CN102181006A - 水性氯乙烯/异丁基乙烯基醚共聚物分散液的制备方法 - Google Patents
水性氯乙烯/异丁基乙烯基醚共聚物分散液的制备方法 Download PDFInfo
- Publication number
- CN102181006A CN102181006A CN 201110071986 CN201110071986A CN102181006A CN 102181006 A CN102181006 A CN 102181006A CN 201110071986 CN201110071986 CN 201110071986 CN 201110071986 A CN201110071986 A CN 201110071986A CN 102181006 A CN102181006 A CN 102181006A
- Authority
- CN
- China
- Prior art keywords
- vinylchlorid
- monomer
- ive
- water
- dispersion
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- BZHJMEDXRYGGRV-UHFFFAOYSA-N Vinyl chloride Chemical group ClC=C BZHJMEDXRYGGRV-UHFFFAOYSA-N 0.000 title claims abstract description 95
- 229920001577 copolymer Polymers 0.000 title claims abstract description 61
- 239000006185 dispersion Substances 0.000 title claims abstract description 60
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 48
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- 239000000178 monomer Substances 0.000 claims abstract description 84
- OZCMOJQQLBXBKI-UHFFFAOYSA-N 1-ethenoxy-2-methylpropane Chemical compound CC(C)COC=C OZCMOJQQLBXBKI-UHFFFAOYSA-N 0.000 claims abstract description 37
- 238000006116 polymerization reaction Methods 0.000 claims abstract description 28
- -1 acrylic hydroxyalkyl ester Chemical class 0.000 claims abstract description 23
- 150000001732 carboxylic acid derivatives Chemical class 0.000 claims abstract description 15
- 239000003999 initiator Substances 0.000 claims abstract description 14
- 150000001412 amines Chemical class 0.000 claims abstract description 12
- 238000006386 neutralization reaction Methods 0.000 claims abstract description 12
- 239000002994 raw material Substances 0.000 claims abstract description 4
- 239000007788 liquid Substances 0.000 claims description 27
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 claims description 22
- GETQZCLCWQTVFV-UHFFFAOYSA-N trimethylamine Chemical compound CN(C)C GETQZCLCWQTVFV-UHFFFAOYSA-N 0.000 claims description 18
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 claims description 14
- 239000003795 chemical substances by application Substances 0.000 claims description 13
- 239000008367 deionised water Substances 0.000 claims description 13
- 229910021641 deionized water Inorganic materials 0.000 claims description 13
- 238000006392 deoxygenation reaction Methods 0.000 claims description 13
- 238000009775 high-speed stirring Methods 0.000 claims description 13
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 claims description 13
- 229920002554 vinyl polymer Polymers 0.000 claims description 13
- ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 claims description 12
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 10
- LVHBHZANLOWSRM-UHFFFAOYSA-N itaconic acid Chemical compound OC(=O)CC(=C)C(O)=O LVHBHZANLOWSRM-UHFFFAOYSA-N 0.000 claims description 10
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 claims description 10
- VLCAYQIMSMPEBW-UHFFFAOYSA-N methyl 3-hydroxy-2-methylidenebutanoate Chemical compound COC(=O)C(=C)C(C)O VLCAYQIMSMPEBW-UHFFFAOYSA-N 0.000 claims description 9
- 230000003472 neutralizing effect Effects 0.000 claims description 9
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 claims description 7
- BEQKKZICTDFVMG-UHFFFAOYSA-N 1,2,3,4,6-pentaoxepane-5,7-dione Chemical compound O=C1OOOOC(=O)O1 BEQKKZICTDFVMG-UHFFFAOYSA-N 0.000 claims description 5
