CN101787326A - 一种复合磺酸钙润滑脂及其制备方法 - Google Patents
一种复合磺酸钙润滑脂及其制备方法 Download PDFInfo
- Publication number
- CN101787326A CN101787326A CN201010105181A CN201010105181A CN101787326A CN 101787326 A CN101787326 A CN 101787326A CN 201010105181 A CN201010105181 A CN 201010105181A CN 201010105181 A CN201010105181 A CN 201010105181A CN 101787326 A CN101787326 A CN 101787326A
- Authority
- CN
- China
- Prior art keywords
- lubricating grease
- calcium
- grease lubricant
- base oil
- calcium sulfonate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000004519 grease Substances 0.000 title claims abstract description 57
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 title claims abstract description 36
- 239000011575 calcium Substances 0.000 title claims abstract description 36
- 229910052791 calcium Inorganic materials 0.000 title claims abstract description 36
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 title claims abstract description 27
- 239000000314 lubricant Substances 0.000 title claims abstract description 24
- 239000002131 composite material Substances 0.000 title claims abstract description 23
- 238000002360 preparation method Methods 0.000 title claims abstract description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 21
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims abstract description 20
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims abstract description 20
- 239000002199 base oil Substances 0.000 claims abstract description 20
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000004327 boric acid Substances 0.000 claims abstract description 16
- 238000003756 stirring Methods 0.000 claims abstract description 15
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 claims abstract description 12
- 239000000920 calcium hydroxide Substances 0.000 claims abstract description 12
- 229910001861 calcium hydroxide Inorganic materials 0.000 claims abstract description 12
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims abstract description 10
- 229910000019 calcium carbonate Inorganic materials 0.000 claims abstract description 10
- 229910021532 Calcite Inorganic materials 0.000 claims abstract description 8
- 235000014113 dietary fatty acids Nutrition 0.000 claims abstract description 7
- 239000000194 fatty acid Substances 0.000 claims abstract description 7
- 229930195729 fatty acid Natural products 0.000 claims abstract description 7
- 238000007872 degassing Methods 0.000 claims abstract description 6
- 230000001050 lubricating effect Effects 0.000 claims description 33
- 238000010792 warming Methods 0.000 claims description 8
- -1 hydroxy fatty acid Chemical class 0.000 claims description 7
- 238000012360 testing method Methods 0.000 claims description 7
- 239000000725 suspension Substances 0.000 claims description 5
- 239000002994 raw material Substances 0.000 claims description 4
- 238000005033 Fourier transform infrared spectroscopy Methods 0.000 claims description 3
- 238000010521 absorption reaction Methods 0.000 claims description 3
- 239000007864 aqueous solution Substances 0.000 claims description 3
- 238000006073 displacement reaction Methods 0.000 claims description 3
- 239000002480 mineral oil Substances 0.000 claims description 3
- 235000010446 mineral oil Nutrition 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 3
- 239000003921 oil Substances 0.000 claims description 3
- 239000002562 thickening agent Substances 0.000 claims description 3
