CN101693683B - 一种从普通叶黄素浸膏中制备高纯度叶黄素浸膏的方法 - Google Patents

一种从普通叶黄素浸膏中制备高纯度叶黄素浸膏的方法 Download PDF

Info

Publication number
CN101693683B
CN101693683B CN2009100756037A CN200910075603A CN101693683B CN 101693683 B CN101693683 B CN 101693683B CN 2009100756037 A CN2009100756037 A CN 2009100756037A CN 200910075603 A CN200910075603 A CN 200910075603A CN 101693683 B CN101693683 B CN 101693683B
Authority
CN
China
Prior art keywords
lutein extract
lutein
extract
purity
common
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN2009100756037A
Other languages
English (en)
Other versions
CN101693683A (zh
Inventor
张志忠
张为其
张建光
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
HEBEI ZHONGJIN BIOTECH CO., LTD.
Original Assignee
HANDAN ZHONGJIN NATURAL PIGMENT CO Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by HANDAN ZHONGJIN NATURAL PIGMENT CO Ltd filed Critical HANDAN ZHONGJIN NATURAL PIGMENT CO Ltd
Priority to CN2009100756037A priority Critical patent/CN101693683B/zh
Publication of CN101693683A publication Critical patent/CN101693683A/zh
Application granted granted Critical
Publication of CN101693683B publication Critical patent/CN101693683B/zh
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/54—Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids

Landscapes

  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Extraction Or Liquid Replacement (AREA)

Abstract

一种从普通叶黄素浸膏中制备高纯度叶黄素浸膏的方法，其特征在于：其工艺步骤为：①将 6.5 ㎏ 的 叶黄素浸膏一次性 装入超临界萃取罐，②在装罐过程中用 120 目不锈钢过滤网 进行过滤，③在 压力为 28MPa 、温度为 50 ℃的工艺条件下 将装入超临界萃取罐的 叶黄素浸膏用 CO 2 萃取 3-4 小时 ，④将萃取出的 叶黄素浸膏 用 120 目不锈钢过滤网 再过滤，⑤在 压力为 7MPa 、温度为 45 ℃的 工艺参数下将杂质与 叶黄素浸膏 分离即得高纯度 叶黄素浸膏 。是一种从普通叶黄素浸膏中制备高纯度叶黄素浸膏的方法。 本发明方法生产的叶黄素浸膏祛除了人体不可吸收的杂质，易吸收。本发明方法生产的叶黄素浸膏不但纯度高，而且从原料到成品的出素率高，出素率为 92% 。

Description

一种从普通叶黄素浸膏中制备高纯度叶黄素浸膏的方法
技术领域
本发明涉及一种叶黄素浸膏的生产方法，尤其是一种从普通叶黄素浸膏中制备高纯度叶黄素浸膏的方法，主要应用于食品着色、医药、保健品和高级化妆品等。
背景技术
目前，在食品、医药、保健品和高级化妆品中使用叶黄素浸膏由于纯度低，人体不能充分吸收。因此，研究一种从普通叶黄素浸膏中制备高纯度叶黄素浸膏的方法，是目前需要解决的技术问题。
发明内容
本发明所要解决的技术问题是提供一种从普通叶黄素浸膏中制备高纯度叶黄素浸膏的方法。
本发明解决其技术问题的技术方案是：
一种从普通叶黄素浸膏中制备高纯度叶黄素浸膏的方法，其工艺步骤为：①将一定量的叶黄素浸膏装入超临界萃取罐，②在装罐过程中进行过滤，③在一定工艺参数下将装入超临界萃取罐的叶黄素浸膏用CO2萃取，④将萃取出的叶黄素浸膏再过滤，⑤在一定工艺参数下将杂质与叶黄素浸膏分离即得高纯度叶黄素浸膏。
本发明解决其技术问题的技术方案还可以是：
本发明一次生产向超临界萃取罐中装入的叶黄素浸膏的量为6.5kg。
本发明所述的过滤为用120目不锈钢过滤网进行过滤。
本发明所述的超临界萃取工艺参数为萃取过程中的压力为28Mpa，温度为50℃，萃取时间为3-4小时。
本发明所述的分离过程的工艺参数为压力为7Mpa、温度为45℃。
本发明的有益效果是：
与现有技术相比，本发明方法生产的叶黄素浸膏祛除了人体不可吸收的杂质，易吸收。本发明方法生产的叶黄素浸膏不但纯度高，而且从原料到成品的出素率高，出素率为92％。
附图说明
附图是本发明的工艺过程图。
具体实施方式
一种从普通叶黄素浸膏中制备高纯度叶黄素浸膏的方法，其工艺步骤为：①将一定量的叶黄素浸膏装入超临界萃取罐，②在装罐过程中进行过滤，③在一定工艺参数下将装入超临界萃取罐的叶黄素浸膏萃取，④将萃取出的叶黄素浸膏再过滤，⑤在一定工艺参数下将杂质与叶黄素浸膏分离即得高纯度叶黄素浸膏。
一次生产向超临界萃取罐中装入的叶黄素浸膏的量为6.5kg。
所述的过滤为用120目不锈钢过滤网进行过滤。
所述的超临界萃取工艺参数为萃取过程中的压力为28Mpa，温度为50℃，萃取时间为3-4小时。
本发明所述的分离过程的工艺参数为压力为7Mpa、温度为45℃。

Claims (1)

1.一种从普通叶黄素浸膏中制备高纯度叶黄素浸膏的方法，其特征在于：其工艺步骤为：①将6.5㎏的叶黄素浸膏一次性装入超临界萃取罐，②在装罐过程中用120目不锈钢过滤网进行过滤，③在压力为28Mpa、温度为50℃的工艺条件下将装入超临界萃取罐的叶黄素浸膏用CO2萃取3-4小时，④将萃取出的叶黄素浸膏用120目不锈钢过滤网再过滤，⑤在压力为7Mpa、温度为45℃的工艺参数下将杂质与叶黄素浸膏分离即得高纯度叶黄素浸膏。
CN2009100756037A 2009-09-26 2009-09-26 一种从普通叶黄素浸膏中制备高纯度叶黄素浸膏的方法 Expired - Fee Related CN101693683B (zh)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2009100756037A CN101693683B (zh) 2009-09-26 2009-09-26 一种从普通叶黄素浸膏中制备高纯度叶黄素浸膏的方法

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2009100756037A CN101693683B (zh) 2009-09-26 2009-09-26 一种从普通叶黄素浸膏中制备高纯度叶黄素浸膏的方法

Publications (2)

Publication Number Publication Date
CN101693683A CN101693683A (zh) 2010-04-14
CN101693683B true CN101693683B (zh) 2012-06-27

Family

ID=42092695

Family Applications (1)

Application Number Title Priority Date Filing Date
CN2009100756037A Expired - Fee Related CN101693683B (zh) 2009-09-26 2009-09-26 一种从普通叶黄素浸膏中制备高纯度叶黄素浸膏的方法

Country Status (1)

Country Link
CN (1) CN101693683B (zh)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102659653B (zh) * 2012-05-05 2013-11-06 邯郸市中进天然色素有限公司 一种叶黄素浸膏到高纯度叶黄素酯的纯化方法
CN102757372B (zh) * 2012-07-31 2014-07-30 云南宏绿辣素有限公司 一种制备食品级叶黄素酯的方法

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1364831A (zh) * 2002-02-06 2002-08-21 中国科学院山西煤炭化学研究所 用超临界二氧化碳从万寿菊花提取叶黄素的方法
CN1800325A (zh) * 2006-01-10 2006-07-12 中国农业大学 万寿菊中叶黄素的超临界co2萃取方法

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1364831A (zh) * 2002-02-06 2002-08-21 中国科学院山西煤炭化学研究所 用超临界二氧化碳从万寿菊花提取叶黄素的方法
CN1800325A (zh) * 2006-01-10 2006-07-12 中国农业大学 万寿菊中叶黄素的超临界co2萃取方法

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
张德权等.叶黄素的超临界CO2流体萃取与精制.《食品超临界CO2流体加工技术》.2005, *
马清香等.超临界CO_2萃取万寿菊花中叶黄素的研究.《农业工程学报》.2007,第23卷(第8期), *

