CN102273537B - Litsea Coreana leve. Var. effervescent tablets and preparation method thereof - Google Patents
Litsea Coreana leve. Var. effervescent tablets and preparation method thereof Download PDFInfo
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- CN102273537B CN102273537B CN 201110246798 CN201110246798A CN102273537B CN 102273537 B CN102273537 B CN 102273537B CN 201110246798 CN201110246798 CN 201110246798 CN 201110246798 A CN201110246798 A CN 201110246798A CN 102273537 B CN102273537 B CN 102273537B
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Abstract
The invention discloses Litsea Coreana leve. Var. effervescent tablets and a preparation method thereof. The effervescent tablets comprise 6 to 8 percent of dry powder of a Litsea Coreana leve. Var. extract, 15 to 20 percent of white granulated sugar, 45 to 55 percent of sodium bicarbonate, 3 to 7 percent of polyethylene glycol and 15 to 25 percent of sodium tartrate. The preparation method for the Litsea Coreana leve. Var. effervescent tablets comprises the following steps of: crushing Litsea Coreana leve. Var. into Litsea Coreana leve. Var. powder, sieving with a 50-mesh sieve, and weighing; adding water in an amount which is 8 to 10 times the weight of the Litsea Coreana leve. Var. powder into an extraction tank, heating to 75 to 90 DEG C at normal temperature, adding the Litsea Coreana leve. Var. powder, stirring and extracting for 8 to 12 minutes, filtering by a filter screen with the meshes of between 200 and 300, heating filtrate to 60 to 80 DEG C, reducing the pressure to -15 to 20KPa and concentrating until the filtrate is one fourth to one third of the total weight of the filtrate, and spray-drying to obtain dry powder; and porphyrizing the dry powder of the Litsea Coreana leve. Var. extract, the polyethylene glycol, the sodium tartrate and the white granulated sugar respectively, sieving to ensure that the dry powder of the Litsea Coreana leve. Var. extract, the polyethylene glycol, the sodium tartrate and the white granulated sugar are mixed uniformly, granulating, and tabletting. The invention has the advantages that: the effervescent tablets have the effects of helping digestion, removing stagnation and strengthening the immunity of human bodies, are convenient to carry, have good mouthfeel, and are more suitable for children and elders.
Description
[technical field]
The present invention relates to effervescent tablet, specifically relate to a kind of Litsea Coreana leve. Var. effervescent tablets and preparation method thereof.
[background technology]
Drinking among the people with a long history of Laoyin tea (Litsea Coreana leve.Vat.), after adopting its tender shoots processing, can work as tea-drinking, steep when drinking than delicate fragrance, flavour is abundant, and is first puckery rear sweet, and flavour is dense and mouthful strength is large, drink more to feel to relieve summer heat in summer and quench one's thirst, refresh oneself and add to the fun, among the people have relieve summer heat and the saying of spleen is opened in stomach invigorating.Records such as " cough-relievings, eliminate the phlegm, relieving asthma, relieve summer heat and quench one's thirst " is just arranged on the Compendium of Material Medica.
The botany classification of Laoyin tea: belong to Lauraceae, Litsea, hair Litsea coreana, be commonly called as " white tea ", " old tea ", also be Laoyin tea, belong to aiphyllium, the leaf alternate, the food value of leaf is thick, and the pool is dark green.
Laoyin tea contains Multiple components, such as materials such as amino acid, mineral element, vitamin C, vitamin B1, vitamin B2, flavonoids, Polyphenols, caffeines.Because it contains high ferro, high selenium, high zinc, high chromium feature, be conducive to improve the function of hemopoietic system and internal system; Other trace element is with health role to cranial nerve and cardiovascular and cerebrovascular such as rubidium, phosphorus, zinc etc.Human body is had that quenching one's thirst drives away summer heat, helps digestion and separates swollen, removing toxicity for detumescence, the intelligence development of refreshing oneself, the stomach invigorating that makes eye bright, blood stasis removing analgesic, antidiarrheal, ends the multiple efficacies such as belch.
The sweet cold of Laoyin tea has the perfume (or spice) of blue musk deer, does not turn sour tool inducing resuscitation, cardiac stimulant, the merit of having one's ideas straightened out, promote the production of body fluid, relieving summer heat through night.
