CN101747164B - 制备甲醛水溶液的方法 - Google Patents
制备甲醛水溶液的方法 Download PDFInfo
- Publication number
- CN101747164B CN101747164B CN200910247179.XA CN200910247179A CN101747164B CN 101747164 B CN101747164 B CN 101747164B CN 200910247179 A CN200910247179 A CN 200910247179A CN 101747164 B CN101747164 B CN 101747164B
- Authority
- CN
- China
- Prior art keywords
- formaldehyde
- content
- formalin
- solution
- weight
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
- C07C45/29—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation of hydroxy groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C47/00—Compounds having —CHO groups
- C07C47/02—Saturated compounds having —CHO groups bound to acyclic carbon atoms or to hydrogen
- C07C47/04—Formaldehyde
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
- G01N21/25—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
- G01N21/31—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
- G01N21/3103—Atomic absorption analysis
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Spectroscopy & Molecular Physics (AREA)
- General Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Investigating Or Analysing Materials By Optical Means (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
- Investigating, Analyzing Materials By Fluorescence Or Luminescence (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102008059701.5 | 2008-11-29 | ||
| DE102008059701A DE102008059701A1 (de) | 2008-11-29 | 2008-11-29 | Verfahren zur Herstellung von wässrigen Formaldehyd-Lösungen |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101747164A CN101747164A (zh) | 2010-06-23 |
| CN101747164B true CN101747164B (zh) | 2014-06-18 |
Family
ID=41809154
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN200910247179.XA Expired - Fee Related CN101747164B (zh) | 2008-11-29 | 2009-11-27 | 制备甲醛水溶液的方法 |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US20100137450A1 (https=) |
| EP (1) | EP2192102B1 (https=) |
| JP (1) | JP5710120B2 (https=) |
| KR (1) | KR101758368B1 (https=) |
| CN (1) | CN101747164B (https=) |
| DE (1) | DE102008059701A1 (https=) |
| DK (1) | DK2192102T3 (https=) |
| ES (1) | ES2446933T3 (https=) |
| PL (1) | PL2192102T3 (https=) |
| PT (1) | PT2192102E (https=) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102010040923A1 (de) | 2010-09-16 | 2012-03-22 | Basf Se | Verfahren zur Herstellung von Acrylsäure aus Ethanol und Formaldehyd |
| US9423801B2 (en) | 2010-12-22 | 2016-08-23 | Colgate-Palmolive Company | Continuous manufacturing system |
| WO2014031678A1 (en) * | 2012-08-20 | 2014-02-27 | Sabic Innovative Plastics Ip B.V. | Real-time online determination of caustic in process scrubbers using near infrared spectroscopy and chemometrics |
| KR101959104B1 (ko) | 2015-09-21 | 2019-03-15 | 유병현 | 타일 갭의 줄눈용 조성물 및 이를 이용한 타일 갭의 줄눈 시공방법 |
| US11365128B2 (en) * | 2017-06-15 | 2022-06-21 | Energysource Minerals Llc | Process for selective adsorption and recovery of lithium from natural and synthetic brines |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4594457A (en) * | 1984-04-12 | 1986-06-10 | Mitsubishi Gas Chemical Company, Inc. | Process for producing aqueous formaldehyde solution |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2444586C3 (de) * | 1974-09-18 | 1986-07-10 | Basf Ag, 6700 Ludwigshafen | Verfahren zur Herstellung von konzentrierten, wäßrigen Lösungen von Formaldehyd |
