CN102206865A - 一种利用蓝晶石矿制备莫来石晶须的方法 - Google Patents
一种利用蓝晶石矿制备莫来石晶须的方法 Download PDFInfo
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- CN102206865A CN102206865A CN 201110117635 CN201110117635A CN102206865A CN 102206865 A CN102206865 A CN 102206865A CN 201110117635 CN201110117635 CN 201110117635 CN 201110117635 A CN201110117635 A CN 201110117635A CN 102206865 A CN102206865 A CN 102206865A
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- Prior art keywords
- crystal whisker
- mullite crystal
- ore
- cyanite
- blue
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- KZHJGOXRZJKJNY-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Si]=O.O=[Al]O[Al]=O.O=[Al]O[Al]=O.O=[Al]O[Al]=O KZHJGOXRZJKJNY-UHFFFAOYSA-N 0.000 title claims abstract description 49
- 229910052863 mullite Inorganic materials 0.000 title claims abstract description 49
- 238000000034 method Methods 0.000 title claims abstract description 16
- 238000001354 calcination Methods 0.000 claims abstract description 25
- 238000000498 ball milling Methods 0.000 claims abstract description 19
- 239000000126 substance Substances 0.000 claims abstract description 19
- 239000000203 mixture Substances 0.000 claims abstract description 12
- 239000000463 material Substances 0.000 claims abstract description 11
- 238000001816 cooling Methods 0.000 claims abstract description 3
- 239000013078 crystal Substances 0.000 claims description 43
- 229910052782 aluminium Inorganic materials 0.000 claims description 17
- KLZUFWVZNOTSEM-UHFFFAOYSA-K Aluminum fluoride Inorganic materials F[Al](F)F KLZUFWVZNOTSEM-UHFFFAOYSA-K 0.000 claims description 7
- IRPGOXJVTQTAAN-UHFFFAOYSA-N 2,2,3,3,3-pentafluoropropanal Chemical compound FC(F)(F)C(F)(F)C=O IRPGOXJVTQTAAN-UHFFFAOYSA-N 0.000 claims description 5
- 238000002156 mixing Methods 0.000 claims description 5
- 229910052500 inorganic mineral Inorganic materials 0.000 claims description 4
- 239000011707 mineral Substances 0.000 claims description 4
- 150000008064 anhydrides Chemical class 0.000 claims description 2
- OYLGJCQECKOTOL-UHFFFAOYSA-L barium fluoride Chemical compound [F-].[F-].[Ba+2] OYLGJCQECKOTOL-UHFFFAOYSA-L 0.000 claims description 2
- 229910001632 barium fluoride Inorganic materials 0.000 claims description 2
- 239000000470 constituent Substances 0.000 claims description 2
- 235000019239 indanthrene blue RS Nutrition 0.000 claims description 2
- UHOKSCJSTAHBSO-UHFFFAOYSA-N indanthrone blue Chemical compound C1=CC=C2C(=O)C3=CC=C4NC5=C6C(=O)C7=CC=CC=C7C(=O)C6=CC=C5NC4=C3C(=O)C2=C1 UHOKSCJSTAHBSO-UHFFFAOYSA-N 0.000 claims description 2
- NROKBHXJSPEDAR-UHFFFAOYSA-M potassium fluoride Chemical compound [F-].[K+] NROKBHXJSPEDAR-UHFFFAOYSA-M 0.000 claims description 2
- 239000002994 raw material Substances 0.000 abstract description 7
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 abstract 2
- INJRKJPEYSAMPD-UHFFFAOYSA-N aluminum;silicic acid;hydrate Chemical compound O.[Al].[Al].O[Si](O)(O)O INJRKJPEYSAMPD-UHFFFAOYSA-N 0.000 description 39
- 239000010443 kyanite Substances 0.000 description 39
- 229910052850 kyanite Inorganic materials 0.000 description 39
- 239000012141 concentrate Substances 0.000 description 27
- 239000004615 ingredient Substances 0.000 description 15
- 229910010413 TiO 2 Inorganic materials 0.000 description 13
- 229910052700 potassium Inorganic materials 0.000 description 13
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 12
- 238000005516 engineering process Methods 0.000 description 9
- 238000002360 preparation method Methods 0.000 description 8
- 229910016569 AlF 3 Inorganic materials 0.000 description 6
- 229910016036 BaF 2 Inorganic materials 0.000 description 4
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 description 4
