CN101935863B - 一种铝合金电解抛光液及制备方法和铝合金电解抛光方法 - Google Patents
一种铝合金电解抛光液及制备方法和铝合金电解抛光方法 Download PDFInfo
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- CN101935863B CN101935863B CN200910108451A CN200910108451A CN101935863B CN 101935863 B CN101935863 B CN 101935863B CN 200910108451 A CN200910108451 A CN 200910108451A CN 200910108451 A CN200910108451 A CN 200910108451A CN 101935863 B CN101935863 B CN 101935863B
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- duraluminum
- polishing fluid
- content
- electrolysis
- aluminum alloy
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- 238000005498 polishing Methods 0.000 title claims abstract description 117
- 238000000034 method Methods 0.000 title claims abstract description 37
- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- 229910000838 Al alloy Inorganic materials 0.000 title abstract description 24
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims abstract description 55
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims abstract description 30
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 29
- 229910052782 aluminium Inorganic materials 0.000 claims abstract description 29
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims abstract description 28
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims abstract description 26
- 229910017053 inorganic salt Inorganic materials 0.000 claims abstract description 21
- 239000000203 mixture Substances 0.000 claims abstract description 5
- 229910000737 Duralumin Inorganic materials 0.000 claims description 88
- 239000012530 fluid Substances 0.000 claims description 72
- 238000005868 electrolysis reaction Methods 0.000 claims description 61
- 239000004411 aluminium Substances 0.000 claims description 24
- 239000013543 active substance Substances 0.000 claims description 23
- 239000000126 substance Substances 0.000 claims description 10
- VWDWKYIASSYTQR-UHFFFAOYSA-N sodium nitrate Chemical compound [Na+].[O-][N+]([O-])=O VWDWKYIASSYTQR-UHFFFAOYSA-N 0.000 claims description 8
- 239000000463 material Substances 0.000 claims description 6
- 239000001508 potassium citrate Substances 0.000 claims description 4
- QEEAPRPFLLJWCF-UHFFFAOYSA-K potassium citrate (anhydrous) Chemical compound [K+].[K+].[K+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O QEEAPRPFLLJWCF-UHFFFAOYSA-K 0.000 claims description 4
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Chemical compound [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 claims description 4
- 235000010344 sodium nitrate Nutrition 0.000 claims description 4
- 239000004317 sodium nitrate Substances 0.000 claims description 4
- 229940001516 sodium nitrate Drugs 0.000 claims description 4
- 235000015870 tripotassium citrate Nutrition 0.000 claims description 4
- IRXRGVFLQOSHOH-UHFFFAOYSA-L dipotassium;oxalate Chemical compound [K+].[K+].[O-]C(=O)C([O-])=O IRXRGVFLQOSHOH-UHFFFAOYSA-L 0.000 claims description 2
- 235000010333 potassium nitrate Nutrition 0.000 claims description 2
- 239000004323 potassium nitrate Substances 0.000 claims description 2
- 239000001509 sodium citrate Substances 0.000 claims description 2
- ZNCPFRVNHGOPAG-UHFFFAOYSA-L sodium oxalate Chemical compound [Na+].[Na+].[O-]C(=O)C([O-])=O ZNCPFRVNHGOPAG-UHFFFAOYSA-L 0.000 claims description 2
- 229940039790 sodium oxalate Drugs 0.000 claims description 2
- HRXKRNGNAMMEHJ-UHFFFAOYSA-K trisodium citrate Chemical compound [Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O HRXKRNGNAMMEHJ-UHFFFAOYSA-K 0.000 claims description 2
- 229940038773 trisodium citrate Drugs 0.000 claims description 2
- 238000002156 mixing Methods 0.000 abstract description 7
- 239000004094 surface-active agent Substances 0.000 abstract 2
- 239000000243 solution Substances 0.000 description 18
- 239000007788 liquid Substances 0.000 description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 14
- 230000005611 electricity Effects 0.000 description 9
- 238000012360 testing method Methods 0.000 description 9
- 230000000694 effects Effects 0.000 description 8
- 230000000052 comparative effect Effects 0.000 description 7
- 239000003795 chemical substances by application Substances 0.000 description 6
- 239000002253 acid Substances 0.000 description 5
- 239000008367 deionised water Substances 0.000 description 5
- 229910021641 deionized water Inorganic materials 0.000 description 5
- 238000003756 stirring Methods 0.000 description 5
- 238000010438 heat treatment Methods 0.000 description 4
- 229910052751 metal Inorganic materials 0.000 description 4
- 239000002184 metal Substances 0.000 description 4
- 238000005406 washing Methods 0.000 description 4
- 230000008859 change Effects 0.000 description 3
- 238000005260 corrosion Methods 0.000 description 3
- 230000007797 corrosion Effects 0.000 description 3
- 230000002950 deficient Effects 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 230000008569 process Effects 0.000 description 3
- -1 Aluminum ion Chemical class 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- 238000007605 air drying Methods 0.000 description 2
