CN101874063B - 形成微孔和抗微生物制品的方法 - Google Patents
形成微孔和抗微生物制品的方法 Download PDFInfo
- Publication number
- CN101874063B CN101874063B CN200880117856.XA CN200880117856A CN101874063B CN 101874063 B CN101874063 B CN 101874063B CN 200880117856 A CN200880117856 A CN 200880117856A CN 101874063 B CN101874063 B CN 101874063B
- Authority
- CN
- China
- Prior art keywords
- composition
- weight
- carbon atoms
- polylactic acid
- acyl group
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C55/00—Shaping by stretching, e.g. drawing through a die; Apparatus therefor
- B29C55/005—Shaping by stretching, e.g. drawing through a die; Apparatus therefor characterised by the choice of materials
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K47/00—Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
- A61K47/30—Macromolecular organic or inorganic compounds, e.g. inorganic polyphosphates
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
- C08J9/0014—Use of organic additives
- C08J9/0023—Use of organic additives containing oxygen
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
- C08J9/0066—Use of inorganic compounding ingredients
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
- C08J9/26—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof by elimination of a solid phase from a macromolecular composition or article, e.g. leaching out
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
- C08J9/28—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof by elimination of a liquid phase from a macromolecular composition or article, e.g. drying of coagulum
- C08J9/283—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof by elimination of a liquid phase from a macromolecular composition or article, e.g. drying of coagulum a discontinuous liquid phase emulsified in a continuous macromolecular phase
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
- B29K2067/00—Use of polyesters or derivatives thereof, as moulding material
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
- B29K2067/00—Use of polyesters or derivatives thereof, as moulding material
- B29K2067/04—Polyesters derived from hydroxycarboxylic acids
- B29K2067/046—PLA, i.e. polylactic acid or polylactide
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
- B29K2105/00—Condition, form or state of moulded material or of the material to be shaped
- B29K2105/04—Condition, form or state of moulded material or of the material to be shaped cellular or porous
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
- B29K2995/00—Properties of moulding materials, reinforcements, fillers, preformed parts or moulds
- B29K2995/0037—Other properties
- B29K2995/0059—Degradable
- B29K2995/006—Bio-degradable, e.g. bioabsorbable, bioresorbable or bioerodible
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2201/00—Foams characterised by the foaming process
- C08J2201/04—Foams characterised by the foaming process characterised by the elimination of a liquid or solid component, e.g. precipitation, leaching out, evaporation
- C08J2201/046—Elimination of a polymeric phase
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2367/00—Characterised by the use of polyesters obtained by reactions forming a carboxylic ester link in the main chain; Derivatives of such polymers
- C08J2367/04—Polyesters derived from hydroxy carboxylic acids, e.g. lactones
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/34—Silicon-containing compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/0008—Organic ingredients according to more than one of the "one dot" groups of C08K5/01 - C08K5/59
