CN101669642A - Fruity sweet tea effervescent tablets and preparation method thereof - Google Patents
Fruity sweet tea effervescent tablets and preparation method thereof Download PDFInfo
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Abstract
The invention discloses fruity sweet tea effervescent tablets, comprising the following components: 5-12% of sweet tea powder, 10-18% of fruit extract, 2-5% of vitamin C, 22-30 %of a edible solid agent, 18-24% of organic acid, 20-28% of sodium bicarbonate, 0.5-2% of sodium chloride and 0.5-2% of lubricant. A preparation method comprises the following steps of mixing raw materials, granulating, drying, finishing granules, mixing granules, tabletting, sterilizing and packing and the like to obtain the fruity sweet tea effervescent tablets. The raw materials comprise the sweet tea and the fruit extracts containing rubusoside, various flavones and polyphenol, etc, and are matched with vitamin C without sugar, therefore the fruity sweet tea effervescent tablets are applicable to the children, the aged and the people who have diabetes, high blood pressure, obesity and like the low calorie food, and are taken conveniently, particularly as instant solid drinks by the cold water.
Description
Technical field
The present invention relates to a kind of health food and preparation method thereof, relate to a kind of Fruity sweet tea effervescent tablets and preparation method thereof in particular.
Background technology
Sweet tea (Rubus suavissimus S.Lee) is a kind of shrub plant of rose family four seasons growth, mainly be distributed in China southern hills area, main product Guangxi, usually grow in the mountain area of 500 meters～1000 meters of height above sea level, because its leaf flavor is sweet, with health role, so the Guangxi tea-drinking usefulness of often doing among the people is name " sweet tea ".Sweet tea, also as the sweetener processed food, also can be used as medicine except that using when tea-drinking among the people, and the effect of heat-clearing, moistening lung, detumescence, hemostasis and cough-relieving is arranged.In Japan, drink sweet tea and be widely used as the effective ways of preventing and treating pollinosis, Japanese scientific research personnel discovers, sweet tea has obvious curative effects to the control of pollen hypersensitivity and other rhinitis, dermatitis etc.The expert praises " the easiest acceptance of taste people of sweet tea is a kind of in the world novel senior sweet taste drink ".Guangxi Folium hydrangeae strigosae is a kind of natural sweet taste beverage, sweet, the delicate fragrance of its flavor, contain crude sweet tea glycosides and Polyphenols, amino acid, vitamin C, mineral matter and other components, have clearing heat and detoxicating, the effect of expelling phlegm and arresting coughing, hypertension, chaff urine disease and obesity patient's long-term drinking have the good health care effect, still are high-temperature operation person's ideal beverage simultaneously.In recent years, relevant scholar of state's year studies confirm that biology, the toxicology of Guangxi Folium hydrangeae strigosae, Guangxi Folium hydrangeae strigosae is a kind of high sugariness, avirulent plant, it is big that animal is taken safe range, production growth, hemopoietic system, hepatic and renal function are not had obstruction, and also not seeing has substantial infringement and accumulate poisoning reaction to main organs such as the animal heart, liver,spleen,kidney, brains, and producing sweet taste in the sweet tea mainly is sweet tea glycosides, be the tetracyclic diterpene glucoside of steviol and glucose be combined into, molecular formula C
22H
50O
12, the sugariness of glycosides is about more than 200 times of sucrose sweetness, is a kind of low heat value, sugariness height, edible very safe natural sweetener.
