1.5 grams, standby;
B, with glucose 1.5 gram, hydrolysis in the distilled water of 60 grams (that is: 60ml), treat that hydrolyzed solution is chilled to room temperature after, add the linking agent Aum-35 of 0.03 gram, with the rotating speed stirring reaction of 800r/min 2 hours, make the glucose Nano microsphere, as carrier, standby;
C, standby 15 gram tea saponins are dissolved in 75 ml waters, add standby glucose Nano microsphere again, add standby sodium alkyl benzene sulfonate simultaneously, stirred at normal temperatures 5 hours, make anti-microbial activity solution (that is: nanometer tea saponin solution), standby;
D, in above-mentioned standby nanometer tea saponin solution, add standby organic fertilizer and trace element, namely get the bio-feritlizer additive (that is: nanometer tea saponin bio-feritlizer additive) that contains the nanometer tea saponin.
Embodiment two:
The preparation method of the bio-feritlizer additive of present embodiment, its technological process is as follows:
A, take by weighing bamfolin 15 gram, organic fertilizer 4 grams, alkylphenol polyoxyethylene phosphoric acid ester 2 grams and trace element 1.5 grams, standby;
B, with glucose 1.5 gram, hydrolysis in the distilled water of 60 grams (that is: 60ml), treat that hydrolyzed solution is chilled to room temperature after, add the linking agent Aum-35 of 0.03 gram, with the rotating speed stirring reaction of 800r/min 2 hours, make the glucose Nano microsphere, as carrier, standby;
C, standby 15 gram bamfolins are dissolved in the 48 gram straight alcohols, add standby glucose Nano microsphere again, add standby alkylphenol polyoxyethylene phosphoric acid ester simultaneously, stirred at normal temperatures 5 hours, make anti-microbial activity solution (that is: nanometer bamfolin solution), standby;
D, in above-mentioned standby nanometer bamfolin solution, add standby organic fertilizer and trace element, namely get the bio-feritlizer additive (that is: nanometer bamfolin bio-feritlizer additive) that contains the nanometer bamfolin.
Embodiment three:
The preparation method of the bio-feritlizer additive of present embodiment, its technological process is as follows:
A, take by weighing tea saponin 14 gram, bamfolin 7 grams, organic fertilizer 6 grams, alkylphenol polyoxyethylene phosphoric acid ester 3 grams and trace element 2 grams, standby;
B, with glucose 1.5 gram, hydrolysis in the distilled water of 60 grams (that is: 60ml), treat that hydrolyzed solution is chilled to room temperature after, add the linking agent Aum-35 of 0.03 gram, with the rotating speed stirring reaction of 800r/min 2 hours, make the glucose Nano microsphere, as carrier, standby;
C, tea saponin 14 gram and bamfolin 7 grams are dissolved in the ethanol of 90 grams 50%, add standby glucose Nano microsphere again, add standby alkylphenol polyoxyethylene phosphoric acid ester simultaneously, stirred at normal temperatures 5 hours, make anti-microbial activity solution (that is: nanometer tea saponin and bamfolin solution), standby;
D, in above-mentioned standby nanometer tea saponin and bamfolin solution, add standby organic fertilizer and trace element, namely get the bio-feritlizer additive (that is: nanometer tea saponin and bamfolin bio-feritlizer additive) that contains nanometer tea saponin and bamfolin.
Use the bio-feritlizer additive that the present invention produces, be used with other fertilizer, both can be used for paddy rice, also can be used for fruit, also can be used for cash crop; Both can be used as base manure, and also can be used as and topdress, also can be used as foliage fertilizer.During as base manure, its addition is 10-15%; Be used as when topdressing, its addition is 20-30%; During as foliage fertilizer, its addition is 30-45%.
Claims (5)
1. the preparation method of a bio-feritlizer additive is characterized in that technological process is as follows:
A, weight share take by weighing antibacterial substance 10-25 part, organic fertilizer 3-8 part, tensio-active agent 1-5 part and micro-1-3 part, and be standby;
B, with the natural sugar hydrolysis of 1.5 parts of weight quota in the distilled water of 60 parts of weight quota, treat that hydrolyzed solution is chilled to room temperature after, add the linking agent Aum-35 of 0.03 part of weight quota, with the rotating speed stirring reaction of 800r/min 2 hours, make the natural sugar Nano microsphere, as carrier, standby;
C, above-mentioned standby antibacterial substance is dissolved in the solvent that 3-5 doubly measures, adds standby natural sugar Nano microsphere again, add standby tensio-active agent simultaneously, stirred at normal temperatures 2-8 hour, make anti-microbial activity solution, standby;
D, in standby anti-microbial activity solution, add standby organic fertilizer and trace element, namely get the bio-feritlizer additive.
2. the preparation method of bio-feritlizer additive according to claim 1 is characterized in that technological process is as follows:
A, weight share take by weighing antibacterial substance 15-21 part, organic fertilizer 4-6 part, tensio-active agent 2-3.75 part and micro-1.5-2 part, and be standby;
B, with the natural sugar hydrolysis of 1.5 parts of weight quota in the distilled water of 60 parts of weight quota, treat that hydrolyzed solution is chilled to room temperature after, add the linking agent Aum-35 of 0.03 part of weight quota, with the rotating speed stirring reaction of 800r/min 2 hours, make the natural sugar Nano microsphere, as carrier, standby;
C, above-mentioned standby antibacterial substance is dissolved in the solvent that 3-5 doubly measures, adds standby natural sugar Nano microsphere again, add standby tensio-active agent simultaneously, stirred at normal temperatures 2-8 hour, make anti-microbial activity solution, standby;
D, in standby anti-microbial activity solution, add standby organic fertilizer and trace element, namely get the bio-feritlizer additive.