Laoyin tea does not affect sleep without excitation, and is rich in mineral matter element, and the metabolism of participant's body protein, amino acid and carbohydrate has a protective effect to cardiovascular.It is remarkable particularly to eliminate greasy effect, but long-term drinking reducing blood lipid, hypotensive, and wherein the selenium of high-load more has the effect of conditioning skin and losing.
It is a lot of that Laoyin tea contains aromatic oil, also contains polyphenol compound, delicate fragrance during the bubble drink, and flavour is abundant, and is first puckery rear sweet, and just the drink person may say; " smell is felt bad " thinks that Laoyin tea mouth strength is large but Chang Yinhou is counter, and flavour is dense and kill mouthful, drinks more to feel to relieve summer heat in summer and quenches one's thirst, refreshes oneself and add to the fun.It is relieved summer heat among the people, and the effect of spleen is opened in stomach invigorating.
Increase along with people's health care meaning, this have the tea of special health care also more and more to receive an acclaim, so that the value of exploiting and utilizing of Laoyin tea is in rapid increase, wherein deep research has been done in Laoyin tea development and use field by the new high-tech enterprise take Anhui Province Ningguo City Yibang Biotechnology Co., Ltd. as representative.
Only there is at present the Chinese scholar to carry out the flavone compound of relevant Laoyin tea (hair Litsea coreana), the chemical composition of Guizhou Laoyin tea, the Primary Study of hair Litsea coreana natural food colour both at home and abroad.Patents to the preparation of extraction, purifying and the Laoyin tea flavone lozenge of the active flavone component of Laoyin tea all has no report.
[summary of the invention]
One of technical problem to be solved by this invention is to provide a kind of Litsea Coreana leve. Var. effervescent tablets, and this effervescent tablet can promoting digestion and removing indigestion, strengthens body immunity.
Two of technical problem to be solved by this invention is to provide a kind of preparation method of above-mentioned Litsea Coreana leve. Var. effervescent tablets.
The present invention is what one of to solve the problems of the technologies described above by the following technical programs: a kind of Litsea Coreana leve. Var. effervescent tablets, composition and the percentage by weight of this Litsea Coreana leve. Var. effervescent tablets are respectively: Extractive dry powder: 6-8%, white granulated sugar: 15%-20%, sodium acid carbonate: 45%-55%, polyethylene glycol: 3%-7%, sodium tartrate: 15%-25%, the extracting method of described Extractive dry powder comprises:
Step 1: Laoyin tea is ground into the tea powder, crosses 50 mesh sieves, weigh;
Step 2: in extractor, add and be equivalent to the water that Laoyin tea powder 8-10 doubly weighs, then normal temperature is heated to 75-90 ℃, add the Laoyin tea powder that step 1 is made, stir and extracted 8-12 minute, then the 200-300 mesh filter screen filters, and filtrate joins in the extractor, be heated to 60-80 ℃, be decompressed to-15 KPa-20KPa is concentrated, and when being concentrated into the 1/4-1/3 of total filtrate weight, spray-drying is made Extractive dry powder.
The composition of this Litsea Coreana leve. Var. effervescent tablets and percentage by weight the best are: Extractive dry powder: 7%, white granulated sugar: 18%, sodium acid carbonate: 50%, polyethylene glycol: 5%, and sodium tartrate: 20%.
The present invention be solve the problems of the technologies described above by the following technical programs two: a kind of preparation method of Litsea Coreana leve. Var. effervescent tablets is characterized in that: comprise the steps:
Step 1: the Laoyin tea of prefabricated effervescent tablet is ground into the tea powder, crosses 50 mesh sieves, weigh;
Step 2: in extractor, add and be equivalent to the water that Laoyin tea powder 8-10 doubly weighs, then normal temperature is heated to 75-90 ℃, add the Laoyin tea powder that step 1 is made, stir and extracted 8-12 minute, then the 200-300 mesh filter screen filters, and filtrate joins in the extractor, is heated to 60-80 ℃, be decompressed to-15 KPa-when 20KPa was concentrated into the 1/4-1/3 of total filtrate weight, spray-drying was made Extractive dry powder;
Step 3: Extractive dry powder, white granulated sugar, sodium acid carbonate, polyethylene glycol, sodium tartrate mixing granulation that step 2 is made, compressing tablet, wherein the percentage by weight of each composition is respectively: Extractive dry powder: 6-8%, white granulated sugar: 15%-20%, sodium acid carbonate: 45%-55%, polyethylene glycol: 3%-7%, sodium tartrate: 15%-25%;
Step 4: packing warehouse-in.