- C08K5/0083—Nucleating agents promoting the crystallisation of the polymer matrix
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/04—Oxygen-containing compounds
- C08K5/10—Esters; Ether-esters
- C08K5/11—Esters; Ether-esters of acyclic polycarboxylic acids
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Medicinal Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Emergency Medicine (AREA)
- Mechanical Engineering (AREA)
- Pharmacology & Pharmacy (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Epidemiology (AREA)
- Manufacture Of Porous Articles, And Recovery And Treatment Of Waste Products (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Biological Depolymerization Polymers (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US98999907P | 2007-11-26 | 2007-11-26 | |
| US60/989,999 | 2007-11-26 | ||
| PCT/US2008/084774 WO2009070630A1 (en) | 2007-11-26 | 2008-11-26 | Methods for forming microporous and antimicrobial articles |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101874063A CN101874063A (zh) | 2010-10-27 |
| CN101874063B true CN101874063B (zh) | 2013-01-02 |
Family
ID=40435056
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN200880117856.XA Expired - Fee Related CN101874063B (zh) | 2007-11-26 | 2008-11-26 | 形成微孔和抗微生物制品的方法 |
Country Status (7)
| Country | Link |
|---|---|
| US (2) | US20100258977A1 (cg-RX-API-DMAC7.html) |
| EP (1) | EP2220150B1 (cg-RX-API-DMAC7.html) |
| JP (2) | JP5612476B2 (cg-RX-API-DMAC7.html) |
| KR (1) | KR101503962B1 (cg-RX-API-DMAC7.html) |
| CN (1) | CN101874063B (cg-RX-API-DMAC7.html) |
| BR (1) | BRPI0820548A8 (cg-RX-API-DMAC7.html) |
| WO (1) | WO2009070630A1 (cg-RX-API-DMAC7.html) |
Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20130165880A1 (en) | 2010-09-17 | 2013-06-27 | David T. Amos | Antimicrobial disposable absorbent articles |
| US20120087968A1 (en) * | 2010-10-07 | 2012-04-12 | Cryovac, Inc. | Antimicrobial Packaging Material and Methods of Making and Using the Same |
| US9637605B2 (en) * | 2011-11-10 | 2017-05-02 | Toray Plastics (America), Inc. | Biaxially oriented cavitated polylactic acid film |
| DE102012001524A1 (de) * | 2012-01-16 | 2013-07-18 | Ewald Dörken Ag | Verfahren zur Herstellung einer hydrophilen Polymermembran und Polymermembran |
| DE102012001544A1 (de) * | 2012-01-16 | 2013-07-18 | Ewald Dörken Ag | Verfahren zur Herstellung einer Mikrofiltrationsmembran und Mikrofiltrationsmembran |
| CN102838858B (zh) * | 2012-09-21 | 2014-12-24 | 上海同杰良生物材料有限公司 | 一种聚乳酸成核剂及其制备和应用 |
| JP6291488B2 (ja) * | 2013-05-20 | 2018-03-14 | 株式会社カネカ | ポリエステル樹脂組成物および該樹脂組成物を含む成形体 |
| US9732184B2 (en) * | 2014-07-29 | 2017-08-15 | W. L. Gore & Associates, Inc. | Process for producing articles formed from polylactic acid and articles made therefrom |
| EP3265135B1 (en) * | 2015-03-06 | 2023-06-07 | John Paul Wilson | Instrinsically antimicrobial porosic matrix composites and method of manufacture thereof |
| US10668458B2 (en) | 2015-09-23 | 2020-06-02 | University Of Ulsan Foundation For Industry Cooperation | Photocatalyst having high visible-light activity |
| WO2020009924A1 (en) * | 2018-07-02 | 2020-01-09 | Celanese EVA Performance Polymers Corporation | Antibiotic beads for treatment of an infection |
| CN110396180B (zh) * | 2019-06-14 | 2021-09-24 | 南京先进生物材料与过程装备研究院有限公司 | 一种利用甜菜碱精密制备脂肪族聚酯的方法 |
| US20220305176A1 (en) * | 2019-08-30 | 2022-09-29 | Northwestern University | Biodegradable soft elastomers for regenerative engineering |