Hawthorn is the fruit of rose family May short, bristly hair or beard thing large-fruited Chinese hawthorn (Crataegus pinnatifida Bge.Major N.E.Br) and fructus crataegi pinnatifidae (C.Pinnatifida Bge), the little delicate fragrance of gas, and flavor acid is little sweet.Ground such as distribution Jiangsu, Zhejiang, Anhui, Hunan, Hubei, Henan, Sichuan, Guizhou, Jiangxi, Fujian, Guangdong, Guangxi, Yunnan, Shaanxi, contain epicatechin (epicatechin), Quercetin (quercetin), hyperin (hyperin), chlorogenic acid (chlorogenic acid), crataegolic acid (crataegolic acid), citric acid (citric acid), amygdalin (amygdalin), glucosidase procyanidins etc., every hectogram hawthorn contains nearly 89 milligrams of vitamin Cs, goes into spleen, stomach, Liver Channel.It is long-pending to help digestion, the hemostasis that looses, and expelling tenia is used to reduce serum ornitrol, effectively prevents and treats atherosclerotic, and it is obvious that antioxidation activity is measured the anti-aging effects that shows hawthorn.
Contain 15% carbohydrate, OPC and pectin in the apple, vitamin A, C, E, potassium and antioxidant equal size are also very abundant, and its calcium content is also abundant than general fruit, contains the mineral element boron and the manganese that can strengthen sclerotin in the apple.Polyphenol that apple is contained and Flavonoid substances are particularly important to the prevention cardiovascular and cerebrovascular disease.Soluble Fiber-pectin in the apple can reduce cholesterol effectively, after the pectin of apple enters human body, can combine with bile acid, absorbs unnecessary cholesterol and triglycerides, excretes then.Pectin and pectous food can promote the discharging of lead, mercury, manganese and beryllium in the intestines and stomach.Find in the test to enterocyte that the bacterium in the human body stomach can discharge a large amount of butyric acid under the effect of apple pectin or apple extract, butyric acid has inhibitory action to the growth of the multiple cancer cell in the human body stomach.
Effervescent tablet is to be a kind of tablet that disintegrant is made with suitable bronsted lowry acids and bases bronsted lowry, drops in the water and can produce a large amount of carbon dioxides, impels whole tablet to dissolve at short notice, the active ingredient onset is rapid, and the bioavilability height helps absorption of human body, compare with liquid preparation, carry more convenient.Sweet tea and apple or hawthorn etc. are made the crowd that effervescent tablet is particularly suitable for children, the elderly and likes low-calorie diet, can be used as a kind of novel solid beverage that is convenient for carrying and drink.
Summary of the invention
The object of the present invention is to provide a kind of is primary raw material with sweet tea of natural materials and fruit extract, the health products effervescent tablet that utilizes little effervescent tablet method to make.
Technical solution of the present invention
A kind of Fruity sweet tea effervescent tablets, the mass percent of its composition is as follows:
Sweet tea powder 5～12%
Fruit extract 10～18%
Vitamin C 2～5%
Edible shape-fixing agent 22～30%
Organic acid 18～24%
Sodium acid carbonate 20～28%,
Sodium chloride 0.5～2%,
Lubricant 0.5～2%
Described sweet tea powder is the sweet tea extract that sweet tea glycosides content is 40～90% mass fractions; Described sweet tea powder can substitute with the Fructus Monordicae extract powder that contains 30～80% Fructus Momordicae fructosides, the qualities of stevia extract that contains 40～90% rebaudiosides, and the preparation method is identical with sweet tea powder; Described fruit extract is oranges and tangerines powder, lemon powder, hawthorn powder, strawberry powder, blueberry powder, apple powder;
Described organic acid comprises citric acid, malic acid or tartaric acid;
Described sodium acid carbonate can substitute with sodium carbonate;
Described edible shape-fixing agent is converted starch, beta-schardinger dextrin-or maltodextrin;
Described lubricant is fumaric acid, dolomol or talcum powder.