- ZMARGGQEAJXRFP-UHFFFAOYSA-N 1-hydroxypropan-2-yl 2-methylprop-2-enoate Chemical compound OCC(C)OC(=O)C(C)=C ZMARGGQEAJXRFP-UHFFFAOYSA-N 0.000 claims description 5
- UEEJHVSXFDXPFK-UHFFFAOYSA-N N-dimethylaminoethanol Chemical compound CN(C)CCO UEEJHVSXFDXPFK-UHFFFAOYSA-N 0.000 claims description 5
- 229960002887 deanol Drugs 0.000 claims description 5
- 239000012972 dimethylethanolamine Substances 0.000 claims description 5
- VVWRJUBEIPHGQF-UHFFFAOYSA-N propan-2-yl n-propan-2-yloxycarbonyliminocarbamate Chemical compound CC(C)OC(=O)N=NC(=O)OC(C)C VVWRJUBEIPHGQF-UHFFFAOYSA-N 0.000 claims description 5
- WSLDOOZREJYCGB-UHFFFAOYSA-N 1,2-Dichloroethane Chemical compound ClCCCl WSLDOOZREJYCGB-UHFFFAOYSA-N 0.000 claims description 4
- WYGWHHGCAGTUCH-UHFFFAOYSA-N 2-[(2-cyano-4-methylpentan-2-yl)diazenyl]-2,4-dimethylpentanenitrile Chemical compound CC(C)CC(C)(C#N)N=NC(C)(C#N)CC(C)C WYGWHHGCAGTUCH-UHFFFAOYSA-N 0.000 claims description 4
- BFSVOASYOCHEOV-UHFFFAOYSA-N 2-diethylaminoethanol Chemical compound CCN(CC)CCO BFSVOASYOCHEOV-UHFFFAOYSA-N 0.000 claims description 4
- OMIGHNLMNHATMP-UHFFFAOYSA-N 2-hydroxyethyl prop-2-enoate Chemical compound OCCOC(=O)C=C OMIGHNLMNHATMP-UHFFFAOYSA-N 0.000 claims description 4
- GWZMWHWAWHPNHN-UHFFFAOYSA-N 2-hydroxypropyl prop-2-enoate Chemical compound CC(O)COC(=O)C=C GWZMWHWAWHPNHN-UHFFFAOYSA-N 0.000 claims description 4
- 239000004342 Benzoyl peroxide Substances 0.000 claims description 4
- OMPJBNCRMGITSC-UHFFFAOYSA-N Benzoylperoxide Chemical compound C=1C=CC=CC=1C(=O)OOC(=O)C1=CC=CC=C1 OMPJBNCRMGITSC-UHFFFAOYSA-N 0.000 claims description 4
- YIVJZNGAASQVEM-UHFFFAOYSA-N Lauroyl peroxide Chemical compound CCCCCCCCCCCC(=O)OOC(=O)CCCCCCCCCCC YIVJZNGAASQVEM-UHFFFAOYSA-N 0.000 claims description 4
- 235000019400 benzoyl peroxide Nutrition 0.000 claims description 4
- 238000005502 peroxidation Methods 0.000 claims description 4
- BWJUFXUULUEGMA-UHFFFAOYSA-N propan-2-yl propan-2-yloxycarbonyloxy carbonate Chemical compound CC(C)OC(=O)OOC(=O)OC(C)C BWJUFXUULUEGMA-UHFFFAOYSA-N 0.000 claims description 4
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims description 3
- 238000013019 agitation Methods 0.000 claims description 3
- 238000010438 heat treatment Methods 0.000 claims description 3
- 238000000034 method Methods 0.000 claims description 3
- 230000008569 process Effects 0.000 claims description 3
- 238000012545 processing Methods 0.000 claims description 3
- 238000012360 testing method Methods 0.000 claims description 3
- REYKZNSVWAIXEG-UHFFFAOYSA-N 2-ethenoxy-4-methylpentane Chemical compound CC(C)CC(C)OC=C REYKZNSVWAIXEG-UHFFFAOYSA-N 0.000 claims description 2
- 239000003960 organic solvent Substances 0.000 abstract description 10
- 238000000576 coating method Methods 0.000 abstract description 9
- 239000011248 coating agent Substances 0.000 abstract description 8
- 239000012855 volatile organic compound Substances 0.000 abstract description 8
- 239000000853 adhesive Substances 0.000 abstract description 2
- 230000001070 adhesive effect Effects 0.000 abstract description 2
- 239000008346 aqueous phase Substances 0.000 abstract 1
- 230000007613 environmental effect Effects 0.000 abstract 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 abstract 1
- 238000003756 stirring Methods 0.000 description 21
- 229920005989 resin Polymers 0.000 description 20