Mixing granulation in the described step 3, the concrete steps of compressing tablet are: take by weighing at first in proportion Extractive dry powder 6-8%, the white granulated sugar 15%-20%, polyethylene glycol 1%-2%, the sodium tartrate 15%-25% that prepare; Pulverizing, mixing add absolute ethyl alcohol, softwood processed; the amount of absolute ethyl alcohol adding " is held agglomerating; the light pressure namely fallen apart " with made softwood and is as the criterion, crosses 24 purpose sieve series wet granulars, with 40 ℃ of dry 1-2 of wet granular hours that prepare; take out; cross the whole grain of 24 mesh sieves, the particle behind the whole grain and particle are mixed, add sodium acid carbonate 45%-55%, polyethylene glycol 1%-6%; mix compressing tablet.
Described step 4 is specially: the diameter of slice, thin piece is 25mm during compressing tablet, and sheet heavily is 1 gram, and hardness is controlled at (3.5 ± 0.5) kg/mm, the packing warehouse-in.
The composition of this Litsea Coreana leve. Var. effervescent tablets and percentage by weight the best are: Extractive dry powder: 7%, white granulated sugar: 18%, sodium acid carbonate: 50%, polyethylene glycol: 5%, and sodium tartrate: 20%.
Advantage of the present invention is: the Litsea Coreana leve. Var. effervescent tablets of producing has promoting digestion and removing indigestion, strengthens body immunity, and is easy to carry and mouthfeel good, and children preferably and old man use.
[specific embodiment]
Embodiment one:
Step 1: Laoyin tea is ground into the tea powder, crosses 50 mesh sieves, weigh;
Step 2: in extractor, add the water that is equivalent to 8 times of weights of Laoyin tea powder, then normal temperature is heated to 85 ℃, add the Laoyin tea powder that step 1 is made, stir and extracted 10 minutes, then 200 mesh filter screens filter, and filtrate joins in the extractor, is heated to 60 ℃, be decompressed to-18KPa is concentrated into 1/4 o'clock of total filtrate weight, and spray-drying is made Extractive dry powder;
Step 3: with the above-mentioned Extractive dry powder that makes, polyethylene glycol (PEG), sodium tartrate, sodium acid carbonate, white granulated sugar is porphyrize respectively, sieve it is mixed, granulate, compressing tablet, described granulation, the equipment of compressing tablet adopts existing general equipment, wherein the percentage by weight of each composition is respectively: Extractive dry powder: 6%, white granulated sugar: 18%, sodium acid carbonate: 50%, polyethylene glycol: 5%, sodium tartrate: 21%, mixing granulation, the concrete steps of compressing tablet are: take by weighing at first in proportion the Extractive dry powder 6% for preparing, white granulated sugar 18%, polyethylene glycol 1%, sodium tartrate 21%; Pulverizing, mixing add absolute ethyl alcohol, softwood processed, softwood is as the criterion with " holding agglomerating; the light pressure namely fallen apart ", crosses 24 purpose sieve series wet granulars, with 40 ℃ of dry 1-2 of wet granular hours that prepare, take out, cross the whole grain of 24 mesh sieves, the particle behind the whole grain and particle are mixed the polyethylene glycol 4% that add sodium acid carbonate 50%, is left, mix compressing tablet;
Step 4: the diameter of slice, thin piece is 25mm during compressing tablet, and sheet heavily is 1 gram, and hardness is controlled at (3.5 ± 0.5) kg/mm, beats code, the packing warehouse-in.