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical group [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 239000006071 cream Substances 0.000 description 2
- 239000013527 degreasing agent Substances 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 125000004435 hydrogen atom Chemical class [H]* 0.000 description 2
- 238000007654 immersion Methods 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 239000003595 mist Substances 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- CHCGWNQHGOGCNA-UHFFFAOYSA-N 2,3-dimethyl-4-nitrobenzoic acid Chemical compound CC1=C(C)C([N+]([O-])=O)=CC=C1C(O)=O CHCGWNQHGOGCNA-UHFFFAOYSA-N 0.000 description 1
- 229910001339 C alloy Inorganic materials 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical group [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 1
- 102000004160 Phosphoric Monoester Hydrolases Human genes 0.000 description 1
- 108090000608 Phosphoric Monoester Hydrolases Proteins 0.000 description 1
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 239000003518 caustics Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000005034 decoration Methods 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 238000007598 dipping method Methods 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000008151 electrolyte solution Substances 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000011010 flushing procedure Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 238000003384 imaging method Methods 0.000 description 1
- 230000005764 inhibitory process Effects 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 229910017604 nitric acid Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 150000003016 phosphoric acids Chemical class 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000002203 pretreatment Methods 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 239000004576 sand Substances 0.000 description 1
- 238000007493 shaping process Methods 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 230000003019 stabilising effect Effects 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Landscapes
- Electrical Discharge Machining, Electrochemical Machining, And Combined Machining (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200910108451A CN101935863B (zh) | 2009-06-30 | 2009-06-30 | 一种铝合金电解抛光液及制备方法和铝合金电解抛光方法 |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200910108451A CN101935863B (zh) | 2009-06-30 | 2009-06-30 | 一种铝合金电解抛光液及制备方法和铝合金电解抛光方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101935863A CN101935863A (zh) | 2011-01-05 |
| CN101935863B true CN101935863B (zh) | 2012-09-05 |
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|---|---|---|---|
| CN200910108451A Expired - Fee Related CN101935863B (zh) | 2009-06-30 | 2009-06-30 | 一种铝合金电解抛光液及制备方法和铝合金电解抛光方法 |
Country Status (1)
| Country | Link |
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| CN (1) | CN101935863B (und) |
Families Citing this family (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102268675B (zh) * | 2011-07-27 | 2012-11-14 | 厦门大学 | 一种两酸铝制品化学抛光液及其使用方法 |
| CN102312276A (zh) * | 2011-08-22 | 2012-01-11 | 吴江市精工铝字制造厂 | 铝硅合金的电解抛光液 |
| CN102797029B (zh) * | 2012-09-10 | 2015-04-15 | 广州波耳化工材料有限公司 | 电解抛光剂 |
| CN102817035B (zh) * | 2012-09-10 | 2014-08-27 | 广州波耳化工材料有限公司 | 应用于自动化生产的铝合金化学抛光剂 |
| CN105369338B (zh) * | 2013-05-17 | 2017-06-16 | 江苏理工学院 | 一种在纯铝表面形成纳米级多孔膜层的方法 |
| TWI568895B (zh) * | 2016-02-05 | 2017-02-01 | Ming Chi Univ Of Tech | Environmentally friendly biocompatible electrolytic polishing solution |
| CN106757298B (zh) * | 2016-12-21 | 2019-08-02 | 江苏和兴汽车科技有限公司 | 一种无铬电抛光液、铝合金电抛光的方法及汽车铝装饰件 |
| CN106987840B (zh) * | 2017-03-03 | 2018-12-11 | 深圳市中盈建科控股有限公司 | 不锈钢8k镜面的抛光液 |
| CN108624947B (zh) * | 2017-03-21 | 2023-02-28 | 浙江瑞特良微电子材料有限公司 | 一种铝合金电解抛光液及其制备方法 |
| CN107675244A (zh) * | 2017-09-28 | 2018-02-09 | 上海理工大学 | 一种用于镍钛合金电化学抛光的抛光液及用途 |
| CN108118386A (zh) * | 2017-12-29 | 2018-06-05 | 重庆全茂合渝科技有限公司 | 一种摩托车拔叉轴电解抛光工艺 |
| CN110578164A (zh) * | 2018-06-11 | 2019-12-17 | 深圳市裕展精密科技有限公司 | 钛及钛合金的电化学抛光电解液及其使用方法 |
| CN108896378A (zh) * | 2018-06-13 | 2018-11-27 | 中国航发北京航空材料研究院 | 一种高温合金的电解抛光腐蚀剂及其使用方法 |
| CN113337876A (zh) * | 2021-04-22 | 2021-09-03 | 中国石油大学(北京) | 电解抛光液以及镍钛合金的电解抛光方法 |
| CN115044959B (zh) * | 2022-04-13 | 2023-08-15 | 东南大学 | 用于检验金刚石/铝硅复合材料界面的腐蚀剂及其使用方法 |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1107904A (zh) * | 1994-12-29 | 1995-09-06 | 华中理工大学 | 铝及铝合金焊丝的电化学抛光方法 |
| CN1412352A (zh) * | 2001-10-10 | 2003-04-23 | Wkw艾尔伯斯略自动化股份有限公司 | 铝电解抛光的方法和其应用 |
-
2009
- 2009-06-30 CN CN200910108451A patent/CN101935863B/zh not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1107904A (zh) * | 1994-12-29 | 1995-09-06 | 华中理工大学 | 铝及铝合金焊丝的电化学抛光方法 |
| CN1412352A (zh) * | 2001-10-10 | 2003-04-23 | Wkw艾尔伯斯略自动化股份有限公司 | 铝电解抛光的方法和其应用 |
Non-Patent Citations (2)
| Title |
|---|
| 方景礼.铝及铝合金制件的电解抛光.《金属材料抛光技术》.国防工业出版社,2007,223-231. * |
| 陈亚等.电化学抛光.《现代实用电镀技术》.国防工业出版社,2003,(第1版),75. * |
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| Publication number | Publication date |
|---|---|
| CN101935863A (zh) | 2011-01-05 |
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