- 239000011347 resin Substances 0.000 description 20
- 238000010792 warming Methods 0.000 description 20
- 239000004721 Polyphenylene oxide Substances 0.000 description 15
- 229920000570 polyether Polymers 0.000 description 15
- NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical compound OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 10
- 238000001816 cooling Methods 0.000 description 10
- 238000004821 distillation Methods 0.000 description 10
- 239000000203 mixture Substances 0.000 description 10
- 238000007789 sealing Methods 0.000 description 10
- 239000002904 solvent Substances 0.000 description 9
- 238000005516 engineering process Methods 0.000 description 8
- 238000007334 copolymerization reaction Methods 0.000 description 6
- 238000007639 printing Methods 0.000 description 6
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 4
- 238000004513 sizing Methods 0.000 description 4
- 150000002148 esters Chemical class 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 230000009257 reactivity Effects 0.000 description 3
- 239000004593 Epoxy Substances 0.000 description 2
- JOYRKODLDBILNP-UHFFFAOYSA-N Ethyl urethane Chemical compound CCOC(N)=O JOYRKODLDBILNP-UHFFFAOYSA-N 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 229920006026 co-polymeric resin Polymers 0.000 description 2
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- RWNUSVWFHDHRCJ-UHFFFAOYSA-N 1-butoxypropan-2-ol Chemical compound CCCCOCC(C)O RWNUSVWFHDHRCJ-UHFFFAOYSA-N 0.000 description 1
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 description 1
- 239000004925 Acrylic resin Substances 0.000 description 1
- 229920000178 Acrylic resin Polymers 0.000 description 1
- OTMSDBZUPAUEDD-UHFFFAOYSA-N Ethane Chemical class CC OTMSDBZUPAUEDD-UHFFFAOYSA-N 0.000 description 1
- CERQOIWHTDAKMF-UHFFFAOYSA-M Methacrylate Chemical compound CC(=C)C([O-])=O CERQOIWHTDAKMF-UHFFFAOYSA-M 0.000 description 1
- VVQNEPGJFQJSBK-UHFFFAOYSA-N Methyl methacrylate Chemical compound COC(=O)C(C)=C VVQNEPGJFQJSBK-UHFFFAOYSA-N 0.000 description 1
- 102100036203 Microfibrillar-associated protein 5 Human genes 0.000 description 1
- 101710147471 Microfibrillar-associated protein 5 Proteins 0.000 description 1
- 239000004902 Softening Agent Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 150000001336 alkenes Chemical class 0.000 description 1
- 229920003180 amino resin Polymers 0.000 description 1
- 150000004945 aromatic hydrocarbons Chemical class 0.000 description 1
- CQEYYJKEWSMYFG-UHFFFAOYSA-N butyl acrylate Chemical compound CCCCOC(=O)C=C CQEYYJKEWSMYFG-UHFFFAOYSA-N 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 125000001309 chloro group Chemical group Cl* 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000005553 drilling Methods 0.000 description 1
- 238000007720 emulsion polymerization reaction Methods 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 238000010528 free radical solution polymerization reaction Methods 0.000 description 1
- FPYJFEHAWHCUMM-UHFFFAOYSA-N maleic anhydride Chemical compound O=C1OC(=O)C=C1 FPYJFEHAWHCUMM-UHFFFAOYSA-N 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 1
- 150000003254 radicals Chemical class 0.000 description 1
- 229920005604 random copolymer Polymers 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000010557 suspension polymerization reaction Methods 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
