CN102093528B - 一种混合型聚醚-聚酯聚氨酯/环氧阻尼复合材料制备方法 - Google Patents
一种混合型聚醚-聚酯聚氨酯/环氧阻尼复合材料制备方法 Download PDFInfo
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- CN102093528B CN102093528B CN 201110000234 CN201110000234A CN102093528B CN 102093528 B CN102093528 B CN 102093528B CN 201110000234 CN201110000234 CN 201110000234 CN 201110000234 A CN201110000234 A CN 201110000234A CN 102093528 B CN102093528 B CN 102093528B
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- Prior art keywords
- polyether
- polyester
- epoxy
- preparation
- polyurethane
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 229920000728 polyester Polymers 0.000 title claims abstract description 60
- 239000004814 polyurethane Substances 0.000 title claims abstract description 49
- 229920002635 polyurethane Polymers 0.000 title claims abstract description 47
- 239000004593 Epoxy Substances 0.000 title claims abstract description 41
- 238000013016 damping Methods 0.000 title claims abstract description 38
- 238000002360 preparation method Methods 0.000 title claims abstract description 28
- 239000002131 composite material Substances 0.000 title claims abstract description 27
- 229920000570 polyether Polymers 0.000 claims abstract description 46
- 229920000642 polymer Polymers 0.000 claims abstract description 43
- 239000004721 Polyphenylene oxide Substances 0.000 claims abstract description 22
- 229920005906 polyester polyol Polymers 0.000 claims abstract description 16
- 239000004970 Chain extender Substances 0.000 claims abstract description 10
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 32
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims description 17
- 229920001451 polypropylene glycol Polymers 0.000 claims description 9
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 8
- UPMLOUAZCHDJJD-UHFFFAOYSA-N 4,4'-Diphenylmethane Diisocyanate Chemical compound C1=CC(N=C=O)=CC=C1CC1=CC=C(N=C=O)C=C1 UPMLOUAZCHDJJD-UHFFFAOYSA-N 0.000 claims description 7
- 238000000034 method Methods 0.000 claims description 7
- DVKJHBMWWAPEIU-UHFFFAOYSA-N toluene 2,4-diisocyanate Chemical compound CC1=CC=C(N=C=O)C=C1N=C=O DVKJHBMWWAPEIU-UHFFFAOYSA-N 0.000 claims description 7
- -1 polyethylene terephthalate Polymers 0.000 claims description 6
- 229920005989 resin Polymers 0.000 claims description 5
- 239000011347 resin Substances 0.000 claims description 5
- 150000002009 diols Chemical class 0.000 claims description 3
- 229920000139 polyethylene terephthalate Polymers 0.000 claims description 3
- 239000005020 polyethylene terephthalate Substances 0.000 claims description 3
- 229920000909 polytetrahydrofuran Polymers 0.000 claims description 3
- 150000002118 epoxides Chemical class 0.000 claims 1
- 239000000463 material Substances 0.000 abstract description 18
- 229920001730 Moisture cure polyurethane Polymers 0.000 abstract description 6
- 239000003822 epoxy resin Substances 0.000 abstract description 3
- 238000002156 mixing Methods 0.000 abstract description 3
- 229920000647 polyepoxide Polymers 0.000 abstract description 3
- 238000005516 engineering process Methods 0.000 abstract description 2
- 239000012567 medical material Substances 0.000 abstract description 2
- 150000003077 polyols Chemical class 0.000 abstract description 2
- 229920005749 polyurethane resin Polymers 0.000 abstract description 2
- 239000003566 sealing material Substances 0.000 abstract description 2
- 125000005442 diisocyanate group Chemical group 0.000 abstract 2
- 238000004132 cross linking Methods 0.000 abstract 1
- 239000013013 elastic material Substances 0.000 abstract 1
- 238000011031 large-scale manufacturing process Methods 0.000 abstract 1
- 229920005862 polyol Polymers 0.000 abstract 1
- 150000002924 oxiranes Chemical class 0.000 description 23
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 20
- 238000006243 chemical reaction Methods 0.000 description 14
- 229910052757 nitrogen Inorganic materials 0.000 description 10
- 239000011159 matrix material Substances 0.000 description 9
- 230000018044 dehydration Effects 0.000 description 8
- 238000006297 dehydration reaction Methods 0.000 description 8
- 238000003756 stirring Methods 0.000 description 8
- 238000001035 drying Methods 0.000 description 6
- 238000010438 heat treatment Methods 0.000 description 6
- 239000000203 mixture Substances 0.000 description 6
- IBOFVQJTBBUKMU-UHFFFAOYSA-N 4,4'-methylene-bis-(2-chloroaniline) Chemical compound C1=C(Cl)C(N)=CC=C1CC1=CC=C(N)C(Cl)=C1 IBOFVQJTBBUKMU-UHFFFAOYSA-N 0.000 description 5
- JOYRKODLDBILNP-UHFFFAOYSA-N Ethyl urethane Chemical compound CCOC(N)=O JOYRKODLDBILNP-UHFFFAOYSA-N 0.000 description 5
- 241001112258 Moca Species 0.000 description 5
- 150000002148 esters Chemical class 0.000 description 4
- 238000007731 hot pressing Methods 0.000 description 4
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 4
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 239000001361 adipic acid Substances 0.000 description 2
- 238000005266 casting Methods 0.000 description 2
- 229920001577 copolymer Polymers 0.000 description 2
- 238000002425 crystallisation Methods 0.000 description 2
- 230000008025 crystallization Effects 0.000 description 2
- 229920001971 elastomer Polymers 0.000 description 2
- 239000000806 elastomer Substances 0.000 description 2
- 230000032050 esterification Effects 0.000 description 2
- 238000005886 esterification reaction Methods 0.000 description 2
- 239000012948 isocyanate Substances 0.000 description 2
- 150000002513 isocyanates Chemical group 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 description 2
- 239000012858 resilient material Substances 0.000 description 2
- KXDHJXZQYSOELW-UHFFFAOYSA-M Carbamate Chemical group NC([O-])=O KXDHJXZQYSOELW-UHFFFAOYSA-M 0.000 description 1
- XFXPMWWXUTWYJX-UHFFFAOYSA-N Cyanide Chemical compound N#[C-] XFXPMWWXUTWYJX-UHFFFAOYSA-N 0.000 description 1
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 1
- 239000005977 Ethylene Substances 0.000 description 1
- GOOHAUXETOMSMM-UHFFFAOYSA-N Propylene oxide Chemical compound CC1CO1 GOOHAUXETOMSMM-UHFFFAOYSA-N 0.000 description 1
- 239000003082 abrasive agent Substances 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 125000002947 alkylene group Chemical group 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229920001400 block copolymer Polymers 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 150000002334 glycols Chemical class 0.000 description 1
- 150000002605 large molecules Chemical group 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Natural products C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 1
- 230000000176 photostabilization Effects 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 238000004513 sizing Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 150000005846 sugar alcohols Polymers 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 229920002725 thermoplastic elastomer Polymers 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Images
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- Polyurethanes Or Polyureas (AREA)
- Vibration Prevention Devices (AREA)
Abstract
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CN 201110000234 CN102093528B (zh) | 2011-01-04 | 2011-01-04 | 一种混合型聚醚-聚酯聚氨酯/环氧阻尼复合材料制备方法 |
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CN 201110000234 CN102093528B (zh) | 2011-01-04 | 2011-01-04 | 一种混合型聚醚-聚酯聚氨酯/环氧阻尼复合材料制备方法 |
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CN102093528A CN102093528A (zh) | 2011-06-15 |
CN102093528B true CN102093528B (zh) | 2013-04-03 |
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CN 201110000234 Expired - Fee Related CN102093528B (zh) | 2011-01-04 | 2011-01-04 | 一种混合型聚醚-聚酯聚氨酯/环氧阻尼复合材料制备方法 |
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Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
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CN102391638B (zh) * | 2011-07-21 | 2013-02-27 | 江苏扬州合力橡胶制品有限公司 | 一种高阻尼结构件组合物、加工方法及包含该结构件的隔震橡胶支座 |
CN103013421B (zh) * | 2012-12-06 | 2014-04-16 | 常熟国和新材料有限公司 | 一种无溶剂聚氨酯复合胶及其制备方法 |
CN104937003B (zh) * | 2013-01-25 | 2019-05-10 | 汉高股份有限及两合公司 | 包含可持续生产的原料的湿气固化聚氨酯组合物 |
CN105062042B (zh) * | 2015-07-17 | 2018-03-30 | 沈阳化工大学 | 一种混合型聚氨酯压电阻尼材料及其制备方法 |
CN106397706B (zh) * | 2015-07-30 | 2019-05-03 | 株洲时代新材料科技股份有限公司 | 高硬度环氧改性聚氨酯复合材料及其制备方法 |
CN116199855B (zh) * | 2023-05-06 | 2023-07-18 | 成都瑞吉龙科技有限责任公司 | 一种聚醚-聚酯混合型聚氨酯及其制备方法 |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5194502A (en) * | 1990-11-20 | 1993-03-16 | Sunstar Giken Kabushiki Kaisha | Epoxy resin, urethane-modified epoxy resin and carboxylated polyester |
CN101193975A (zh) * | 2005-06-09 | 2008-06-04 | 株式会社艾迪科 | 固化性树脂组合物 |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
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JPS6067525A (ja) * | 1983-09-22 | 1985-04-17 | Dainippon Ink & Chem Inc | 成形用弾性樹脂 |
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2011
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Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5194502A (en) * | 1990-11-20 | 1993-03-16 | Sunstar Giken Kabushiki Kaisha | Epoxy resin, urethane-modified epoxy resin and carboxylated polyester |
CN101193975A (zh) * | 2005-06-09 | 2008-06-04 | 株式会社艾迪科 | 固化性树脂组合物 |
Non-Patent Citations (1)
Title |
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JP昭60-67525A 1985.04.17 |
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CN102093528A (zh) | 2011-06-15 |
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Effective date of registration: 20170714 Address after: 110021 No. 47-2 Shen Liaodong Road, Tiexi District, Liaoning, Shenyang 3031 Patentee after: Chen Erfan Address before: 110142 Shenyang economic and Technological Development Zone, Liaoning, No. 11 Patentee before: Shenyang University of Chemical Technology |
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Effective date of registration: 20170804 Address after: 110021 No. 47-2 Shen Liaodong Road, Tiexi District, Liaoning, Shenyang 3031 Patentee after: Shenyang macromolecule macromolecule research and Development Center Co.,Ltd. Address before: 110021 No. 47-2 Shen Liaodong Road, Tiexi District, Liaoning, Shenyang 3031 Patentee before: Chen Erfan |
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Effective date of registration: 20170906 Address after: 110021 No. 47-2 Shen Liaodong Road, Tiexi District, Liaoning, Shenyang 3031 Patentee after: SHENYANG HUADA R & D CENTER OF POLYMER MATERIALS Co.,Ltd. Address before: 110021 No. 47-2 Shen Liaodong Road, Tiexi District, Liaoning, Shenyang 3031 Patentee before: Chen Erfan |
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Application publication date: 20110615 Assignee: Tieling Efan R & D Rubber and Plastic Co.,Ltd. Assignor: SHENYANG HUADA R & D CENTER OF POLYMER MATERIALS Co.,Ltd. Contract record no.: 2018210000017 Denomination of invention: Preparation method of mixed polyether-polyester polyurethane/epoxy damping composite Granted publication date: 20130403 License type: Common License Record date: 20180702 |
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