3. the preparation method of bio-feritlizer additive according to claim 1 and 2 is characterized in that technological process is as follows:
A, weight share take by weighing 1.5 parts of 15 parts of antibacterial substances, 6 parts in organic fertilizer, 3.75 parts in tensio-active agent and trace elements, and be standby;
B, with the natural sugar hydrolysis of 1.5 parts of weight quota in the distilled water of 60 parts of weight quota, treat that hydrolyzed solution is chilled to room temperature after, add the linking agent Aum-35 of 0.03 part of weight quota, with the rotating speed stirring reaction of 800r/min 2 hours, make the natural sugar Nano microsphere, as carrier, standby;
C, above-mentioned standby antibacterial substance is dissolved in the solvent that 3-5 doubly measures, adds standby natural sugar Nano microsphere again, add standby tensio-active agent simultaneously, stirred at normal temperatures 2-8 hour, make anti-microbial activity solution, standby;
D, in standby anti-microbial activity solution, add standby organic fertilizer and trace element, namely get the bio-feritlizer additive.
4. the preparation method of bio-feritlizer additive according to claim 1 and 2 is characterized in that technological process is as follows:
A, weight share take by weighing 1.5 parts of 15 parts of antibacterial substances, 4 parts in organic fertilizer, 2 parts in tensio-active agent and trace elements, and be standby;
B, with the natural sugar hydrolysis of 1.5 parts of weight quota in the distilled water of 60 parts of weight quota, treat that hydrolyzed solution is chilled to room temperature after, add the linking agent Aum-35 of 0.03 part of weight quota, with the rotating speed stirring reaction of 800r/min 2 hours, make the natural sugar Nano microsphere, as carrier, standby;
C, above-mentioned standby antibacterial substance is dissolved in the solvent that 3-5 doubly measures, adds standby natural sugar Nano microsphere again, add standby tensio-active agent simultaneously, stirred at normal temperatures 2-8 hour, make anti-microbial activity solution, standby;
D, in standby anti-microbial activity solution, add standby organic fertilizer and trace element, namely get the bio-feritlizer additive.
5. the preparation method of bio-feritlizer additive according to claim 1 and 2 is characterized in that technological process is as follows:
A, weight share take by weighing 2 parts of 21 parts of antibacterial substances, 6 parts in organic fertilizer, 3 parts in tensio-active agent and trace elements, and be standby;
B, with the natural sugar hydrolysis of 1.5 parts of weight quota in the distilled water of 60 parts of weight quota, treat that hydrolyzed solution is chilled to room temperature after, add the linking agent Aum-35 of 0.03 part of weight quota, with the rotating speed stirring reaction of 800r/min 2 hours, make the natural sugar Nano microsphere, as carrier, standby;
C, above-mentioned standby antibacterial substance is dissolved in the solvent that 3-5 doubly measures, adds standby natural sugar Nano microsphere again, add standby tensio-active agent simultaneously, stirred at normal temperatures 2-8 hour, make anti-microbial activity solution, standby;
D, in standby anti-microbial activity solution, add standby organic fertilizer and trace element, namely get the bio-feritlizer additive.
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| CN 201110179941 CN102329165B (en) | 2011-06-24 | 2011-06-24 | Preparation method of biological fertilizer additive |
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| CN 201110179941 CN102329165B (en) | 2011-06-24 | 2011-06-24 | Preparation method of biological fertilizer additive |
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| CN102329165B true CN102329165B (en) | 2013-07-10 |
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Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104446999A (en) * | 2014-12-04 | 2015-03-25 | 柳州华晟科技有限公司 | Preparation method of rice fertilizer additive |
| CN104447004A (en) * | 2014-12-04 | 2015-03-25 | 柳州华晟科技有限公司 | Rice fertilizer additive |
| CN104529618A (en) * | 2014-12-09 | 2015-04-22 | 张亮 | Preparation method for fertilizer additive of hilly tea trees |
| CN104496663A (en) * | 2014-12-09 | 2015-04-08 | 张亮 | Additive for fertilizer of mountain camellia sinensis |
| CN106748037A (en) * | 2016-12-04 | 2017-05-31 | 钦州市星火计划办公室 | A kind of rice biological fertilizer and preparation method thereof |
| CN113875464A (en) * | 2021-09-27 | 2022-01-04 | 广西绿循环新材料技术有限责任公司 | Method for biologically preventing and treating aniseed anthracnose by combining nano antibacterial agent |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1454879A (en) * | 2002-04-29 | 2003-11-12 | 么向和 | Multifunctional fertilizer additive |
| CN1590528A (en) * | 2003-08-29 | 2005-03-09 | 郭伟光 | Multieffect microbiological active liquid and its production technology |
| CN101591206A (en) * | 2009-05-27 | 2009-12-02 | 江西百叶神生态科技有限公司 | A kind of biological liquid fertilizer and preparation method thereof |
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1454879A (en) * | 2002-04-29 | 2003-11-12 | 么向和 | Multifunctional fertilizer additive |
| CN1590528A (en) * | 2003-08-29 | 2005-03-09 | 郭伟光 | Multieffect microbiological active liquid and its production technology |
| CN101591206A (en) * | 2009-05-27 | 2009-12-02 | 江西百叶神生态科技有限公司 | A kind of biological liquid fertilizer and preparation method thereof |
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