A kind of Fruity sweet tea effervescent tablets, its preparation method comprises the steps:
(1), the preparation of raw material
(a), the preparation of fruit extract
With the fresh fruit is raw material, after fruit is cleaned, carries out break process; With 5～10 times of volume floodings twice, temperature is controlled to be 70～90 ℃ again, lixiviate 40～60min, and after lixiviate finished, it was 20～50% that leaching liquor is concentrated to solid content; Adopting microencapsulation technology to carry out spray-drying, is that the wall material adds in the concentrate with the edible shape-fixing agent of leaching liquor concentrate mass fraction 5～10%, and inlet temperature is 105～125 ℃, and outlet temperature is 80～90 ℃, fruity extract powder cooling back is standby;
(b), the preparation of sweet tea powder
With sweet tea prophyll is raw material, drying, remove debranching and stalk, pulverizing after, take by weighing the sweet tea sample and put into extraction vessel, distilled water with 8～15 times of volumes extracts it, be heated to 60～80 ℃, filter, go up chromatographic column then the extract purifying, the Choice of Resin of chromatographic column comprises macroreticular resin and polyamide, purification step:
1., in advance resin is carried out preliminary treatment, with the resin wet method dress post of handling well;
2., use deionized water rinsing, the preliminary treatment solvent is caught up with to the greatest extent, liquid level is higher than resin, keeps resin not dewater;
3., chromatographic column on the sweet tea stoste that will extract, applied sample amount is got 1～3% of weight resin in stoste solid content dry content;
4., colourless with washed with de-ionized water to flowing out liquid;
5., with 40%～80% ethanol elution, collection eluent;
6., collect liquid and concentrate, remove the second alcohol and water, being concentrated to solid content is 20～50%;
7., the concentrated collection liquid that will obtain carries out spray-drying, charging rate is 0.9～1.5L/h, inlet temperature is 105～130 ℃, outlet temperature is 75～90 ℃, the sweet tea powder cooling back that obtains is standby;
(c), vitamin C, edible shape-fixing agent, organic acid, sodium acid carbonate, sodium chloride, lubricant are the commercially available prod;
(2), batch mixing
The edible shape-fixing agent of the ready sodium acid carbonate of step (1), sodium chloride and 12% is carried out drying and crushing before batch mixing, and cross 40 mesh sieves, again through ultraviolet sterilization 10～20min, raw material is added one by one carry out batch mixing in the container then, mixing time is 20～40min, gets compound A;
Again the ready sweet tea powder of step (1), fruit extract, vitamin C, remaining edible shape-fixing agent, organic acid are carried out drying and crushing before batch mixing, and mistake 40 mesh sieves, again through ultraviolet sterilization 10～20min, then raw material is added one by one and carry out batch mixing in the container, mixing time is 20～40min, gets compound B;
(3), granulate
Mix 5～8% the water that adds its mixed material gross weight in back compound A of gained and the B material respectively to step (2), mix 10～15min, respectively the material of abundant mixing being put into granulator then granulates, the granulation screen cloth adopts 20～40 orders, obtains two kinds of particles of meta-alkalescence and slant acidity respectively;
(4), drying
To granulate through step (3), to put into temperature respectively be that 50～60 ℃ baking oven carries out drying for the meta-alkalescence of back gained and two kinds of particles of slant acidity, and raw material is paved into thick about 5～8mm, controls 30min drying time;
(5), whole grain and mixed grain
After step (4) the feed particles drying, take out cooling respectively, and meta-alkalescence and two kinds of particles of slant acidity are carried out whole grain through 20 orders and 40 mesh sieves respectively successively, add 0.5～2% lubricant then, two kinds of particles are mixed;
(6), compressing tablet
After (5) two kinds of particles of step are mixed, with the grinding tool of the cooperation of tablet press machine drift and bed die, material is put into tablet press machine carry out compressing tablet, pressure is 4-6kg, promptly gets compressing tablet;
(7), sterilization, packing
The compressing tablet of step (6) gained through ultraviolet sterilization, is packed between aseptic packaging, promptly got a kind of Fruity sweet tea effervescent tablets of the present invention.
Beneficial effect of the present invention
The present invention is raw materials used to be natural sweet tea and fruit extract, contains multiple natural materials such as sweet tea glycosides, multiple flavones, organic acid and vitamin C, allows to replenish the natural nutrient substance of needed by human body.This product preservative free is a sweetener with the sweet tea glycosides of high sugariness, does not add sugar, is applicable to crowds such as glycosuria disease, hypertension and obesity, also is fit to the crowd that children etc. suffer from carious tooth easily.Product of the present invention can be taken after mixing it with water with cold water with the effervescent tablet form, is equivalent to one glass of fruit drink after being dissolved in cold water, helps absorbing, and greatly facilitates simultaneously and carries, takes and transport.Effervescent tablet will help to reduce cost of transportation than liquid beverage.