Embodiment two:
Step 1: Laoyin tea is ground into the tea powder, crosses 50 mesh sieves, weigh;
Step 2: in extractor, add the water that is equivalent to 9 times of weights of Laoyin tea powder, then normal temperature is heated to 75 ℃, add the Laoyin tea powder that step 1 is made, stir and extracted 8 minutes, then 250 mesh filter screens filter, and filtrate joins in the extractor, is heated to 70 ℃, be decompressed to-15KPa is concentrated into 1/3 o'clock of total filtrate weight, and spray-drying is made Extractive dry powder;
Step 3: with the above-mentioned Extractive dry powder that makes, polyethylene glycol (PEG), sodium tartrate, sodium acid carbonate, white granulated sugar is porphyrize respectively, sieve it is mixed, granulate, compressing tablet, described granulation, the equipment of compressing tablet adopts existing general equipment, wherein the percentage by weight of each composition is respectively: Extractive dry powder: 8%, white granulated sugar: 15%, sodium acid carbonate: 45%, polyethylene glycol: 7%, sodium tartrate: 25%, mixing granulation, the concrete steps of compressing tablet are: take by weighing at first in proportion the Extractive dry powder 8% for preparing, white granulated sugar 15%, polyethylene glycol 1.5%, sodium tartrate 25%; Pulverizing, mixing add absolute ethyl alcohol, softwood processed, softwood is as the criterion with " holding agglomerating; the light pressure namely fallen apart ", crosses 24 purpose sieve series wet granulars, with 40 ℃ of dry 1-2 of wet granular hours that prepare, take out, cross the whole grain of 24 mesh sieves, the particle behind the whole grain and particle are mixed the polyethylene glycol 5.5% that add sodium acid carbonate 45%, is left, mix compressing tablet;
Step 4: the diameter of slice, thin piece is 25mm during compressing tablet, and sheet heavily is 1 gram, and hardness is controlled at (3.5 ± 0.5) kg/mm, beats code, the packing warehouse-in.
Embodiment three:
Step 1: Laoyin tea is ground into the tea powder, crosses 50 mesh sieves, weigh;
Step 2: in extractor, add the water that is equivalent to 10 times of weights of Laoyin tea powder, then normal temperature is heated to 90 ℃, add the Laoyin tea powder that step 1 is made, stir and extracted 12 minutes, then 300 mesh filter screens filter, and filtrate joins in the extractor, is heated to 80 ℃, be decompressed to-20KPa is concentrated into 1/4 o'clock of total filtrate weight, and spray-drying is made Extractive dry powder;
Step 3: with the above-mentioned Extractive dry powder that makes, polyethylene glycol (PEG), sodium tartrate, sodium acid carbonate, white granulated sugar is porphyrize respectively, sieve it is mixed, granulate, compressing tablet, described granulation, the equipment of compressing tablet adopts existing general equipment, wherein the percentage by weight of each composition is respectively: Extractive dry powder: 7%, white granulated sugar: 20%, sodium acid carbonate: 55%, polyethylene glycol: 3%, sodium tartrate: 15%, mixing granulation, the concrete steps of compressing tablet are: take by weighing at first in proportion the Extractive dry powder 7% for preparing, white granulated sugar 20%, polyethylene glycol 2%, sodium tartrate 15%; Pulverizing, mixing add absolute ethyl alcohol, softwood processed, softwood is as the criterion with " holding agglomerating; the light pressure namely fallen apart ", crosses 24 purpose sieve series wet granulars, with 40 ℃ of dry 1-2 of wet granular hours that prepare, take out, cross the whole grain of 24 mesh sieves, the particle behind the whole grain and particle are mixed the polyethylene glycol 1% that add sodium acid carbonate 55%, is left, mix compressing tablet;
Step 4: the diameter of slice, thin piece is 25mm during compressing tablet, and sheet heavily is 1 gram, and hardness is controlled at (3.5 ± 0.5) kg/mm, beats code, the packing warehouse-in.
Claims (6)
1. Litsea Coreana leve. Var. effervescent tablets, it is characterized in that: the raw material and the percentage by weight that prepare this Litsea Coreana leve. Var. effervescent tablets are respectively: Extractive dry powder: 6-8%, white granulated sugar: 15%-20%, sodium acid carbonate: 45%-55%, polyethylene glycol: 3%-7%, sodium tartrate: 15%-25%, the extracting method of described Extractive dry powder comprises:
Step 1: Laoyin tea is ground into the tea powder, crosses 50 mesh sieves, weigh;
Step 2: in extractor, add and be equivalent to the water that Laoyin tea powder 8-10 doubly weighs, then normal temperature is heated to 75-90 ℃, add the Laoyin tea powder that step 1 is made, stir and extracted 8-12 minute, then the 200-300 mesh filter screen filters, and filtrate joins in the extractor, be heated to 60-80 ℃, be decompressed to-15KPa is concentrated to-20KPa, and when being concentrated into the 1/4-1/3 of total filtrate weight, spray-drying is made Extractive dry powder.
