CN101657253B - 大的单晶金刚石 - Google Patents
大的单晶金刚石 Download PDFInfo
- Publication number
- CN101657253B CN101657253B CN2008800121066A CN200880012106A CN101657253B CN 101657253 B CN101657253 B CN 101657253B CN 2008800121066 A CN2008800121066 A CN 2008800121066A CN 200880012106 A CN200880012106 A CN 200880012106A CN 101657253 B CN101657253 B CN 101657253B
- Authority
- CN
- China
- Prior art keywords
- single crystal
- growth
- crystal diamond
- seed
- diamond material
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
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Classifications
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- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B25/00—Single-crystal growth by chemical reaction of reactive gases, e.g. chemical vapour-deposition growth
- C30B25/02—Epitaxial-layer growth
- C30B25/18—Epitaxial-layer growth characterised by the substrate
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J3/00—Processes of utilising sub-atmospheric or super-atmospheric pressure to effect chemical or physical change of matter; Apparatus therefor
- B01J3/06—Processes using ultra-high pressure, e.g. for the formation of diamonds; Apparatus therefor, e.g. moulds or dies
- B01J3/062—Processes using ultra-high pressure, e.g. for the formation of diamonds; Apparatus therefor, e.g. moulds or dies characterised by the composition of the materials to be processed
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2203/00—Processes utilising sub- or super atmospheric pressure
- B01J2203/06—High pressure synthesis
- B01J2203/0605—Composition of the material to be processed
- B01J2203/061—Graphite
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2203/00—Processes utilising sub- or super atmospheric pressure
- B01J2203/06—High pressure synthesis
- B01J2203/0605—Composition of the material to be processed
- B01J2203/062—Diamond
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2203/00—Processes utilising sub- or super atmospheric pressure
- B01J2203/06—High pressure synthesis
- B01J2203/065—Composition of the material produced
- B01J2203/0655—Diamond
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2203/00—Processes utilising sub- or super atmospheric pressure
- B01J2203/06—High pressure synthesis
- B01J2203/0675—Structural or physico-chemical features of the materials processed
- B01J2203/068—Crystal growth
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/24—Structurally defined web or sheet [e.g., overall dimension, etc.]
- Y10T428/24942—Structurally defined web or sheet [e.g., overall dimension, etc.] including components having same physical characteristic in differing degree
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/30—Self-sustaining carbon mass or layer with impregnant or other layer
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Crystallography & Structural Chemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
- Carbon And Carbon Compounds (AREA)
- Nonmetal Cutting Devices (AREA)
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB0704516.4 | 2007-03-08 | ||
| GBGB0704516.4A GB0704516D0 (en) | 2007-03-08 | 2007-03-08 | Diamond |
| US89492007P | 2007-03-15 | 2007-03-15 | |
| US60/894,920 | 2007-03-15 | ||
| PCT/IB2008/050851 WO2008107860A2 (en) | 2007-03-08 | 2008-03-07 | Large single crystal diamonds |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101657253A CN101657253A (zh) | 2010-02-24 |
| CN101657253B true CN101657253B (zh) | 2013-01-23 |
Family
ID=37988627
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2008800121066A Active CN101657253B (zh) | 2007-03-08 | 2008-03-07 | 大的单晶金刚石 |
Country Status (6)
| Country | Link |
|---|---|
| US (2) | US8574535B2 (enExample) |
| EP (1) | EP2125188B1 (enExample) |
| JP (1) | JP5522606B2 (enExample) |
| CN (1) | CN101657253B (enExample) |
| GB (1) | GB0704516D0 (enExample) |
| WO (1) | WO2008107860A2 (enExample) |