Also Published As

Publication number Publication date
CN101693683A (zh) 2010-04-14

Similar Documents

Publication Publication Date Title
CN103073915A (zh) 一种生物酶处理提取分离辣椒红色素和辣椒碱的工艺
CN105038948A (zh) 一种葡萄籽油的超临界萃取方法
CN101693683B (zh) 一种从普通叶黄素浸膏中制备高纯度叶黄素浸膏的方法
CN103285063A (zh) 一种金银花提取物的制备方法
CN104046511B (zh) 提高亚麻籽油品质的亚麻籽油制备方法
CN104531344A (zh) 一种核桃油的生产方法
CN103333740A (zh) 一种亚麻籽油及其超临界co2萃取方法
CN101693859A (zh) 一种从啤酒花中制备高纯度啤酒花浸膏的方法
CN103657170A (zh) 一种加压过滤装置
CN102994219A (zh) 黄粉虫油超临界萃取工艺
CN103937610A (zh) 一种精油的提取工艺
CN102558252A (zh) 一种亚麻木酚素的生产工艺
CN105037133B (zh) 一种从蒜头果中提取神经酸的方法
CN103288902A (zh) 一种从淫羊藿中提取淫羊藿苷的制备方法
CN101693785B (zh) 一种从普通辣椒红色素中制备高纯度辣椒红色素的方法
CN102408368A (zh) 一种由金盏菊提取物制备叶黄素的方法
CN104017653A (zh) 一种葛根精油的超临界二氧化碳萃取方法
CN100999461A (zh) 八角莽草酸提取分离技术
CN106350220A (zh) 利用洋甘菊提取精油的方法
WO2017185281A1 (zh) 一种贝母花提取物的制备方法
CN101822785A (zh) 一种提取玉米甾醇的方法
CN103937608A (zh) 一种用柑橘类果皮制作精油的工艺
CN105524035A (zh) 一种桑葚花青素的制造方法
CN103584046A (zh) 花椒麻素的制备方法
CN111110761A (zh) 一种牡荆油提取方法

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
ASS Succession or assignment of patent right

Owner name: HANDAN ZHONGJIN NATURAL PIGMENT CO., LTD.

Free format text: FORMER OWNER: MAKER (HEBEI) BIO-TECHNOLOGY CO., LTD.

Effective date: 20110621

C41 Transfer of patent application or patent right or utility model
COR Change of bibliographic data

Free format text: CORRECT: ADDRESS; FROM: 056002 NO. 2, 28/F, TOWER B, INTERNATIONAL TRADE CENTER, NO. 208, RENMIN ROAD, HANDAN CITY, HEBEI PROVINCE TO: 056107 NORTH OF WEST HEAD-END OF CHUANGYE ROAD, EAST AREA OF DEVELOPMENT ZONE, HANDAN CITY, HEBEI PROVINCE

TA01 Transfer of patent application right

Effective date of registration: 20110621

Address after: 056107, Hebei Handan Development Zone, East Road West Road heading north

Applicant after: Handan ZhongJin Natural Pigment Co., Ltd.

Address before: 056002 No. 28, No. 2, block B, China World Trade Center center, No. 208 Renmin Road, Hebei, Handan

Applicant before: Maker (Hebei) Bio-technology Co., Ltd.

C14 Grant of patent or utility model
GR01 Patent grant
C56 Change in the name or address of the patentee

Owner name: HEBEI ZHONGJIN BIOLOGICAL SCIENCE AND TECHNOLOGY C

Free format text: FORMER NAME: HANDAN ZHONGJIN NATURAL PIGMENT CO., LTD.

CP01 Change in the name or title of a patent holder

Address after: 056107, Hebei Handan Development Zone, East Road West Road heading north

Patentee after: HEBEI ZHONGJIN BIOTECH CO., LTD.

Address before: 056107, Hebei Handan Development Zone, East Road West Road heading north

Patentee before: Handan ZhongJin Natural Pigment Co., Ltd.

CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20120627

Termination date: 20160926