2. a kind of Litsea Coreana leve. Var. effervescent tablets as claimed in claim 1, it is characterized in that: the raw material and the percentage by weight that prepare this Litsea Coreana leve. Var. effervescent tablets are respectively: Extractive dry powder: 7%, white granulated sugar: 18%, sodium acid carbonate: 50%, polyethylene glycol: 5%, and sodium tartrate: 20%.
3. the preparation method of a Litsea Coreana leve. Var. effervescent tablets is characterized in that: comprise the steps:
Step 1: the Laoyin tea of prefabricated effervescent tablet is ground into the tea powder, crosses 50 mesh sieves, weigh;
Step 2: in extractor, add and be equivalent to the water that Laoyin tea powder 8-10 doubly weighs, then normal temperature is heated to 75-90 ℃, add the Laoyin tea powder that step 1 is made, stir and extracted 8-12 minute, then the 200-300 mesh filter screen filters, and filtrate joins in the extractor, is heated to 60-80 ℃, be decompressed to-15KPa to-when 20KPa was concentrated into the 1/4-1/3 of total filtrate weight, spray-drying was made Extractive dry powder;
Step 3: Extractive dry powder, white granulated sugar, sodium acid carbonate, polyethylene glycol, sodium tartrate mixing granulation that step 2 is made, compressing tablet, wherein the percentage by weight of each composition is respectively: Extractive dry powder: 6-8%, white granulated sugar: 15%-20%, sodium acid carbonate: 45%-55%, polyethylene glycol: 3%-7%, sodium tartrate: 15%-25%;
Step 4: packing warehouse-in.
4. the preparation method of a kind of Litsea Coreana leve. Var. effervescent tablets as claimed in claim 3, it is characterized in that: mixing granulation in the described step 3, the concrete steps of compressing tablet are: take by weighing at first in proportion Extractive dry powder 6-8%, the white granulated sugar 15%-20%, polyethylene glycol 1%-2%, the sodium tartrate 15%-25% that prepare; Pulverizing, mixing add absolute ethyl alcohol, softwood processed; softwood with " hold agglomerating; light press namely loose " be as the criterion, cross 24 purpose sieve series wet granulars, with 40 ℃ of dryings of wet granular of preparation 12 hours; take out; cross the whole grain of 24 mesh sieves, the particle behind the whole grain and particle are mixed, add sodium acid carbonate 45%-55%, polyethylene glycol 1%-6%; mix compressing tablet.
5. the preparation method of a kind of Litsea Coreana leve. Var. effervescent tablets as claimed in claim 3, it is characterized in that: described step 4 is specially: the diameter of slice, thin piece is 25mm during compressing tablet, and sheet heavily is 1 gram, and hardness is controlled at (3.5 ± 0.5) kg/mm
2, the packing warehouse-in.
6. the preparation method of a kind of Litsea Coreana leve. Var. effervescent tablets as claimed in claim 3, it is characterized in that: the raw material and the percentage by weight that prepare this Litsea Coreana leve. Var. effervescent tablets are respectively: Extractive dry powder: 7%, white granulated sugar: 18%, sodium acid carbonate: 50%, polyethylene glycol: 5%, and sodium tartrate: 20%.
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| CN 201110246798 CN102273537B (en) | 2011-08-26 | 2011-08-26 | Litsea Coreana leve. Var. effervescent tablets and preparation method thereof |
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| CN 201110246798 CN102273537B (en) | 2011-08-26 | 2011-08-26 | Litsea Coreana leve. Var. effervescent tablets and preparation method thereof |
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| CN102273537B true CN102273537B (en) | 2013-03-20 |
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Families Citing this family (3)
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| CN105497136A (en) * | 2015-12-08 | 2016-04-20 | 肇庆医学高等专科学校 | Five flower tea effervescent tablet and preparation method thereof |
| CN106720718A (en) * | 2016-11-17 | 2017-05-31 | 西华大学 | Granulated litsea coreana and preparation method thereof |
| CN110012945A (en) * | 2019-04-28 | 2019-07-16 | 刘翔宇 | A kind of manufacture craft of tea cake |
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2011
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| CN1302655A (en) * | 2000-12-29 | 2001-07-11 | 广西大学 | Compound broadleaf holly leaf buccal tablet and preparation method thereof |
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