CN101874027B - 使用分子筛将反式-顺式荆芥内酯转化成顺式-反式荆芥内酯的方法 - Google Patents

使用分子筛将反式-顺式荆芥内酯转化成顺式-反式荆芥内酯的方法 Download PDF

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Publication number
CN101874027B
CN101874027B CN200880117731.7A CN200880117731A CN101874027B CN 101874027 B CN101874027 B CN 101874027B CN 200880117731 A CN200880117731 A CN 200880117731A CN 101874027 B CN101874027 B CN 101874027B
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CN
China
Prior art keywords
trans
nepetalactone
cis
mixture
molecular sieves
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Expired - Fee Related
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CN200880117731.7A
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English (en)
Chinese (zh)
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CN101874027A (zh
Inventor
Y·冈萨雷斯
D·R·科尔宾
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EIDP Inc
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EI Du Pont de Nemours and Co
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D311/00—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings
    • C07D311/02—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings ortho- or peri-condensed with carbocyclic rings or ring systems
    • C07D311/94—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings ortho- or peri-condensed with carbocyclic rings or ring systems condensed with rings other than six-membered or with ring systems containing such rings

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Fats And Perfumes (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Seasonings (AREA)
  • Pyrane Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
CN200880117731.7A 2007-11-26 2008-11-26 使用分子筛将反式-顺式荆芥内酯转化成顺式-反式荆芥内酯的方法 Expired - Fee Related CN101874027B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US99011707P 2007-11-26 2007-11-26
US60/990,117 2007-11-26
PCT/US2008/084795 WO2009070641A1 (en) 2007-11-26 2008-11-26 Method for converting trans-cis nepetalactone to cis-trans nepetalactone using molecular sieves

Publications (2)

Publication Number Publication Date
CN101874027A CN101874027A (zh) 2010-10-27
CN101874027B true CN101874027B (zh) 2014-08-20

Family

ID=40364434

Family Applications (1)

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CN200880117731.7A Expired - Fee Related CN101874027B (zh) 2007-11-26 2008-11-26 使用分子筛将反式-顺式荆芥内酯转化成顺式-反式荆芥内酯的方法

Country Status (10)

Country Link
US (1) US8802870B2 (https=)
EP (1) EP2217586B1 (https=)
JP (1) JP5377508B2 (https=)
KR (1) KR101577472B1 (https=)
CN (1) CN101874027B (https=)
CA (1) CA2705367C (https=)
ES (1) ES2442010T3 (https=)
MX (1) MX2010005706A (https=)
WO (1) WO2009070641A1 (https=)
ZA (1) ZA201003220B (https=)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7547793B2 (en) * 2003-03-19 2009-06-16 E.I. Du Pont De Nemours And Company Method for making insect repellent composition
CA2648270C (en) * 2006-05-10 2014-07-08 E.I. Du Pont De Nemours And Company Formulated tick and insect repellent compositions comprising dihydronepetalactone
US9521844B2 (en) 2006-12-21 2016-12-20 E I Du Pont De Nemours And Company Solvent addition and removal in the hydrogenation of catmint oil
SI2121885T1 (sl) * 2006-12-21 2017-10-30 E.I. Du Pont De Nemours And Company Parna destilacija mačje mete
WO2008079253A1 (en) 2006-12-21 2008-07-03 E. I. Du Pont De Nemours And Company Hydrogenation of catmint oil
SI2114911T1 (sl) * 2006-12-21 2015-12-31 E.I. Du Pont De Nemours And Company Produkcija dihidronepetalaktona s hidrogeniranjem nepetalaktona
BRPI0719453A2 (pt) * 2006-12-21 2014-03-18 Du Pont Processo de preparação de óleo de erva dos gatos hidrogenado, processo de preparação de produtos formulados com um óleo de erva dos gatos hidrogenado e óleo de erva dos gatos hidrogenado
CA2705367C (en) 2007-11-26 2016-05-31 E.I. Du Pont De Nemours And Company Method for converting trans-cis nepetalactone to cis-trans nepetalactone using molecular sieves
JP5805099B2 (ja) 2009-11-11 2015-11-04 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニーＥ．Ｉ．Ｄｕ Ｐｏｎｔ Ｄｅ Ｎｅｍｏｕｒｓ Ａｎｄ Ｃｏｍｐａｎｙ イヌハッカ油の回収を向上させる方法
EP2762873A4 (en) 2011-09-26 2015-05-20 Toto Ltd METHOD FOR SPECIFIC DETECTION OF A TEST SUBSTANCE
JP6107466B2 (ja) 2012-06-28 2017-04-05 セントラル硝子株式会社 トランス−１，３，３，３−テトラフルオロプロペンの精製方法
CN103012338B (zh) * 2012-12-07 2014-10-08 南京中医药大学 一种荆芥内酯对溴苯甲酸酯及其制备工艺和用途
CN114324645B (zh) * 2021-12-24 2023-10-24 广州白云山汉方现代药业有限公司 一种快速鉴别藏荆芥药材的方法
US12378213B1 (en) 2024-08-13 2025-08-05 William Allen Boulanger Process for the hydrogenation of catnip oil