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 3
- 238000004458 analytical method Methods 0.000 description 3
- BNGXYYYYKUGPPF-UHFFFAOYSA-M (3-methylphenyl)methyl-triphenylphosphanium;chloride Chemical compound [Cl-].CC1=CC=CC(C[P+](C=2C=CC=CC=2)(C=2C=CC=CC=2)C=2C=CC=CC=2)=C1 BNGXYYYYKUGPPF-UHFFFAOYSA-M 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- 230000000996 additive effect Effects 0.000 description 2
- 230000036571 hydration Effects 0.000 description 2
- 238000006703 hydration reaction Methods 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 description 2
- 229910052622 kaolinite Inorganic materials 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 239000002243 precursor Substances 0.000 description 2
- 229910052710 silicon Inorganic materials 0.000 description 2
- 239000011863 silicon-based powder Substances 0.000 description 2
- 238000003980 solgel method Methods 0.000 description 2
- 238000002441 X-ray diffraction Methods 0.000 description 1
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 1
- 238000010306 acid treatment Methods 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000005188 flotation Methods 0.000 description 1
- 238000000713 high-energy ball milling Methods 0.000 description 1
- 238000003837 high-temperature calcination Methods 0.000 description 1
- 239000003317 industrial substance Substances 0.000 description 1
- 239000010453 quartz Substances 0.000 description 1
- 230000002787 reinforcement Effects 0.000 description 1
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Images
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- Crystals, And After-Treatments Of Crystals (AREA)
Abstract
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CN2011101176356A CN102206865B (zh) | 2011-05-09 | 2011-05-09 | 一种利用蓝晶石矿制备莫来石晶须的方法 |
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CN2011101176356A CN102206865B (zh) | 2011-05-09 | 2011-05-09 | 一种利用蓝晶石矿制备莫来石晶须的方法 |
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CN102206865A true CN102206865A (zh) | 2011-10-05 |
CN102206865B CN102206865B (zh) | 2012-11-14 |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103074686A (zh) * | 2013-02-01 | 2013-05-01 | 河北联合大学 | 蓝晶石精矿低温制备高纯莫来石单晶的方法 |
CN108298974A (zh) * | 2018-03-28 | 2018-07-20 | 许水仙 | 一种可微波加热骨质瓷的制备方法 |
CN108315810A (zh) * | 2018-02-24 | 2018-07-24 | 陕西大秦钾业有限公司 | 一种以钾霞石为原料合成莫来石晶须的方法 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1785893A (zh) * | 2005-10-18 | 2006-06-14 | 山东大学 | 一种莫来石晶须的制备方法 |
US20080095690A1 (en) * | 2006-10-24 | 2008-04-24 | Wei Liu | Nano-sized needle crystal mullite film and method of making |
CN101498049A (zh) * | 2009-01-21 | 2009-08-05 | 景德镇陶瓷学院 | 一种非水解溶胶-凝胶工艺制备莫来石晶须的方法 |
-
2011
- 2011-05-09 CN CN2011101176356A patent/CN102206865B/zh active Active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1785893A (zh) * | 2005-10-18 | 2006-06-14 | 山东大学 | 一种莫来石晶须的制备方法 |
US20080095690A1 (en) * | 2006-10-24 | 2008-04-24 | Wei Liu | Nano-sized needle crystal mullite film and method of making |
CN101498049A (zh) * | 2009-01-21 | 2009-08-05 | 景德镇陶瓷学院 | 一种非水解溶胶-凝胶工艺制备莫来石晶须的方法 |
Non-Patent Citations (2)
Title |
---|
《中国优秀硕士学位论文全文数据库(电子期刊)》 20021231 邓纲 干熄焦用莫来石材料组成结构及性能研究 , 第2期 * |
《北京科技大学学报》 20000228 倪文等 蓝晶石在不同环境中分解行为 第22卷, 第1期 * |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103074686A (zh) * | 2013-02-01 | 2013-05-01 | 河北联合大学 | 蓝晶石精矿低温制备高纯莫来石单晶的方法 |
CN103074686B (zh) * | 2013-02-01 | 2015-05-27 | 河北联合大学 | 蓝晶石精矿低温制备高纯莫来石单晶的方法 |
CN108315810A (zh) * | 2018-02-24 | 2018-07-24 | 陕西大秦钾业有限公司 | 一种以钾霞石为原料合成莫来石晶须的方法 |
CN108298974A (zh) * | 2018-03-28 | 2018-07-20 | 许水仙 | 一种可微波加热骨质瓷的制备方法 |
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CN102206865B (zh) | 2012-11-14 |
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