| JPH0629204B2 (ja) * | 1984-09-28 | 1994-04-20 | 三井東圧化学株式会社 | 高濃度ホルマリンの製造方法 |
| JP2649667B2 (ja) * | 1990-06-28 | 1997-09-03 | 株式会社堀場製作所 | 分光分析における多成分分析方法 |
| JPH08301793A (ja) * | 1995-05-01 | 1996-11-19 | Asahi Chem Ind Co Ltd | 近赤外線による反応制御方法 |
| ES2103193B1 (es) * | 1995-05-16 | 1998-04-01 | Patentes Novedades Sa | Procedimiento para la preparacion en continuo de soluciones acuosas de formaldehido. |
| JPH09241202A (ja) * | 1996-03-08 | 1997-09-16 | Mitsui Toatsu Chem Inc | ホルムアルデヒド水溶液の製造方法 |
| JP2001174408A (ja) * | 1999-12-22 | 2001-06-29 | Firmware Technology Co Ltd | ホルムアルデヒドの測定方法および測定装置 |
| GB0031522D0 (en) | 2000-12-22 | 2001-02-07 | Enigma Nv | Use of NIR (near-infra red spectroscopy) in composite production |
| BR0302120A (pt) | 2003-06-24 | 2005-05-17 | Enigma Nv | Uso de nir (espectroscopia no infravermelho próximo) na produção de painel compósito |
| JP2006119945A (ja) * | 2004-10-22 | 2006-05-11 | Iwai Kikai Kogyo Co Ltd | 液体製品製造システム |
-
2008
- 2008-11-29 DE DE102008059701A patent/DE102008059701A1/de not_active Withdrawn
-
2009
- 2009-11-18 PT PT90143876T patent/PT2192102E/pt unknown
- 2009-11-18 PL PL09014387T patent/PL2192102T3/pl unknown
- 2009-11-18 DK DK09014387.6T patent/DK2192102T3/da active
- 2009-11-18 EP EP09014387.6A patent/EP2192102B1/de not_active Not-in-force
- 2009-11-18 ES ES09014387.6T patent/ES2446933T3/es active Active
- 2009-11-19 US US12/621,588 patent/US20100137450A1/en not_active Abandoned
- 2009-11-27 KR KR1020090115642A patent/KR101758368B1/ko not_active Expired - Fee Related
- 2009-11-27 CN CN200910247179.XA patent/CN101747164B/zh not_active Expired - Fee Related
- 2009-11-27 JP JP2009270303A patent/JP5710120B2/ja not_active Expired - Fee Related
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4594457A (en) * | 1984-04-12 | 1986-06-10 | Mitsubishi Gas Chemical Company, Inc. | Process for producing aqueous formaldehyde solution |
Non-Patent Citations (2)
| Title |
|---|
| A review of process near infrared spectroscopy:1980-1994;Jerry Workman, Jr;《J. Near Infrared Spectrosc.》;19931231(第1期);正文第1-2段 * |
| Jerry Workman, Jr.A review of process near infrared spectroscopy:1980-1994.《J. Near Infrared Spectrosc.》.1993,(第1期),第221页. |
Also Published As
| Publication number | Publication date |
|---|---|
| KR101758368B1 (ko) | 2017-07-14 |
| DE102008059701A1 (de) | 2010-06-02 |
| JP2010127942A (ja) | 2010-06-10 |
| ES2446933T3 (es) | 2014-03-10 |
| CN101747164A (zh) | 2010-06-23 |
| KR20100061615A (ko) | 2010-06-08 |
| EP2192102A1 (de) | 2010-06-02 |
| US20100137450A1 (en) | 2010-06-03 |
| EP2192102B1 (de) | 2013-12-25 |
| JP5710120B2 (ja) | 2015-04-30 |
| PL2192102T3 (pl) | 2014-05-30 |
| DK2192102T3 (da) | 2014-03-31 |
| PT2192102E (pt) | 2014-02-21 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101747164B (zh) | 制备甲醛水溶液的方法 | |
| Cervera-Padrell et al. | Monitoring and control of a continuous Grignard reaction for the synthesis of an active pharmaceutical ingredient intermediate using inline NIR spectroscopy | |
| JP2004502747A (ja) | 酢酸製造のプロセスコントロール | |
| Shee et al. | Kinetic parameter estimation for supported vanadium oxide catalysts for propane ODH reaction: Effect of loading and support | |
| RU2585614C2 (ru) | Способ получения винилацетата | |