Citations (1)

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CN85103199A (zh) * 1984-04-13 1986-10-22 联合碳化公司 分子筛合成物

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US5072063A (en) * 1990-01-09 1991-12-10 Dowelanco Process for rearranging allylic geminal dihalogen compounds
WO1998021170A1 (en) * 1996-11-13 1998-05-22 Chevron Chemical Company Llc Process for olefin isomerization
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US20030235601A1 (en) 2002-03-20 2003-12-25 Hallahan David L. Insect repellent compounds
EP1490351B1 (en) 2002-04-03 2007-06-06 E.I. Du Pont De Nemours And Company Production of dihydronepetalactone by hydrogenation of nepetalactone
WO2003086069A2 (en) 2002-04-08 2003-10-23 Jodi Haenke Materials and methods for controlling wood-boring insects
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GB0409542D0 (en) 2004-04-29 2004-06-02 Unilever Plc Cosmetic compositions
CA2584354C (en) 2004-11-03 2015-02-24 E.I. Du Pont De Nemours And Company Insect repellent compositions comprising dihydronepetalactone, an alcohol and an ester
CN101316510A (zh) 2005-09-30 2008-12-03 纳幕尔杜邦公司 蒲勒酸昆虫驱避剂
CA2648270C (en) 2006-05-10 2014-07-08 E.I. Du Pont De Nemours And Company Formulated tick and insect repellent compositions comprising dihydronepetalactone
BRPI0719453A2 (pt) 2006-12-21 2014-03-18 Du Pont Processo de preparação de óleo de erva dos gatos hidrogenado, processo de preparação de produtos formulados com um óleo de erva dos gatos hidrogenado e óleo de erva dos gatos hidrogenado
SI2121885T1 (sl) 2006-12-21 2017-10-30 E.I. Du Pont De Nemours And Company Parna destilacija mačje mete
EP2129643A2 (en) 2006-12-21 2009-12-09 E. I. Du Pont de Nemours and Company Hydrogenation of caryophyllene
SI2114911T1 (sl) 2006-12-21 2015-12-31 E.I. Du Pont De Nemours And Company Produkcija dihidronepetalaktona s hidrogeniranjem nepetalaktona
WO2008079253A1 (en) 2006-12-21 2008-07-03 E. I. Du Pont De Nemours And Company Hydrogenation of catmint oil
DE102007026049A1 (de) 2007-05-31 2008-12-04 Beiersdorf Ag Repellentien gegen Wespen
CA2705367C (en) 2007-11-26 2016-05-31 E.I. Du Pont De Nemours And Company Method for converting trans-cis nepetalactone to cis-trans nepetalactone using molecular sieves

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN85103199A (zh) * 1984-04-13 1986-10-22 联合碳化公司 分子筛合成物

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* Cited by examiner, † Cited by third party
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Ilme Liblikas等.Simplified Isolation Procedure and Interconversion of the Diastereomers of Nepetalactone and Nepetalactol.《J. Nat. Prod.》.2005,第68卷886-890. *

Also Published As

Publication number Publication date
MX2010005706A (es) 2010-06-02
WO2009070641A1 (en) 2009-06-04
CN101874027A (zh) 2010-10-27
US20100261915A1 (en) 2010-10-14
US8802870B2 (en) 2014-08-12
JP5377508B2 (ja) 2013-12-25
CA2705367C (en) 2016-05-31
KR101577472B1 (ko) 2015-12-14
EP2217586B1 (en) 2013-11-13
JP2011504882A (ja) 2011-02-17
ES2442010T3 (es) 2014-02-07
ZA201003220B (en) 2011-08-31
KR20100099207A (ko) 2010-09-10
CA2705367A1 (en) 2009-06-04
EP2217586A1 (en) 2010-08-18

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Granted publication date: 20140820

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