Families Citing this family (58)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB0704516D0 (en) | 2007-03-08 | 2007-04-18 | Element Six Ltd | Diamond |
| US20090260396A1 (en) * | 2008-04-16 | 2009-10-22 | Eitan Broukman | Methods for processing ornamental diamonds and corresponding ornamental diamonds |
| GB0900771D0 (en) * | 2009-01-16 | 2009-03-04 | Element Six Ltd | Diamond |
| US20100272627A1 (en) * | 2009-04-23 | 2010-10-28 | Chien-Min Sung | Multi-Faceted Diamond and Associated Methods |
| GB201107730D0 (en) * | 2011-05-10 | 2011-06-22 | Element Six Ltd | Diamond sensors, detectors and quantum devices |
| CN104160061B (zh) * | 2011-12-16 | 2017-10-10 | 六号元素技术有限公司 | 大面积光学质量合成多晶金刚石窗户 |
| KR101299136B1 (ko) * | 2012-02-08 | 2013-08-22 | 한국과학기술연구원 | 다이아몬드 열방산체 및 그 제조방법 |
| GB201204533D0 (en) * | 2012-03-15 | 2012-04-25 | Element Six Ltd | Process for manufacturing synthetic single crystal diamond material |
| GB201320304D0 (en) * | 2013-11-18 | 2014-01-01 | Element Six Ltd | Methods of fabricating synthetic diamond materials using microwave plasma actived chemical vapour deposition techniques and products obtained using said |
| US10006973B2 (en) | 2016-01-21 | 2018-06-26 | Lockheed Martin Corporation | Magnetometer with a light emitting diode |
| US10088336B2 (en) | 2016-01-21 | 2018-10-02 | Lockheed Martin Corporation | Diamond nitrogen vacancy sensed ferro-fluid hydrophone |
| US9824597B2 (en) | 2015-01-28 | 2017-11-21 | Lockheed Martin Corporation | Magnetic navigation methods and systems utilizing power grid and communication network |
| US9614589B1 (en) | 2015-12-01 | 2017-04-04 | Lockheed Martin Corporation | Communication via a magnio |
| US9910105B2 (en) | 2014-03-20 | 2018-03-06 | Lockheed Martin Corporation | DNV magnetic field detector |
| US9551763B1 (en) | 2016-01-21 | 2017-01-24 | Lockheed Martin Corporation | Diamond nitrogen vacancy sensor with common RF and magnetic fields generator |
| US10168393B2 (en) | 2014-09-25 | 2019-01-01 | Lockheed Martin Corporation | Micro-vacancy center device |
| US10338162B2 (en) | 2016-01-21 | 2019-07-02 | Lockheed Martin Corporation | AC vector magnetic anomaly detection with diamond nitrogen vacancies |
| US9910104B2 (en) | 2015-01-23 | 2018-03-06 | Lockheed Martin Corporation | DNV magnetic field detector |
| US9829545B2 (en) | 2015-11-20 | 2017-11-28 | Lockheed Martin Corporation | Apparatus and method for hypersensitivity detection of magnetic field |
| US9853837B2 (en) | 2014-04-07 | 2017-12-26 | Lockheed Martin Corporation | High bit-rate magnetic communication |
| US9638821B2 (en) | 2014-03-20 | 2017-05-02 | Lockheed Martin Corporation | Mapping and monitoring of hydraulic fractures using vector magnetometers |
| US9557391B2 (en) | 2015-01-23 | 2017-01-31 | Lockheed Martin Corporation | Apparatus and method for high sensitivity magnetometry measurement and signal processing in a magnetic detection system |
| CA2945016A1 (en) | 2014-04-07 | 2015-10-15 | Lockheed Martin Corporation | Energy efficient controlled magnetic field generator circuit |
| KR101811761B1 (ko) * | 2014-10-11 | 2017-12-22 | 허난 페이머스 다이아몬드 인더스트리얼 씨오. 엘티디 | 거친 표면의 금강석의 합성방법 |
| EP3251193A4 (en) | 2015-01-28 | 2018-08-08 | Lockheed Martin Corporation | In-situ power charging |
| WO2016126436A1 (en) | 2015-02-04 | 2016-08-11 | Lockheed Martin Corporation | Apparatus and method for recovery of three dimensional magnetic field from a magnetic detection system |
| WO2016126435A1 (en) | 2015-02-04 | 2016-08-11 | Lockheed Martin Corporation | Apparatus and method for estimating absolute axes' orientations for a magnetic detection system |
| CN105327654A (zh) * | 2015-10-23 | 2016-02-17 | 重庆天宇弘锋新材料科技有限责任公司 | 一种生命钻石的制备工艺 |
| WO2017078766A1 (en) | 2015-11-04 | 2017-05-11 | Lockheed Martin Corporation | Magnetic band-pass filter |