| Blanco et al. | Monitoring alcoholic fermentation by joint use of soft and hard modelling methods | |
| Chen et al. | In situ monitoring of heterogeneous hydrosilylation reactions using infrared and Raman spectroscopy: normalization using phase-specific internal standards | |
| CA2432605A1 (en) | Use of nir (near-infrared spectroscopy) in composite panel production | |
| CN116804658B (zh) | 三羟甲基丙烷合成产物tmp及其副产物的近红外光谱在线定量模型建立方法及应用 | |
| EP2893322A1 (en) | Real-time online determination of caustic in process scrubbers using near infrared spectroscopy and chemometrics | |
| CN107356556A (zh) | 一种近红外光谱定量分析的双集成建模方法 | |
| Zyuzin et al. | Kinetics of methoxy-NNO-Azoxymethane hydrolysis in strong acids | |
| CN106470969A (zh) | 酯的制造方法和酯的制造装置 | |
| CN101173952B (zh) | 一种确定对羧基苯甲醛含量的软测量方法 | |
| JP2000063352A (ja) | 芳香族アルキルヒドロペルオキシドの製造方法 | |
| CN113552091A (zh) | 一种高纯度2,6-二甲酚近红外光谱在线检测方法 | |
| Rodrigues et al. | Mid‐infrared spectroscopy as a tool for real‐time monitoring of ethanol absorption in glycols | |
| JP2003340270A (ja) | 反応器の運転制御方法 | |
| KR20170041834A (ko) | 알킬방향족 탄화수소의 하이드로퍼옥사이드의 개열 제어 방법 | |
| JP7830474B2 (ja) | センサ(s)によって閉ループ制御される少なくとも1つの制御ユニットを使用してアルコールを(メタ)アクリル酸と反応させることによる(メタ)アクリレートの連続調製のためのプロセス | |
| Rosenberger et al. | Spectrophotometric Determination of Stabilized Diszonium Compounds | |
| Paul | Raman spectroscopy for online monitoring of a homogeneous hydroformylation process in microemulsion | |
| Baffelli et al. | Quantitative Analysis of Atom Economy Using Reaction SMILES: A Computational Approach | |
| IT202000002104A1 (it) | Metodo per la determinazione della composizione di reflui e liquami da allevamento animale o da digestione anaerobica | |
| CN119213296A (zh) | 改进冰乙酸工艺控制的方法 |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C53 | Correction of patent of invention or patent application | ||
| CB02 | Change of applicant information |
Address after: Germany Leverkusen Applicant after: BAYER MATERIALSCIENCE AG Address before: Germany Leverkusen Applicant before: BAYER MATERIALSCIENCE AG |
|
| COR | Change of bibliographic data |
Free format text: CORRECT: APPLICANT; FROM: BAYER AG TO: CARCOUSTICS TECHCONSULT GMBH |
|
| EE01 | Entry into force of recordation of patent licensing contract |
Application publication date: 20100623 Assignee: Bayer Intellectual Property GmbH Assignor: BAYER MATERIALSCIENCE AG Contract record no.: 2012990000854 Denomination of invention: Method for preparing formalin License type: Common License Record date: 20121128 |
|
| LICC | Enforcement, change and cancellation of record of contracts on the licence for exploitation of a patent or utility model | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C41 | Transfer of patent application or patent right or utility model | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20160615 Address after: German Monheim Patentee after: BAYER INTELLECTUAL PROPERTY GmbH Address before: Germany Leverkusen Patentee before: BAYER MATERIALSCIENCE AG Effective date of registration: 20160615 Address after: Germany Leverkusen Patentee after: COVESTRO DEUTSCHLAND AG Address before: German Monheim Patentee before: BAYER INTELLECTUAL PROPERTY GmbH |
|
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20140618 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |