CN102056879B - 制备六氟异丙醇的连续方法 - Google Patents

制备六氟异丙醇的连续方法 Download PDF

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Publication number
CN102056879B
CN102056879B CN200980121726.8A CN200980121726A CN102056879B CN 102056879 B CN102056879 B CN 102056879B CN 200980121726 A CN200980121726 A CN 200980121726A CN 102056879 B CN102056879 B CN 102056879B
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CN
China
Prior art keywords
reactor
catalyst
hexafluoroisopropanol
hydrogen
hfip
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
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CN200980121726.8A
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English (en)
Chinese (zh)
Other versions
CN102056879A (zh
Inventor
S·M·蒂里
J·J·黑格多恩
J·A·舒尔茨
T·M·莱布
S·H·沃尔夫
S·K·森古普塔
G·P·尚克维茨
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Chemours Co FC LLC
Original Assignee
EI Du Pont de Nemours and Co
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Publication of CN102056879A publication Critical patent/CN102056879A/zh
Application granted granted Critical
Publication of CN102056879B publication Critical patent/CN102056879B/zh
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/132—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
    • C07C29/136—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH
    • C07C29/143—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of ketones
    • C07C29/145—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of ketones with hydrogen or hydrogen-containing gases

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CN200980121726.8A 2008-06-12 2009-06-24 制备六氟异丙醇的连续方法 Expired - Fee Related CN102056879B (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US12/138,002 US7524995B1 (en) 2008-06-12 2008-06-12 Continuous process to produce hexafluoroisopropanol
PCT/US2009/046078 WO2009152006A2 (en) 2008-06-12 2009-06-24 Continuous process to produce hexafluoroisopropanol

Publications (2)

Publication Number Publication Date
CN102056879A CN102056879A (zh) 2011-05-11
CN102056879B true CN102056879B (zh) 2014-11-05

Family

ID=40568899

Family Applications (1)

Application Number Title Priority Date Filing Date
CN200980121726.8A Expired - Fee Related CN102056879B (zh) 2008-06-12 2009-06-24 制备六氟异丙醇的连续方法

Country Status (5)

Country Link
US (1) US7524995B1 (cg-RX-API-DMAC7.html)
EP (1) EP2398754B1 (cg-RX-API-DMAC7.html)
JP (1) JP5400148B2 (cg-RX-API-DMAC7.html)
CN (1) CN102056879B (cg-RX-API-DMAC7.html)
WO (1) WO2009152006A2 (cg-RX-API-DMAC7.html)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102716761B (zh) * 2012-07-03 2013-10-23 浙江师范大学 用于三水六氟丙酮气相加氢生产六氟异丙醇的催化剂
CN106187691B (zh) * 2015-05-05 2019-01-18 浙江蓝天环保高科技股份有限公司 一种从含六氟异丙醇和氢气的混合气中回收六氟异丙醇的方法
JP2021066674A (ja) * 2019-10-18 2021-04-30 セントラル硝子株式会社 ヘキサフルオロイソプロパノールの統合再利用システムおよびヘキサフルオロイソプロパノールの統合再利用方法
CN111960429B (zh) * 2020-08-26 2022-07-12 万华化学集团股份有限公司 一种多级孔磷酸铝分子筛催化剂的制备方法、由其制备的催化剂及其在烯烃异构中的应用
CN119661320B (zh) * 2025-02-19 2025-06-27 淄博飞源化工有限公司 六氟异丙醇的合成方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3607952A (en) * 1969-03-28 1971-09-21 Du Pont Process for preparation of hexafluoroisopropanol
US5256163A (en) * 1991-09-11 1993-10-26 Philip Morris Incorporated Flow liquid-phase chemical reaction process
US7041857B1 (en) * 2005-09-07 2006-05-09 Air Products And Chemicals, Inc. Hydrogenation of acetone