Adopted microencapsulation technology during spray-dryings such as lemon powder, hawthorn powder, strawberry powder, apple powder or blueberry powder, edible shape-fixing agents such as interpolation cyclodextrin wrap up active ingredient, help the maintenance of fruit fragrance.Rise chip technology by microvesicle, the active ingredient of product is kept when edible has also kept the strong fragrant fragrance of a flower and fruital simultaneously.This product is on technology; the technical process and the parameter that help to protect nutritional labeling have been selected for use; the drying process with atomizing process is selected suitable wall material and use amount; its powder delivery exquisiteness; production cost is lower than Vacuum Freezing ﹠ Drying Technology, and does not destroy active ingredient in the raw material, has effectively protected the natural component of sweet tea and fruit; be real fruit juice beverage, but not existing effervescent tablet with the essence seasoning on the market.Adopt column chromatography technology when sweet tea extracts purifying, efficiently the sweet tea extract of sweet tea glycosides is rich in the preparation of fast and low-cost ground.It is moderate to be prepared into its disintegration rate of Fruity sweet tea effervescent tablets with this technology, and it is effective to bubble, and mouthfeel is good, nutritious and help absorption of human body.And cost of transportation is low.
The specific embodiment
Below by embodiment the present invention is described in further detail, but do not limit the present invention.
Embodiment 1
A kind of apple sweet tea effervescent tablets, its composition is as follows by mass percentage:
Sweet tea powder 8%
Apple extract 13%
Vitamin C 4%
Converted starch 26%
Citric acid 22%
Sodium acid carbonate 26%
Sodium chloride 0.5%
Fumaric acid 0.5%
The preparation method of described apple sweet tea effervescent tablets comprises the steps:
(1), feedstock production
(a), the preparation method of apple extract: choose apple after cleaning, protect look, lixiviate concentrates, and adds the wall material, and spray-drying obtains finished product.
1) raw material: with the green apple is raw material, takes by weighing apple 50g; After the fruit cleaning, carry out break process;
2) protect look:, add 0.4% citric acid and protect look in order to prevent apple generation brown stain;
3) lixiviate: with the lixiviate of 500mL distilled water, temperature is 75 ℃, and extraction time is that 40min is that condition is carried out twice lixiviate;
4) concentrate: after the filtration, with rotary evaporator leaching liquor being concentrated to solid content is 40%;
5) add the wall material: selecting mass fraction for use is that 8% beta-schardinger dextrin-adds in the concentrate;
6) spray-drying: inlet temperature is 110 ℃, and outlet temperature is 80 ℃, and charging rate is 1.2L/h;
7) the apple extract cooling back that obtains is standby;
(b), the preparation of sweet tea powder
1) raw material: the sweet tea with natural air drying is a raw material, takes by weighing sweet tea 50g;
2) extract: the extraction vessel with the sweet tea sample that weighs up is put into, with 600mL distilled water it is extracted, be heated to 80 ℃;
3) purifying: go up chromatographic column to the extract purifying, the Choice of Resin macroreticular resin of chromatographic column; In advance resin is carried out preliminary treatment,, use deionized water rinsing, the preliminary treatment etoh solvent is caught up with to the greatest extent the resin wet method handled well dress post, applied sample amount be column material resin dry weight 3% in, use 80% ethanol elution, collection eluent, filtration;
4) concentrate: after the filtration, with rotary evaporator leaching liquor being concentrated to solid content is 35%;
5) spray-drying: inlet temperature is 115 ℃, and outlet temperature is that 90 ℃ of charging rates are 1.2L/h;
6) the sweet tea powder cooling back that obtains is standby;
(2), batch mixing
The ready various raw materials of step (1) are carried out drying and crushing before batch mixing, and cross 40 mesh sieves, again through ultraviolet sterilization 15min, in proportion raw material is added one by one then and carry out batch mixing in the container, mixing time is 25min;
(3), granulate
Material after step (2) mixes adds 6% water of raw material gross weight, get sodium acid carbonate 26g, sodium chloride 0.5g, converted starch 10g mixes them, then the material of abundant mixing is put into that granulator is granulated, whole grain, get sweet tea powder 8g simultaneously, apple extract 13g, vitamin C 4g, converted starch 12.8g, citric acid 22g powder 10min puts into granulator with the material of abundant mixing then and granulates, and the granulation screen cloth adopts 20 orders; Obtain two kinds of particles of meta-alkalescence and slant acidity respectively;
(4), drying
To granulate through step (3), to put into temperature be that 50 ℃ baking oven carries out drying for the particle of back gained, raw material is paved into about 5mm thickness, the time 30min of drying;
(5), whole grain and mixed grain
After step (4) the feed particles drying, take out cooling, and meta-alkalescence and two kinds of particles of slant acidity are carried out whole grain through 20 orders and 40 mesh sieves respectively successively, add 0.5% fumaric acid then, two kinds of particles are mixed;
(6), compressing tablet
After (5) two kinds of particles of step are mixed, with the grinding tool of the cooperation of tablet press machine drift and bed die, material is put into tablet press machine carry out compressing tablet, pressure is 4kg;
(7), sterilization, packing
The compressing tablet of step (6) gained through ultraviolet sterilization 10min, is packed between aseptic packaging, promptly got a kind of apple sweet tea effervescent tablets of the present invention.
Embodiment 2
A kind of hawthorn sweet tea effervescent tablets, its composition is as follows by mass percentage:
Sweet tea powder 12%
Haw thorn extract 14%
Vitamin C 3%
Converted starch 26%
Tartaric acid 19%
Sodium acid carbonate 24%,
Sodium chloride 1%,
Fumaric acid 1%.
The preparation method of described hawthorn sweet tea effervescent tablets comprises the steps:
(1) raw material is prepared:
(a), the preparation method of haw thorn extract:
Choose hawthorn after cleaning, protect look, lixiviate concentrates, and adds the wall material, and spray-drying obtains finished product.
1) raw material: with the hawthorn fresh fruit is raw material, takes by weighing hawthorn 50g;
2) clean: after fruit is cleaned, carry out break process;
3) lixiviate: with the 400mL flooding, temperature is 70 ℃, and extraction time is that 60min is that condition is carried out twice lixiviate;
4) concentrate: after the filtration, with rotary evaporator leaching liquor being concentrated to solid content is 30%;
5) add the wall material: selecting mass fraction for use is that 8% beta-schardinger dextrin-adds in the concentrate;
6) spray-drying: inlet temperature is 110 ℃, and outlet temperature is 80 ℃, and charging rate is 1.0L/h;
7) haw thorn extract cooling back is standby;
(b), the preparation of sweet tea powder.
1) raw material: the sweet tea with natural air drying is a raw material, takes by weighing sweet tea 50g;
2) extract: the extraction vessel with the sweet tea sample that weighs up is put into, with 500mL distilled water it is extracted, be heated to 75 ℃;
3) purifying: go up chromatographic column to the extract purifying, the Choice of Resin polyamide of chromatographic column; In advance resin is carried out preliminary treatment,, use deionized water rinsing, the preliminary treatment etoh solvent is caught up with to the greatest extent the resin wet method handled well dress post, applied sample amount be column material resin dry weight 2% in, use 70% ethanol elution, collection eluent, filtration;
4) concentrate: after the filtration, with rotary evaporator leaching liquor being concentrated to solid content is 30%;
5) spray-drying: inlet temperature is 115 ℃, and outlet temperature is 85 ℃, and charging rate is 1.0L/h;
6) the sweet tea powder cooling back that obtains is standby;
(2), batch mixing
The ready various raw materials of step (1) are carried out drying and crushing before batch mixing, and cross 60 mesh sieves, again through ultraviolet sterilization 10min, in proportion raw material is added one by one then and carry out batch mixing in the container, mixing time is 30min;
(3), granulate
Material after step (2) mixes adds 5～8% water of raw material gross weight, to get sodium acid carbonate 24g, sodium chloride 1g, converted starch 10g mixes them, then the material of abundant mixing is put into that granulator is granulated, whole grain, get sweet tea powder 12g simultaneously, haw thorn extract 14g, vitamin C 3g, converted starch 13.6g, tartaric acid 19g powder 15min puts into granulator with the material of abundant mixing then and granulates, and the granulation screen cloth adopts 20～40 orders; Obtain two kinds of particles of meta-alkalescence and slant acidity respectively;
(4), drying
To granulate through step (3), to put into temperature be that 55 ℃ baking oven carries out drying for the particle of back gained, raw material is paved into about 7mm thickness, about the time 30min of drying, to prevent the citric acid thawing;
(5), whole grain and mixed grain
After step (4) the feed particles drying, take out cooling, and meta-alkalescence and two kinds of particles of slant acidity are carried out whole grain through 20 orders and 40 mesh sieves respectively successively, add 1% fumaric acid then, two kinds of particles are mixed;
(6), compressing tablet
After (5) two kinds of particles of step are mixed, with the grinding tool of the cooperation of tablet press machine drift and bed die, material is put into tablet press machine carry out compressing tablet, pressure is 5kg;
(7), sterilization, packing
The compressing tablet of step (6) gained through ultraviolet sterilization, is packed between aseptic packaging, promptly got a kind of hawthorn Fruity sweet tea effervescent tablets of the present invention.
Embodiment 3
A kind of Momordica grosvenori strawberry effervescent tablet, its composition is as follows by mass percentage:
Mangosteen powder 5%
Strawberry powder extract 18%
Vitamin C 3%
Converted starch 28%
Malic acid 22%
Sodium acid carbonate 22%,
Sodium chloride 1.5%,
Fumaric acid 0.5%.
The preparation method of described strawberry sweet tea effervescent tablets comprises the steps:
(1) raw material is prepared:
(a), the preparation method of Fragaia ananassa Duchesne extract:
Choose strawberry after cleaning, protect look, lixiviate concentrates, and adds the wall material, and spray-drying obtains finished product.
1) raw material: with the strawberry fresh fruit is raw material, takes by weighing strawberry 50g;
2) clean: after fruit is cleaned, carry out break process;
3) lixiviate: with the 400mL flooding, temperature is 75 ℃, and extraction time is that 50min is that condition is carried out twice lixiviate;
4) concentrate: after the filtration, with rotary evaporator leaching liquor being concentrated to solid content is 30%;
5) add the wall material: selecting mass fraction for use is that 9% beta-schardinger dextrin-adds in the concentrate;
6) spray-drying: inlet temperature is 110 ℃, and outlet temperature is 85 ℃, and charging rate is 1.0L/h;
7) Fragaia ananassa Duchesne extract cooling back is standby;
(b), the preparation of mangosteen powder.