- 238000000034 method Methods 0.000 abstract description 20
- 238000005516 engineering process Methods 0.000 abstract description 9
- 239000003795 chemical substances by application Substances 0.000 abstract description 8
- 230000001131 transforming effect Effects 0.000 abstract description 7
- 239000013078 crystal Substances 0.000 abstract description 5
- 238000010438 heat treatment Methods 0.000 abstract description 4
- 230000008901 benefit Effects 0.000 abstract description 2
- 239000003513 alkali Substances 0.000 abstract 1
- 239000002585 base Substances 0.000 abstract 1
- 239000004615 ingredient Substances 0.000 abstract 1
- 238000002156 mixing Methods 0.000 abstract 1
- 238000013096 assay test Methods 0.000 description 4
- 230000015572 biosynthetic process Effects 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 2
- 239000004990 Smectic liquid crystal Substances 0.000 description 2
- FYHXNYLLNIKZMR-UHFFFAOYSA-N calcium;carbonic acid Chemical compound [Ca].OC(O)=O FYHXNYLLNIKZMR-UHFFFAOYSA-N 0.000 description 2
- 239000000084 colloidal system Substances 0.000 description 2
- 229910052802 copper Inorganic materials 0.000 description 2
- 239000010949 copper Substances 0.000 description 2
- 230000007797 corrosion Effects 0.000 description 2
- 238000005260 corrosion Methods 0.000 description 2
- VLHZUYUOEGBBJB-UHFFFAOYSA-N hydroxy stearic acid Natural products OCCCCCCCCCCCCCCCCCC(O)=O VLHZUYUOEGBBJB-UHFFFAOYSA-N 0.000 description 2
- 235000012204 lemonade/lime carbonate Nutrition 0.000 description 2
- 230000007774 longterm Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 230000009466 transformation Effects 0.000 description 2
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 238000013329 compounding Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000004567 concrete Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000003628 erosive effect Effects 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 230000008676 import Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 230000002335 preservative effect Effects 0.000 description 1
- 238000005245 sintering Methods 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
Landscapes
- Lubricants (AREA)
Abstract
Description
项目 | 检验结果 | 试验方法 |
工作锥入度,1/10mm | 276 | GB/T269 |
滴点,℃ | 330 | GB/T3498 |
延长工作锥入度(10万次),1/10mm | 279 | GB/T269 |
滚筒试验(25℃),0h | 65 | - |
2h | 66 | SH/T0122 |
加水10%,2h | 66 | SH/T0122 |
项目 | 检验结果 | 试验方法 |
腐蚀(T2铜片,100℃,24h) | 合格 | GB/T7326(乙法) |
钢网分油(100,30h) | 0.94 | SH/T0324 |
抗水淋(38℃,1h) | 0.85 | SH/T0109 |
四球试验PB Kg | 120 | GB/T3142 |
PD Kg | 620 | GB/T3142 |
项目 | 检验结果 | 试验方法 |
工作锥入度,1/10mm | 306 | GB/T269 |
滴点,℃ | 330 | GB/T3498 |
延长工作锥入度(10万次),1/10mm | 310 | GB/T269 |
滚筒试验(25℃),0h | 71 | - |
2h | 75 | SH/T0122 |
项目 | 检验结果 | 试验方法 |
加水10%,2h | 71 | SH/T0122 |
腐蚀(T2铜片,100℃,24h) | 合格 | GB/T7326(乙法) |
钢网分油(100,24h) | 0.9 | SH/T0324 |
抗水淋(38℃,1h) | 0.87 | SH/T0109 |
四球试验PB Kg | 120 | GB/T3142 |
PD Kg | 620 | GB/T3142 |
Claims (4)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN 201010105181 CN101787326B (zh) | 2010-02-03 | 2010-02-03 | 一种复合磺酸钙润滑脂及其制备方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN 201010105181 CN101787326B (zh) | 2010-02-03 | 2010-02-03 | 一种复合磺酸钙润滑脂及其制备方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN101787326A true CN101787326A (zh) | 2010-07-28 |
CN101787326B CN101787326B (zh) | 2013-01-16 |
Family
ID=42530708
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN 201010105181 Active CN101787326B (zh) | 2010-02-03 | 2010-02-03 | 一种复合磺酸钙润滑脂及其制备方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN101787326B (zh) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104024162A (zh) * | 2011-10-31 | 2014-09-03 | Nch公司 | 羟基磷灰石钙基磺酸钙油脂组合物及其制备方法 |
EP3458557A4 (en) * | 2016-05-18 | 2019-06-26 | NCH Corporation | COMPOSITION AND PROCESS FOR PRODUCING MAGNESIUM SULFONATE FAT AND CALCIUM WITHOUT CLASSIC NONAQUEOUS CONVERSION AGENT |
CN115181599A (zh) * | 2021-09-28 | 2022-10-14 | 福斯润滑油(中国)有限公司 | 一种低温复合磺酸钙润滑脂组合物及其制备方法 |
Family Cites Families (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5126062A (en) * | 1991-01-15 | 1992-06-30 | Nch Corporation | Calcium sulfonate grease and method of manufacture |
CN100358984C (zh) * | 2005-08-05 | 2008-01-02 | 鞍山海华油脂化学有限公司 | 复合磺酸钙润滑脂 |
CN101319164A (zh) * | 2008-07-18 | 2008-12-10 | 杭州得润宝油脂有限公司 | 一种复合磺酸钙润滑脂及其制备方法 |
-
2010
- 2010-02-03 CN CN 201010105181 patent/CN101787326B/zh active Active
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104024162A (zh) * | 2011-10-31 | 2014-09-03 | Nch公司 | 羟基磷灰石钙基磺酸钙油脂组合物及其制备方法 |
CN104024162B (zh) * | 2011-10-31 | 2017-11-28 | Nch公司 | 羟基磷灰石钙基磺酸钙油脂组合物及其制备方法 |
EP3458557A4 (en) * | 2016-05-18 | 2019-06-26 | NCH Corporation | COMPOSITION AND PROCESS FOR PRODUCING MAGNESIUM SULFONATE FAT AND CALCIUM WITHOUT CLASSIC NONAQUEOUS CONVERSION AGENT |
CN115181599A (zh) * | 2021-09-28 | 2022-10-14 | 福斯润滑油(中国)有限公司 | 一种低温复合磺酸钙润滑脂组合物及其制备方法 |
Also Published As
Publication number | Publication date |
---|---|
CN101787326B (zh) | 2013-01-16 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN101319164A (zh) | 一种复合磺酸钙润滑脂及其制备方法 | |
CN103740435B (zh) | 一种复合磺酸钙润滑脂组合物及其制备方法 | |
CN101792689B (zh) | 一种高性能复合锂钙基润滑脂组合物及其制备方法 | |
CN102977979B (zh) | 一种复合锂钙基润滑脂及其制备方法 | |
CN100395321C (zh) | 一种复合磺酸钙润滑脂及其制备方法 | |
CN102618371A (zh) | 高滴点钢丝绳脂及其制备方法 | |
CN101993767A (zh) | 一种含纳米碳酸钙的复合磺酸钙润滑脂及其生产方法 | |
CN101787326B (zh) | 一种复合磺酸钙润滑脂及其制备方法 | |
CN106350162B (zh) | 一种螺杆空压机润滑油氧化抑制组合物及其制备方法 | |
CN103952215A (zh) | 一种高性能复合磺酸钙基润滑脂及其制备方法 | |
CN102268323A (zh) | 一种复合磺酸钙基润滑脂及其制备方法 | |
CN104711080B (zh) | 改性复合磺酸钙润滑脂及其制备方法 | |
CN108546584B (zh) | 一种具有抗水性的钠-钙基润滑脂及其制备方法 | |
CN102703185B (zh) | 一种复合磺酸钙基润滑脂及其制备方法 | |
CN104498165A (zh) | 一种用于热轧无缝钢管的水基石墨润滑剂及其制备方法 | |
CN100404655C (zh) | 复合锂基润滑脂及其制备方法 | |
CN108165356B (zh) | 采棉机摘锭润滑脂及其制备方法 | |
CN104312665B (zh) | 一种双复合锂基润滑脂及其制备方法 | |
CN102899134A (zh) | 食品级复合磺酸钙基润滑脂的组合物及制备方法 | |
CN106316446A (zh) | 一种高强度耐高温的合金水泥顶头尖 | |
CN102703176B (zh) | 减速机防漏润滑剂 | |
CN101619260B (zh) | 一种高剪切安定性锂基润滑脂的制备方法 | |
CN101921647A (zh) | 一种复合磺酸钙基润滑脂及其制备方法 | |
CN102989996B (zh) | 一种精密铸造用脱模剂的制备方法 | |
CN101619256B (zh) | 一种轧钢机主联轴器专用润滑脂及其制备方法 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
C56 | Change in the name or address of the patentee |
Owner name: SHANGHAI HITECRUN SPECIALTY LUBRICATION TECHNOLOGY Free format text: FORMER NAME: SHANGHAI HITECRUN SPECIALTY LUBRICANTS CO., LTD. |
|
CP01 | Change in the name or title of a patent holder |
Address after: 200331 No. 358, Dunhuang Road, Shanghai, Putuo District Patentee after: SHANGHAI HITECRUN SPECIAL LUBRICATE SCIENCE & TECHNOLOGY CO.,LTD. Address before: 200331 No. 358, Dunhuang Road, Shanghai, Putuo District Patentee before: SHANGHAI HITECRUN SPECIALTY LUBRICATION TECHNOLOGY Co.,Ltd. |
|
DD01 | Delivery of document by public notice |
Addressee: SHANGHAI HITECRUN SPECIAL LUBRICATE SCIENCE & TECHNOLOGY CO.,LTD. Person in charge of patents Document name: payment instructions |