| US11179663B1 (en) * | 2021-02-01 | 2021-11-23 | Aviro Llc | Polyurethane-based materials |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1911982A (zh) * | 2006-08-24 | 2007-02-14 | 中国民航大学 | 一种可生物降解的微孔发泡聚合物及其制备方法 |
| CN1939543A (zh) * | 2006-09-14 | 2007-04-04 | 同济大学 | 聚乳酸基/纳米羟基磷灰石复合支架材料及其制备方法 |
Family Cites Families (42)
| Publication number | Priority date | Publication date | Assignee | Title |
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| US3565985A (en) | 1969-04-10 | 1971-02-23 | Dow Chemical Co | Method of preparing multilayer plastic articles |
| US4247498A (en) * | 1976-08-30 | 1981-01-27 | Akzona Incorporated | Methods for making microporous products |
| US4539256A (en) | 1982-09-09 | 1985-09-03 | Minnesota Mining And Manufacturing Co. | Microporous sheet material, method of making and articles made therewith |
| DE3620685A1 (de) * | 1986-06-20 | 1987-12-23 | Henkel Kgaa | Neue mittel zur abdeckung unverletzter und/oder verletzter bereiche menschlicher oder tierischer haut |
| US4726989A (en) * | 1986-12-11 | 1988-02-23 | Minnesota Mining And Manufacturing | Microporous materials incorporating a nucleating agent and methods for making same |
| AU618517B2 (en) * | 1986-12-23 | 1992-01-02 | Eugene J. Van Scott | Additives enhancing topical actions of therapeutic agents |
| US4867881A (en) * | 1987-09-14 | 1989-09-19 | Minnesota Minning And Manufacturing Company | Orientied microporous film |
| US5238618A (en) * | 1987-09-14 | 1993-08-24 | Minnesota Mining And Manufacturing Company | Method for preparing oriented microporous film |
| US5443727A (en) * | 1990-10-30 | 1995-08-22 | Minnesota Mining And Manufacturing Company | Articles having a polymeric shell and method for preparing same |
| CA2116679C (en) | 1991-10-01 | 2003-11-04 | David B. Herridge | Coextruded pressure-sensitive adhesive tape and method of making |
| US5589122A (en) | 1991-10-01 | 1996-12-31 | Minnesota Mining And Manufacturing Company | Method of making double-sided pressure-sensitive adhesive tape |
| CA2106262C (en) | 1992-10-01 | 2003-11-18 | Ralph H. Bland | Tear resistant multilayer films and articles incorporating such films |
| JP3359744B2 (ja) * | 1994-07-14 | 2002-12-24 | 三井化学株式会社 | 多孔性フィルムおよびその製造方法 |
| US5804610A (en) * | 1994-09-09 | 1998-09-08 | Minnesota Mining And Manufacturing Company | Methods of making packaged viscoelastic compositions |
| JPH09157425A (ja) * | 1995-12-11 | 1997-06-17 | Mitsubishi Rayon Co Ltd | 多孔体およびその製造方法 |
| US5993954A (en) * | 1997-04-29 | 1999-11-30 | 3M Innovative Properties Company | Temperature-sensitive microporous film |
| ATE277208T1 (de) * | 1997-05-02 | 2004-10-15 | Cargill Inc | Abbaubare polymerfasern: herstellung, produkte und verwendungsverfahren |
| JP4052707B2 (ja) * | 1998-01-07 | 2008-02-27 | 旭化成ケミカルズ株式会社 | 多層微多孔フィルムの製造方法 |
| US6171689B1 (en) * | 1999-01-15 | 2001-01-09 | 3M Innovative Properties Company | Flame retardant microporous materials |
| JP2002541925A (ja) * | 1999-04-16 | 2002-12-10 | ラトガーズ,ザ ステイト ユニバーシティ | 組織工学用多孔質ポリマー足場 |
| WO2001060157A2 (en) * | 2000-02-18 | 2001-08-23 | The Procter & Gamble Company | Antibacterial agents and compositions |
| EP2548739B1 (en) * | 2000-06-02 | 2015-12-16 | Fujifilm Corporation | Lithographic printing plate precursor |
| JP3410075B2 (ja) * | 2000-11-17 | 2003-05-26 | ユニチカ株式会社 | 結晶性ポリ乳酸樹脂組成物、これを用いたフィルムおよびシート |
| JP3461808B2 (ja) * | 2001-03-13 | 2003-10-27 | ユニチカ株式会社 | ポリ乳酸系梱包バンド |
| US6660211B2 (en) * | 2001-04-23 | 2003-12-09 | Kimberly-Clark Worldwide, Inc. | Methods of making biodegradable films having enhanced ductility and breathability |
| JP3748832B2 (ja) * | 2001-06-19 | 2006-02-22 | 理研ビタミン株式会社 | 脂肪族ポリエステル組成物及び可撓性成形物 |
| JP4531395B2 (ja) * | 2001-08-01 | 2010-08-25 | 旭化成メディカル株式会社 | 多層微多孔膜 |
| US7114621B2 (en) * | 2001-12-14 | 2006-10-03 | 3M Innovative Properties Company | Membrane module elements |
| US6858290B2 (en) * | 2002-05-29 | 2005-02-22 | 3M Innovative Properties Company | Fluid repellent microporous materials |
| US20040265565A1 (en) * | 2003-06-30 | 2004-12-30 | Fischer Patrick J. | Microporous article containing flame retardant |
| US7338692B2 (en) * | 2003-09-12 | 2008-03-04 | 3M Innovative Properties Company | Microporous PVDF films |
| US20050112352A1 (en) * | 2003-11-26 | 2005-05-26 | Laney Thomas M. | Polylactic-acid-based sheet material and method of making |
| CN100447198C (zh) * | 2004-03-04 | 2008-12-31 | 尤尼吉可株式会社 | 生物降解性聚酯树脂组合物、其制造方法及其泡沫体和成形物 |
| US20060051384A1 (en) | 2004-09-07 | 2006-03-09 | 3M Innovative Properties Company | Antiseptic compositions and methods of use |
| US20060148915A1 (en) * | 2004-12-30 | 2006-07-06 | Floyd Robert M | Microporous materials and methods of making |
| JP2006335909A (ja) * | 2005-06-03 | 2006-12-14 | Fujifilm Holdings Corp | 電子機器用部材 |
| US20070065655A1 (en) * | 2005-09-19 | 2007-03-22 | Floyd Robert M | Flame retardant porous film |
| JP2007138148A (ja) * | 2005-10-19 | 2007-06-07 | Kao Corp | 多孔性シート |
| AU2007236549B2 (en) * | 2006-04-07 | 2011-11-03 | The University Of Melbourne | Porous polymer blend structures |
| EP2010595A4 (en) | 2006-04-07 | 2010-09-08 | Univ Queensland | POROUS POLYMER STRUCTURES |
| WO2008026684A1 (en) * | 2006-08-31 | 2008-03-06 | Nisshinbo Industries, Inc. | Porous film and printing base |
| US9555167B2 (en) * | 2006-12-11 | 2017-01-31 | 3M Innovative Properties Company | Biocompatible antimicrobial compositions |
-
2008
- 2008-11-26 WO PCT/US2008/084774 patent/WO2009070630A1/en not_active Ceased
- 2008-11-26 KR KR1020107014087A patent/KR101503962B1/ko not_active Expired - Fee Related
- 2008-11-26 BR BRPI0820548A patent/BRPI0820548A8/pt not_active Application Discontinuation
- 2008-11-26 EP EP08855728.5A patent/EP2220150B1/en not_active Not-in-force
- 2008-11-26 US US12/743,290 patent/US20100258977A1/en not_active Abandoned
- 2008-11-26 CN CN200880117856.XA patent/CN101874063B/zh not_active Expired - Fee Related
- 2008-11-26 JP JP2010535120A patent/JP5612476B2/ja not_active Expired - Fee Related
-
2012
- 2012-12-03 US US13/692,391 patent/US20130096194A1/en not_active Abandoned
-
2014
- 2014-07-10 JP JP2014142182A patent/JP6042848B2/ja not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1911982A (zh) * | 2006-08-24 | 2007-02-14 | 中国民航大学 | 一种可生物降解的微孔发泡聚合物及其制备方法 |
| CN1939543A (zh) * | 2006-09-14 | 2007-04-04 | 同济大学 | 聚乳酸基/纳米羟基磷灰石复合支架材料及其制备方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| KR20100110310A (ko) | 2010-10-12 |
| JP2011504945A (ja) | 2011-02-17 |
| JP2014208844A (ja) | 2014-11-06 |
| CN101874063A (zh) | 2010-10-27 |
| WO2009070630A1 (en) | 2009-06-04 |
| JP5612476B2 (ja) | 2014-10-22 |
| JP6042848B2 (ja) | 2016-12-14 |
| KR101503962B1 (ko) | 2015-03-18 |
| BRPI0820548A8 (pt) | 2015-09-29 |
| EP2220150B1 (en) | 2013-11-06 |
| BRPI0820548A2 (pt) | 2015-06-16 |
| US20100258977A1 (en) | 2010-10-14 |
| EP2220150A1 (en) | 2010-08-25 |
| US20130096194A1 (en) | 2013-04-18 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20130102 Termination date: 20181126 |