1) raw material: the Momordica grosvenori with natural air drying is a raw material, takes by weighing Momordica grosvenori 50g;
2) extract: the extraction vessel with the Momordica grosvenori sample that weighs up is put into, with 500mL distilled water it is extracted, be heated to 75 ℃;
3) purifying: go up chromatographic column to the extract purifying, the Choice of Resin of chromatographic column is gathered macroreticular resin; In advance resin is carried out preliminary treatment,, use deionized water rinsing, the preliminary treatment etoh solvent is caught up with to the greatest extent the resin wet method handled well dress post, applied sample amount be column material resin dry weight 2% in, use 60% ethanol elution, collection eluent, filtration;
4) concentrate: after the filtration, with rotary evaporator leaching liquor being concentrated to solid content is 30%;
5) spray-drying: inlet temperature is 110 ℃, and outlet temperature is 80 ℃, and charging rate is 1.2L/h;
6) the sweet tea powder cooling back that obtains is standby;
(2), batch mixing
The ready various raw materials of step (1) are carried out drying and crushing before batch mixing, and cross 60 mesh sieves, again through ultraviolet sterilization 10min, in proportion raw material is added one by one then and carry out batch mixing in the container, mixing time is 30min;
(3), granulate
Material after step (2) mixes adds 5% water of raw material gross weight, to get sodium acid carbonate 22g, sodium chloride 1.5g, converted starch 11g mixes them, then the material of abundant mixing is put into that granulator is granulated, whole grain, get mangosteen powder 5g simultaneously, Fragaia ananassa Duchesne extract 18g, vitamin C 3g, converted starch 14.3g, malic acid 22g powder 12min puts into granulator with the material of abundant mixing then and granulates, and the granulation screen cloth adopts 20～40 orders; Obtain two kinds of particles of meta-alkalescence and slant acidity respectively;
(4), drying
Will be after step (3) be granulated the particle of gained to put into temperature be that 65 ℃ baking oven carries out drying, it is thick that raw material is paved into about 8mm, about dry 40min;
(5), whole grain and mixed grain
After step (4) the feed particles drying, take out cooling, and meta-alkalescence and two kinds of particles of slant acidity are carried out whole grain through 20 orders and 40 mesh sieves respectively successively, add 0.5% fumaric acid then, two kinds of particles are mixed;
(6), compressing tablet
After (5) two kinds of particles of step are mixed, with the grinding tool of the cooperation of tablet press machine drift and bed die, material is put into tablet press machine carry out compressing tablet, pressure is 6kg;
(7), sterilization, packing
The compressing tablet of step (6) gained through ultraviolet sterilization, is packed between aseptic packaging, promptly got a kind of Momordica grosvenori strawberry effervescent tablet of the present invention.
Described content only is the basic explanation of the present invention under conceiving, and according to any equivalent transformation that technical scheme of the present invention is done, all should belong to protection scope of the present invention.
Claims (9)
1, a kind of Fruity sweet tea effervescent tablets, proportioning is as follows by mass percentage to it is characterized in that its component:
Sweet tea powder 5～12%
Fruit extract 10～18%
Vitamin C 2～5%
Edible shape-fixing agent 22～30%
Organic acid 18～24%
Sodium acid carbonate 20～28%
Sodium chloride 0.5～2%
Lubricant 0.5～2%
2, Fruity sweet tea effervescent tablets according to claim 1 is characterized in that described fruit extract is oranges and tangerines powder, lemon powder, hawthorn powder, strawberry powder, blueberry powder or apple powder.
3, Fruity sweet tea effervescent tablets according to claim 1 is characterized in that described sweet tea powder is is that the sweet tea glycosides content that raw material extracts is the sweet tea extract of 40～90% mass fractions with the sweet tea.
4, Fruity sweet tea effervescent tablets according to claim 1 is characterized in that described sweet tea powder can substitute with Fructus Monordicae extract powder that contains 30～80% Fructus Momordicae fructosides or the qualities of stevia extract that contains 40～90% rebaudiosides.
5, Fruity sweet tea effervescent tablets according to claim 1 is characterized in that described organic acid is citric acid, malic acid or tartaric acid.
6, Fruity sweet tea effervescent tablets according to claim 1 is characterized in that described edible shape-fixing agent is converted starch, beta-schardinger dextrin-or maltodextrin.
7, Fruity sweet tea effervescent tablets according to claim 1 is characterized in that described lubricant is fumaric acid, dolomol or talcum powder.
8, Fruity sweet tea effervescent tablets as claimed in claim 1, but it is characterized in that described sodium acid carbonate substitutes with sodium carbonate.
9, a kind of as the described Fruity sweet tea effervescent tablets of the arbitrary claim of claim 1 to 8, it is characterized in that its preparation method comprises the steps:
(1), the preparation of raw material
(a), the preparation of fruit extract
With the fresh fruit is raw material, after fruit is cleaned, carries out break process; With 5～10 times of volume floodings twice, temperature is controlled to be 70～90 ℃, lixiviate 40～60min; After lixiviate finished, it was 20～50% that leaching liquor is concentrated to solid content; Edible shape-fixing agent with leaching liquor concentrate mass fraction 5～10% is that the wall material adds in the concentrate, carries out spray-drying, and inlet temperature is 105～125 ℃, and outlet temperature is 80～90 ℃, and the fruity extract powder cooling back that obtains is standby;
(b), the preparation of sweet tea powder
With sweet tea prophyll is raw material, drying, remove debranching and stalk, pulverizing after, take by weighing the sweet tea sample and put into extraction vessel, distilled water with 8～15 times of volumes extracts it, be heated to 60～80 ℃, filter, go up chromatographic column then the extract purifying, the Choice of Resin of chromatographic column comprises macroreticular resin and polyamide, purification step:
1., in advance resin is carried out preliminary treatment, with the resin wet method dress post of handling well;
2., water will wash, and the preliminary treatment solvent is caught up with to the greatest extent, liquid level is higher than resin, keeps resin not dewater;
3., chromatographic column on the sweet tea stoste that will extract, applied sample amount is got 1～3% of weight resin in stoste solid content dry content;
4., colourless with washed with de-ionized water to flowing out liquid;
5., with 40%～80% ethanol elution, collection eluent;
6., collect liquid and concentrate, remove the second alcohol and water, being concentrated to solid content is 20～50%;
7., the concentrated collection liquid that will obtain carries out spray-drying, charging rate is 0.9～1.5L/h, inlet temperature is 105～130 ℃, outlet temperature is 75～90 ℃, the sweet tea powder cooling back that obtains is standby;
(c), vitamin C, edible shape-fixing agent, organic acid, sodium acid carbonate, sodium chloride, lubricant are the commercially available prod;
(2), batch mixing
The edible shape-fixing agent of the ready sodium acid carbonate of step (1), sodium chloride and 12% is carried out drying and crushing before batch mixing, and cross 40 mesh sieves, again through ultraviolet sterilization 10～20min, raw material is added one by one carry out batch mixing in the container then, mixing time is 20～40min, gets compound A;
Again the ready sweet tea powder of step (1), fruit extract, vitamin C, remaining edible shape-fixing agent, organic acid are carried out drying and crushing before batch mixing, and mistake 40 mesh sieves, again through ultraviolet sterilization 10～20min, then raw material is added one by one and carry out batch mixing in the container, mixing time is 20～40min, gets compound B;
(3), granulate
Mix 5～8% the water that adds its mixed material gross weight in back compound A of gained and the B material respectively to step (2), mix 10～15min, respectively the material of abundant mixing being put into granulator then granulates, the granulation screen cloth adopts 20～40 orders, obtains two kinds of particles of meta-alkalescence and slant acidity respectively;
(4), drying
To granulate through step (3), to put into temperature respectively be that 50～60 ℃ baking oven carries out drying for the meta-alkalescence of back gained and two kinds of particles of slant acidity, and raw material is paved into thick about 5～8mm, controls 30min drying time;
(5), whole grain and mixed grain
After step (4) the feed particles drying, take out cooling respectively, and meta-alkalescence and two kinds of particles of slant acidity are carried out whole grain through 20 orders and 40 mesh sieves respectively successively, add 0.5～2% lubricant then, two kinds of particles are mixed;
(6), compressing tablet
After (5) two kinds of particles of step are mixed,, material is put into tablet press machine carry out compressing tablet, promptly get compressing tablet with the grinding tool of the cooperation of tablet press machine drift and bed die;
(7), sterilization, packing
The compressing tablet of step (6) gained through ultraviolet sterilization, is packed between aseptic packaging, promptly got a kind of Fruity sweet tea effervescent tablets of the present invention.
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