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- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
Abstract
Description
Claims (6)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201110071986 CN102181006B (zh) | 2011-03-24 | 2011-03-24 | 水性氯乙烯/异丁基乙烯基醚共聚物分散液的制备方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201110071986 CN102181006B (zh) | 2011-03-24 | 2011-03-24 | 水性氯乙烯/异丁基乙烯基醚共聚物分散液的制备方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102181006A true CN102181006A (zh) | 2011-09-14 |
| CN102181006B CN102181006B (zh) | 2013-07-03 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 201110071986 Active CN102181006B (zh) | 2011-03-24 | 2011-03-24 | 水性氯乙烯/异丁基乙烯基醚共聚物分散液的制备方法 |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102181006B (zh) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102492077A (zh) * | 2011-11-14 | 2012-06-13 | 江苏利思德化工有限公司 | 改性氯醚树脂制备方法 |
| CN107602751A (zh) * | 2017-09-08 | 2018-01-19 | 北京化工大学 | 一种低分子量含羟基氯醚树脂及其制备方法 |
| CN108359043A (zh) * | 2018-01-10 | 2018-08-03 | 江苏利思德新材料有限公司 | 一种水性氯乙烯共聚树脂的制备方法 |
| CN111205410A (zh) * | 2020-01-10 | 2020-05-29 | 江苏利思德新材料有限公司 | 一种丙烯酸酯改性氯乙烯-异丁基乙烯基醚共聚物乳液及其制备方法和应用 |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0073282A1 (en) * | 1981-09-02 | 1983-03-09 | Tenneco Polymers, Inc. | Conductive moulding compositions comprising vinyl chloride-vinyl ether copolymers |
| JPS61207418A (ja) * | 1985-03-12 | 1986-09-13 | Nippon Zeon Co Ltd | プラスチゾル混和用樹脂の製造法 |
| CN101161693A (zh) * | 2007-11-19 | 2008-04-16 | 上海氯碱化工股份有限公司 | 制备氯醚树脂的方法 |
| CN101580569A (zh) * | 2009-06-22 | 2009-11-18 | 中国海洋石油总公司 | 化学改性氯醚树脂及其防腐蚀涂料 |
| CN101812154A (zh) * | 2009-10-19 | 2010-08-25 | 杭州电化集团有限公司 | 氯乙烯-异丁基乙烯基醚-丙烯酸环氧丙酯共聚树脂及制备方法 |
-
2011
- 2011-03-24 CN CN 201110071986 patent/CN102181006B/zh active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0073282A1 (en) * | 1981-09-02 | 1983-03-09 | Tenneco Polymers, Inc. | Conductive moulding compositions comprising vinyl chloride-vinyl ether copolymers |
| JPS61207418A (ja) * | 1985-03-12 | 1986-09-13 | Nippon Zeon Co Ltd | プラスチゾル混和用樹脂の製造法 |
| CN101161693A (zh) * | 2007-11-19 | 2008-04-16 | 上海氯碱化工股份有限公司 | 制备氯醚树脂的方法 |
| CN101580569A (zh) * | 2009-06-22 | 2009-11-18 | 中国海洋石油总公司 | 化学改性氯醚树脂及其防腐蚀涂料 |
| CN101812154A (zh) * | 2009-10-19 | 2010-08-25 | 杭州电化集团有限公司 | 氯乙烯-异丁基乙烯基醚-丙烯酸环氧丙酯共聚树脂及制备方法 |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102492077A (zh) * | 2011-11-14 | 2012-06-13 | 江苏利思德化工有限公司 | 改性氯醚树脂制备方法 |
| CN107602751A (zh) * | 2017-09-08 | 2018-01-19 | 北京化工大学 | 一种低分子量含羟基氯醚树脂及其制备方法 |
| CN108359043A (zh) * | 2018-01-10 | 2018-08-03 | 江苏利思德新材料有限公司 | 一种水性氯乙烯共聚树脂的制备方法 |
| CN111205410A (zh) * | 2020-01-10 | 2020-05-29 | 江苏利思德新材料有限公司 | 一种丙烯酸酯改性氯乙烯-异丁基乙烯基醚共聚物乳液及其制备方法和应用 |
| CN111205410B (zh) * | 2020-01-10 | 2022-03-15 | 江苏利思德新材料有限公司 | 一种丙烯酸酯改性氯乙烯-异丁基乙烯基醚共聚物乳液及其制备方法和应用 |
Also Published As
| Publication number | Publication date |
|---|---|
| CN102181006B (zh) | 2013-07-03 |
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Denomination of invention: Preparation method of water-based chloroethylene/isobutyl vinyl ether copolymer dispersion Effective date of registration: 20171207 Granted publication date: 20130703 Pledgee: Taizhou Guoxin Company limited by guarantee Pledgor: Jiangsu Liside New Material Co.,Ltd. Registration number: 2017990001125 |
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