| WO2017087013A1 (en) | 2015-11-20 | 2017-05-26 | Lockheed Martin Corporation | Apparatus and method for closed loop processing for a magnetic detection system |
| WO2017123261A1 (en) | 2016-01-12 | 2017-07-20 | Lockheed Martin Corporation | Defect detector for conductive materials |
| AU2016387312A1 (en) | 2016-01-21 | 2018-09-06 | Lockheed Martin Corporation | Magnetometer with light pipe |
| EP3405603A4 (en) | 2016-01-21 | 2019-10-16 | Lockheed Martin Corporation | DIAMOND NITROGEN SENSOR WITH SWITCHING ON DIAMOND |
| WO2017127096A1 (en) | 2016-01-21 | 2017-07-27 | Lockheed Martin Corporation | Diamond nitrogen vacancy sensor with dual rf sources |
| WO2017127090A1 (en) | 2016-01-21 | 2017-07-27 | Lockheed Martin Corporation | Higher magnetic sensitivity through fluorescence manipulation by phonon spectrum control |
| US10345396B2 (en) | 2016-05-31 | 2019-07-09 | Lockheed Martin Corporation | Selected volume continuous illumination magnetometer |
| US10317279B2 (en) | 2016-05-31 | 2019-06-11 | Lockheed Martin Corporation | Optical filtration system for diamond material with nitrogen vacancy centers |
| US20170343621A1 (en) | 2016-05-31 | 2017-11-30 | Lockheed Martin Corporation | Magneto-optical defect center magnetometer |
| US10274550B2 (en) | 2017-03-24 | 2019-04-30 | Lockheed Martin Corporation | High speed sequential cancellation for pulsed mode |
| US10571530B2 (en) | 2016-05-31 | 2020-02-25 | Lockheed Martin Corporation | Buoy array of magnetometers |
| US10338163B2 (en) | 2016-07-11 | 2019-07-02 | Lockheed Martin Corporation | Multi-frequency excitation schemes for high sensitivity magnetometry measurement with drift error compensation |
| US10345395B2 (en) | 2016-12-12 | 2019-07-09 | Lockheed Martin Corporation | Vector magnetometry localization of subsurface liquids |
| US10408890B2 (en) | 2017-03-24 | 2019-09-10 | Lockheed Martin Corporation | Pulsed RF methods for optimization of CW measurements |
| US10527746B2 (en) | 2016-05-31 | 2020-01-07 | Lockheed Martin Corporation | Array of UAVS with magnetometers |
| US10145910B2 (en) | 2017-03-24 | 2018-12-04 | Lockheed Martin Corporation | Photodetector circuit saturation mitigation for magneto-optical high intensity pulses |
| US10371765B2 (en) | 2016-07-11 | 2019-08-06 | Lockheed Martin Corporation | Geolocation of magnetic sources using vector magnetometer sensors |
| US10359479B2 (en) | 2017-02-20 | 2019-07-23 | Lockheed Martin Corporation | Efficient thermal drift compensation in DNV vector magnetometry |
| US10330744B2 (en) | 2017-03-24 | 2019-06-25 | Lockheed Martin Corporation | Magnetometer with a waveguide |
| US10228429B2 (en) | 2017-03-24 | 2019-03-12 | Lockheed Martin Corporation | Apparatus and method for resonance magneto-optical defect center material pulsed mode referencing |
| US10677953B2 (en) | 2016-05-31 | 2020-06-09 | Lockheed Martin Corporation | Magneto-optical detecting apparatus and methods |
| US10281550B2 (en) | 2016-11-14 | 2019-05-07 | Lockheed Martin Corporation | Spin relaxometry based molecular sequencing |
| GB201620413D0 (en) * | 2016-12-01 | 2017-01-18 | Element Six Tech Ltd | Single crystal synthetic diamond material via chemical vapour deposition |
| US10371760B2 (en) | 2017-03-24 | 2019-08-06 | Lockheed Martin Corporation | Standing-wave radio frequency exciter |
| US10459041B2 (en) | 2017-03-24 | 2019-10-29 | Lockheed Martin Corporation | Magnetic detection system with highly integrated diamond nitrogen vacancy sensor |
| US10379174B2 (en) | 2017-03-24 | 2019-08-13 | Lockheed Martin Corporation | Bias magnet array for magnetometer |
| US10338164B2 (en) | 2017-03-24 | 2019-07-02 | Lockheed Martin Corporation | Vacancy center material with highly efficient RF excitation |
| CN107675249B (zh) * | 2017-09-08 | 2020-07-07 | 西安电子科技大学 | 单晶金刚石的扩径生长方法 |
| GB202305972D0 (en) * | 2023-04-24 | 2023-06-07 | Element Six Tech Ltd | Method of manufacturing single crystal diamonds |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0136408A1 (en) * | 1983-07-01 | 1985-04-10 | Sumitomo Electric Industries Limited | Synthetic diamond heat sink |
