CN102090417A - Preparation method of living disinfectant - Google Patents
Preparation method of living disinfectant Download PDFInfo
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- CN102090417A CN102090417A CN2010106005157A CN201010600515A CN102090417A CN 102090417 A CN102090417 A CN 102090417A CN 2010106005157 A CN2010106005157 A CN 2010106005157A CN 201010600515 A CN201010600515 A CN 201010600515A CN 102090417 A CN102090417 A CN 102090417A
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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Abstract
The invention relates to a preparation method of a living disinfectant. The method comprises preparation of raw materials, preparation of stable chlorine dioxide and preparation of the product of the living disinfectant. By using the product of the living disinfectant produced by the method provided by the invention, the diplococcus gonorrhoeae, colibacillus, staphylococcus aureus, candida albicans, bacillus subtilis virus, hepatitis B virus, influenza virus, fungus, mould and transmissible pathogenic bacteria can be quickly killed; the product is colorless, tasteless and nontoxic, does not produce secondary pollution, generate resistance to drugs and stimulate eyes, skin and mucosa of a respiratory tract, is an environment-friendly product and can be applied to disinfection for object surfaces, traumatic inflammation and red and swollen vulva suffering pruritus so as to clear the peculiar smell.
Description
Technical field
The invention belongs to the sterile products production technical field, relate to and a kind of body surface or exogenous injury of human body inflammation and the red and swollen itch of vulva are carried out disinfection and remove the preparation method of the life thimerosal of peculiar smell.
Background technology
At present, the thimerosal kind that China's health and environmental administration are adopted is a lot, but the effect of these thimerosals is limited, and most of side effect in addition.
Summary of the invention
In order to overcome the above-mentioned shortcoming of prior art, the invention provides a kind of preparation method that can kill the life thimerosal of diplococcus, Escherichia coli, staphylococcus aureus, Candida albicans, withered grass gemma virus, hepatitis B, common cold virus, fungi, mould and propagated pathogenic bacteria fast.
The present invention solves the technical method that its technical problem adopts: a kind of preparation method of life thimerosal, and its processing step is:
The first step is the preparation of raw material:
In 60 ℃ soda ash liquid preparation jar, add sodium carbonate and the water of 60-80kg, after 2 hours, make the sodium carbonate liquor that weight percent concentration is 60-80% through stirring and dissolving;
Adding weight percent concentration in 80 ℃ sulfuric acid liquid preparation jar is the sulfuric acid solution of 92-96%, leaves standstill 2 hours;
In the sodium chlorite preparation jar of 30 ℃ of temperature, add sodium chlorite and the water of 85-98kg, after 2 hours, make the sodium chlorite solution that weight percent concentration is 85-98% through stirring and dissolving;
Second step was the preparation of stabilizing chlorine dioxide:
To join after metering in the reactor through prepared sulfuric acid solution of the first step and sodium chlorite solution, the temperature of control in the reactor is that 70 ℃, pressure are negative pressure 600mmHg post; After reacting 8 hours, prepared chlorine dioxide in the reactor is joined in the tourie, and add the sodium carbonate liquor that makes through the first step in tourie, the temperature under the condition of normal pressure in the control tourie is 40 ℃, after absorbing 8 hours, make the stabilizing chlorine dioxide finished product;
The 3rd step was the preparation of life thimerosal product:
Synthesize preparation in prepared stabilizing chlorine dioxide finished product of second step, adding pure water, auxiliary material and active material, make and contain the life thimerosal finished product that weight percent concentration is the chlorine dioxide of 0.09-0.1%, adding by weight ratio in per 100 gram life thimerosal finished products is tarragon 10-20 again: cassia twig 1-2: galangal 1-2: Pogostemon cablin 0.5-1: dalbergia wood 1-2: rhizoma cyperi 0.5-1 root of Dahurain angelica 1-2: the soup 1-5 gram that Radix Aconiti 0.5-1 boils is the life thimerosal product that 50ml/ props up through the canned specification that makes then.
Described auxiliary material employing weight percent concentration is 0.05～0.5% peppermint oil.
Described active material employing weight percent concentration is 0.03～0.1% emulsifier.
The weight percent concentration of arsenic is less than 0.0003 in the described life thimerosal finished product, and less than 0.0002, the pH value of life thimerosal finished product is 7-8 in the weight percent concentration of the heavy metal of lead.
The invention has the beneficial effects as follows: the life thimerosal that utilizes the present invention to produce can be killed diplococcus, Escherichia coli, staphylococcus aureus, Candida albicans, withered grass gemma virus, hepatitis B, common cold virus, fungi, mould and propagated pathogenic bacteria fast; This product is colourless, tasteless, nontoxic, non-secondary pollution, do not develop immunity to drugs, and is non-stimulated to eyes, skin, respiratory mucosa, is a kind of environment-friendly products, can be used for the red and swollen itch sterilization of body surface, wound inflammation and vulva, removes peculiar smell.
Description of drawings
Fig. 1 is a stabilizing chlorine dioxide technological process of production block diagram of the present invention.
Fig. 2 is a technological process of production block diagram of the present invention.
Embodiment
The present invention is further described below in conjunction with drawings and Examples.
Referring to Fig. 1 and Fig. 2, a kind of preparation method of life thimerosal, its processing step is:
The first step is the preparation of raw material:
In the soda ash liquid preparation jar of 60 ℃ of temperature, add 60-80kg sodium carbonate and water, after 2 hours, make the sodium carbonate liquor that weight percent concentration is 60-80% through stirring and dissolving;
Adding weight percent concentration in the sulfuric acid liquid preparation jar of 80 ℃ of temperature is the sulfuric acid solution of 92-96%, leaves standstill 2 hours;
In the sodium chlorite preparation jar of 30 ℃ of temperature, add 85-98kg sodium chlorite and water, after 2 hours, make the sodium chlorite solution that weight percent concentration is 85-98% through stirring and dissolving;
Second step was the preparation of stabilizing chlorine dioxide:
To after measuring, join in the reactor through prepared sulfuric acid solution of the first step and sodium chlorite solution, the reaction temperature of control in the reactor is that 70 ℃, pressure are negative pressure 600mmHg post, after reacting 8 hours, prepared chlorine dioxide in the reactor is joined in the tourie, and the sodium carbonate liquor that adding makes through the first step in tourie, temperature under the condition of normal pressure in the control tourie is 40 ℃, after absorbing 8 hours, makes the stabilizing chlorine dioxide finished product;
The 3rd step was the preparation of life thimerosal product:
To in prepared stabilizing chlorine dioxide finished product of second step, adding pure water, auxiliary material and active material synthesize preparation, auxiliary material employing weight percent concentration is 0.05～0.5% peppermint oil, it is that 0.03～0.1% emulsifier synthesizes preparation that active material adopts weight percent concentration, make and contain the life thimerosal finished product that weight percent concentration is the chlorine dioxide of 0.09-0.1%, adding by weight ratio in per 100 gram life thimerosal finished products is tarragon 10-20 again: cassia twig 1-2: galangal 1-2: Pogostemon cablin 0.5-1: dalbergia wood 1-2: rhizoma cyperi 0.5-1 root of Dahurain angelica 1-2: the soup 1-5 gram that Radix Aconiti 0.5-1 boils, be the life thimerosal product that 50ml/ props up through the canned specification that makes then, the weight percent concentration of arsenic is less than 0.0003 in the above-mentioned life thimerosal finished product, less than 0.0002, the pH value of life thimerosal finished product is 7-8 in the weight percent concentration of the heavy metal of lead.Clinical test results: cure rate 92%, efficient 99.5% in 500 routine diplococcuses, Escherichia coli, staphylococcus aureus, Candida albicans, withered grass gemma virus, hepatitis B, common cold virus, fungi, mould and propagated pathogenic bacteria patient's clinical treatment.。
The stabilizing chlorine dioxide finished product that the present invention produced has: the one, and broad spectrum activity: the thalline that can kill virus, bacterium, protist, algae, fungi and various spore and sporulation; The 2nd, can kill all bacterial propagules and many pathogenic bacteria under high efficiency: the 0.1ppm, 50ppm is kill vegetative forms of bacteria, hepatitis viruse, phage and bacterial spore fully; The 3rd, it is little influenced by temperature and ammonia, fungicidal effectiveness basically identical under low temperature and higher temperature; The 4th, pH is applied widely, can keep very high germicidal efficiency in pH2-10 scope; The 5th, safe noresidue not with organic matter generation chlorination, does not produce three and causes material and other noxious material; The 6th, to advantages such as human body are non-stimulated, when being lower than 500ppm, its influence can be ignored, and 100ppm is following not to have any influence to the people.
The life thimerosal product that utilizes the present invention to produce can be killed diplococcus, Escherichia coli, staphylococcus aureus, Candida albicans, withered grass gemma virus, hepatitis B, common cold virus, fungi, mould and propagated pathogenic bacteria fast; This product is colourless, tasteless, nontoxic, non-secondary pollution, do not develop immunity to drugs, and is non-stimulated to eyes, skin, respiratory mucosa, is a kind of environment-friendly products, can be used for body surface, and peculiar smell is removed in the red and swollen itch sterilization of wound inflammation and vulva.
Claims (4)
1. the preparation method of a life thimerosal is characterized in that processing step is:
The first step is the preparation of raw material:
In 60 ℃ soda ash liquid preparation jar, add sodium carbonate and the water of 60-80kg, after 2 hours, make the sodium carbonate liquor that weight percent concentration is 60-80% through stirring and dissolving;
Adding weight percent concentration in 80 ℃ sulfuric acid liquid preparation jar is the sulfuric acid solution of 92-96%, leaves standstill 2 hours;
In the sodium chlorite preparation jar of 30 ℃ of temperature, add sodium chlorite and the water of 85-98kg, after 2 hours, make the sodium chlorite solution that weight percent concentration is 85-98% through stirring and dissolving;
Second step was the preparation of stabilizing chlorine dioxide:
To join after metering in the reactor through prepared sulfuric acid solution of the first step and sodium chlorite solution, the temperature of control in the reactor is that 70 ℃, pressure are negative pressure 600mmHg post; After reacting 8 hours, prepared chlorine dioxide in the reactor is joined in the tourie, and add the sodium carbonate liquor that makes through the first step in tourie, the temperature under the condition of normal pressure in the control tourie is 40 ℃, after absorbing 8 hours, make the stabilizing chlorine dioxide finished product;
The 3rd step was the preparation of life thimerosal product:
Synthesize preparation in prepared stabilizing chlorine dioxide finished product of second step, adding pure water, auxiliary material and active material, make and contain the life thimerosal finished product that weight percent concentration is the chlorine dioxide of 0.09-0.1%, adding by weight ratio in per 100 gram life thimerosal finished products is tarragon 10-20 again: cassia twig 1-2: galangal 1-2: Pogostemon cablin 0.5-1: dalbergia wood 1-2: rhizoma cyperi 0.5-1 root of Dahurain angelica 1-2: the soup 1-5 gram that Radix Aconiti 0.5-1 boils is the life thimerosal product that 50ml/ props up through the canned specification that makes then.
2. the preparation method of life thimerosal as claimed in claim 1 is characterized in that: described auxiliary material employing weight percent concentration is 0.05～0.5% peppermint oil.
3. the preparation method of life thimerosal as claimed in claim 1 is characterized in that: described active material employing weight percent concentration is 0.03～0.1% emulsifier.
4. the preparation method of life thimerosal as claimed in claim 1, it is characterized in that: the weight percent concentration of arsenic is less than 0.0003 in the described life thimerosal finished product, less than 0.0002, the pH value of life thimerosal finished product is 7-8 in the weight percent concentration of the heavy metal of lead.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010106005157A CN102090417B (en) | 2010-12-22 | 2010-12-22 | Preparation method of living disinfectant |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010106005157A CN102090417B (en) | 2010-12-22 | 2010-12-22 | Preparation method of living disinfectant |
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| Publication Number | Publication Date |
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| CN102090417A true CN102090417A (en) | 2011-06-15 |
| CN102090417B CN102090417B (en) | 2013-07-03 |
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| CN2010106005157A Active CN102090417B (en) | 2010-12-22 | 2010-12-22 | Preparation method of living disinfectant |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103931685A (en) * | 2013-01-17 | 2014-07-23 | 上海市环境工程设计科学研究院有限公司 | Bacterium inhibiting agent for controlling pollutant gas emission during household garbage collection and transportation process, preparation and applications thereof |
| CN106135267A (en) * | 2015-04-24 | 2016-11-23 | 沈阳市梅杉化工厂 | A kind of mildew removing agent |
| CN106212575A (en) * | 2016-07-21 | 2016-12-14 | 南通铁人体育设施工程有限公司 | Furniture disinfectant |
| CN110403956A (en) * | 2019-08-31 | 2019-11-05 | 韶关蓝威消毒药业有限公司 | A kind of preparation method of skin wound antibacterial agent |
| CN113142250A (en) * | 2020-04-15 | 2021-07-23 | 广东爱锝医药技术研究院有限公司 | Air sterilization and disinfection composition |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1177445A (en) * | 1997-09-26 | 1998-04-01 | 叶中良 | Hygiene sterilizing liquid containing chlorine dioxide |
| CN1060138C (en) * | 1997-01-31 | 2001-01-03 | 陈秀珍 | Method for preparing high-purity high-concentration and stable chlorine dioxide |
| CN1067889C (en) * | 1997-05-26 | 2001-07-04 | 褚成炎 | Powerful disinfactant |
| CN1177755C (en) * | 2001-12-28 | 2004-12-01 | 南京理工大学 | Preparation equipment of high-purity chlorinedioxide stable liquor and its preparation process |
-
2010
- 2010-12-22 CN CN2010106005157A patent/CN102090417B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1060138C (en) * | 1997-01-31 | 2001-01-03 | 陈秀珍 | Method for preparing high-purity high-concentration and stable chlorine dioxide |
| CN1067889C (en) * | 1997-05-26 | 2001-07-04 | 褚成炎 | Powerful disinfactant |
| CN1177445A (en) * | 1997-09-26 | 1998-04-01 | 叶中良 | Hygiene sterilizing liquid containing chlorine dioxide |
| CN1177755C (en) * | 2001-12-28 | 2004-12-01 | 南京理工大学 | Preparation equipment of high-purity chlorinedioxide stable liquor and its preparation process |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103931685A (en) * | 2013-01-17 | 2014-07-23 | 上海市环境工程设计科学研究院有限公司 | Bacterium inhibiting agent for controlling pollutant gas emission during household garbage collection and transportation process, preparation and applications thereof |
| CN103931685B (en) * | 2013-01-17 | 2016-01-20 | 上海市环境工程设计科学研究院有限公司 | A kind of bacteriostatic agent and preparation and application thereof controlling Domestic Waste Collection fortune process contamination gas discharging |
| CN106135267A (en) * | 2015-04-24 | 2016-11-23 | 沈阳市梅杉化工厂 | A kind of mildew removing agent |
| CN106212575A (en) * | 2016-07-21 | 2016-12-14 | 南通铁人体育设施工程有限公司 | Furniture disinfectant |
| CN110403956A (en) * | 2019-08-31 | 2019-11-05 | 韶关蓝威消毒药业有限公司 | A kind of preparation method of skin wound antibacterial agent |
| CN113142250A (en) * | 2020-04-15 | 2021-07-23 | 广东爱锝医药技术研究院有限公司 | Air sterilization and disinfection composition |
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| Publication number | Publication date |
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| CN102090417B (en) | 2013-07-03 |
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