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JPS6036411B2 (ja) * 1980-04-03 1985-08-20 セントラル硝子株式会社 １，１，１，３，３，３−ヘキサフルオロ−プロパン−２−オ−ルの製造法
JPS6054931B2 (ja) 1981-11-24 1985-12-03 旭硝子株式会社 １，１，１，３，３，３‐ヘキサフルオロ‐２‐プロパノールの製法
JPS59204142A (ja) 1983-04-28 1984-11-19 Nippon Mektron Ltd ヘキサフルオロイソプロピルアルコ−ルの製造法
JPS6069047A (ja) * 1983-09-27 1985-04-19 Central Glass Co Ltd １．１．１．３．３．３−ヘキサフルオロプロパン−２−オ−ルの製造法
JPH01301631A (ja) 1988-05-31 1989-12-05 Central Glass Co Ltd １，１，１，３，３，３−ヘキサフルオロプロパン−２−オールの製造法
JP2834495B2 (ja) * 1989-10-20 1998-12-09 三井化学株式会社 イソプロパノールの製造方法及び装置
JP2638727B2 (ja) 1992-12-21 1997-08-06 セントラル硝子株式会社 １，１，１，３，３，３−ヘキサフルオロプロパン−２−オ−ルの製造法
NL1004961C2 (nl) 1997-01-09 1998-07-13 Dsm Nv Monolietreactor.
JP4174079B2 (ja) 1997-06-24 2008-10-29 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー ２相水素化処理
US7291257B2 (en) 1997-06-24 2007-11-06 Process Dynamics, Inc. Two phase hydroprocessing
US6005143A (en) 1998-08-07 1999-12-21 Air Products And Chemicals, Inc. Use of a monolith catalyst for the hydrogenation of dinitrotoluene to toluenediamine
EP1121976A1 (en) * 2000-02-03 2001-08-08 Engelhard Corporation Chemical process in reactor with structured catalyst
US6506361B1 (en) 2000-05-18 2003-01-14 Air Products And Chemicals, Inc. Gas-liquid reaction process including ejector and monolith catalyst
AU2001290289A1 (en) 2000-09-27 2002-04-08 Asahi Glass Company, Limited Process for producing fluorinated alcohol
JP4288451B2 (ja) 2001-03-23 2009-07-01 ダイキン工業株式会社 １，１，１，３，３，３−ヘキサフルオロプロパン−２−オールの製造方法
US6479704B1 (en) 2001-04-20 2002-11-12 Air Products And Chemicals, Inc. Hydrogenation with monolith reactor under conditions of immiscible liquid phases
JP5028731B2 (ja) 2001-09-18 2012-09-19 旭硝子株式会社 ハロゲン化アルコ−ルの製造方法
DE602005024516D1 (de) 2004-02-04 2010-12-16 Halocarbon Prod Corp Aufreinigung von 1,1,1,3,3,3-hexafluorisopropanol
CN100420661C (zh) 2006-11-28 2008-09-24 上海三爱富新材料股份有限公司 1,1,1,3,3,3-六氟异丙醇的合成方法

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3607952A (en) * 1969-03-28 1971-09-21 Du Pont Process for preparation of hexafluoroisopropanol
US5256163A (en) * 1991-09-11 1993-10-26 Philip Morris Incorporated Flow liquid-phase chemical reaction process
US7041857B1 (en) * 2005-09-07 2006-05-09 Air Products And Chemicals, Inc. Hydrogenation of acetone

Also Published As

Publication number Publication date
WO2009152006A8 (en) 2011-08-11
WO2009152006A2 (en) 2009-12-17
CN102056879A (zh) 2011-05-11
WO2009152006A3 (en) 2010-03-04
JP5400148B2 (ja) 2014-01-29
EP2398754A2 (en) 2011-12-28
US7524995B1 (en) 2009-04-28
JP2011523957A (ja) 2011-08-25
EP2398754B1 (en) 2015-06-03

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Effective date of registration: 20180105

Address after: Delaware, USA

Patentee after: Como Efsee Co.,Ltd.

Address before: Delaware, USA

Patentee before: E. I. du Pont de Nemours and Co.

TR01 Transfer of patent right
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20141105

Termination date: 20190624

CF01 Termination of patent right due to non-payment of annual fee