| CN88103598A (zh) * | 1987-05-08 | 1988-12-07 | 住友电气工业株式会社 | 合成大尺寸金刚石的方法 |
| JP2932559B2 (ja) * | 1990-01-19 | 1999-08-09 | 住友電気工業株式会社 | 大型ダイヤモンド単結晶の合成方法 |
| EP1671726A1 (en) * | 2003-10-10 | 2006-06-21 | Sumitomo Electric Industries, Ltd. | Diamond tool, synthetic single crystal diamond and method for synthesizing single crystal diamond, and diamond jewelry |
Family Cites Families (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4034066A (en) | 1973-11-02 | 1977-07-05 | General Electric Company | Method and high pressure reaction vessel for quality control of diamond growth on diamond seed |
| US4544540A (en) * | 1982-06-25 | 1985-10-01 | Sumitomo Electric Industries, Ltd. | Diamond single crystals, a process of manufacturing and tools for using same |
| AU4245693A (en) | 1992-05-04 | 1993-11-29 | Case Western Reserve University | Growth of diamond crystals |
| US5474021A (en) | 1992-09-24 | 1995-12-12 | Sumitomo Electric Industries, Ltd. | Epitaxial growth of diamond from vapor phase |
| ATE248020T1 (de) * | 1995-12-21 | 2003-09-15 | Element Six Pty Ltd | Diamantsynthese |
| AU7062698A (en) * | 1997-04-17 | 1998-11-11 | De Beers Industrial Diamond Division (Proprietary) Limited | Sintering process for diamond and diamond growth |
| JP4032482B2 (ja) | 1997-04-18 | 2008-01-16 | 住友電気工業株式会社 | 単結晶ダイヤモンドの製造方法 |
| US7128547B2 (en) * | 2004-01-13 | 2006-10-31 | Chien-Min Sung | High pressure split die and associated methods |
| JP5362993B2 (ja) | 2004-12-09 | 2013-12-11 | エレメント シックス テクノロジーズ (プロプライアタリー)リミテッド | ダイヤモンド結晶の結晶完全性を改良する方法 |
| JP5002982B2 (ja) | 2005-04-15 | 2012-08-15 | 住友電気工業株式会社 | 単結晶ダイヤモンドの製造方法 |
| JP4613314B2 (ja) | 2005-05-26 | 2011-01-19 | 独立行政法人産業技術総合研究所 | 単結晶の製造方法 |
| WO2006135093A1 (ja) * | 2005-06-17 | 2006-12-21 | Sumitomo Electric Industries, Ltd. | ダイヤモンド電子放射陰極、電子放射源、電子顕微鏡及び電子ビーム露光機 |
| JP5323492B2 (ja) | 2005-12-09 | 2013-10-23 | エレメント シックス テクノロジーズ (プロプライアタリー) リミテッド | 高結晶品質の合成ダイヤモンド |
| GB0704516D0 (en) | 2007-03-08 | 2007-04-18 | Element Six Ltd | Diamond |
| GB0900771D0 (en) * | 2009-01-16 | 2009-03-04 | Element Six Ltd | Diamond |
-
2007
- 2007-03-08 GB GBGB0704516.4A patent/GB0704516D0/en not_active Ceased
-
2008
- 2008-03-07 WO PCT/IB2008/050851 patent/WO2008107860A2/en not_active Ceased
- 2008-03-07 JP JP2009552319A patent/JP5522606B2/ja active Active
- 2008-03-07 EP EP08719613.5A patent/EP2125188B1/en active Active
- 2008-03-07 CN CN2008800121066A patent/CN101657253B/zh active Active
- 2008-03-07 US US12/529,183 patent/US8574535B2/en active Active
-
2013
- 2013-09-06 US US14/019,663 patent/US9034296B2/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0136408A1 (en) * | 1983-07-01 | 1985-04-10 | Sumitomo Electric Industries Limited | Synthetic diamond heat sink |
| CN88103598A (zh) * | 1987-05-08 | 1988-12-07 | 住友电气工业株式会社 | 合成大尺寸金刚石的方法 |
| JP2932559B2 (ja) * | 1990-01-19 | 1999-08-09 | 住友電気工業株式会社 | 大型ダイヤモンド単結晶の合成方法 |
| EP1671726A1 (en) * | 2003-10-10 | 2006-06-21 | Sumitomo Electric Industries, Ltd. | Diamond tool, synthetic single crystal diamond and method for synthesizing single crystal diamond, and diamond jewelry |
Non-Patent Citations (1)
| Title |
|---|
| JP第2932559号B2 1999.08.09 |
Also Published As
| Publication number | Publication date |
|---|---|
| US20140020620A1 (en) | 2014-01-23 |
| CN101657253A (zh) | 2010-02-24 |
| GB0704516D0 (en) | 2007-04-18 |
| WO2008107860A3 (en) | 2008-10-30 |
| US9034296B2 (en) | 2015-05-19 |
| WO2008107860A2 (en) | 2008-09-12 |
| EP2125188B1 (en) | 2017-11-15 |
| US8574535B2 (en) | 2013-11-05 |
| US20100119790A1 (en) | 2010-05-13 |
| EP2125188A2 (en) | 2009-12-02 |
| JP2010520146A (ja) | 2010-06-10 |
| JP5522606B2 (ja) | 2014-06-18 |
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| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant |