CN101600954B - 固相及催化实现的自动同位素稀释和物种化同位素稀释质谱法 - Google Patents

固相及催化实现的自动同位素稀释和物种化同位素稀释质谱法 Download PDF

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CN101600954B
CN101600954B CN2007800509715A CN200780050971A CN101600954B CN 101600954 B CN101600954 B CN 101600954B CN 2007800509715 A CN2007800509715 A CN 2007800509715A CN 200780050971 A CN200780050971 A CN 200780050971A CN 101600954 B CN101600954 B CN 101600954B
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species
solid phase
isotope
analyte
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CN101600954A (zh
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H·M·金斯顿
M·拉赫曼
D·利内曼
M·帕穆克丘
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APPLIED ISOTOPE TECHNOLOGIES Inc
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    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00—Sampling; Preparing specimens for investigation
    • G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/44—Sample treatment involving radiation, e.g. heat
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00—Sampling; Preparing specimens for investigation
    • G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/40—Concentrating samples
    • G01N1/405—Concentrating samples by adsorption or absorption
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T436/00—Chemistry: analytical and immunological testing
    • Y10T436/14—Heterocyclic carbon compound [i.e., O, S, N, Se, Te, as only ring hetero atom]
    • Y10T436/141111—Diverse hetero atoms in same or different rings [e.g., alkaloids, opiates, etc.]
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T436/00—Chemistry: analytical and immunological testing
    • Y10T436/14—Heterocyclic carbon compound [i.e., O, S, N, Se, Te, as only ring hetero atom]
    • Y10T436/142222—Hetero-O [e.g., ascorbic acid, etc.]
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T436/00—Chemistry: analytical and immunological testing
    • Y10T436/19—Halogen containing
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T436/00—Chemistry: analytical and immunological testing
    • Y10T436/20—Oxygen containing
    • Y10T436/200833—Carbonyl, ether, aldehyde or ketone containing
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T436/00—Chemistry: analytical and immunological testing
    • Y10T436/20—Oxygen containing
    • Y10T436/203332—Hydroxyl containing
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T436/00—Chemistry: analytical and immunological testing
    • Y10T436/21—Hydrocarbon
    • Y10T436/212—Aromatic
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T436/00—Chemistry: analytical and immunological testing
    • Y10T436/24—Nuclear magnetic resonance, electron spin resonance or other spin effects or mass spectrometry
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T436/00—Chemistry: analytical and immunological testing
    • Y10T436/25—Chemistry: analytical and immunological testing including sample preparation
    • Y10T436/25375—Liberation or purification of sample or separation of material from a sample [e.g., filtering, centrifuging, etc.]
    • Y10T436/255—Liberation or purification of sample or separation of material from a sample [e.g., filtering, centrifuging, etc.] including use of a solid sorbent, semipermeable membrane, or liquid extraction
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T436/00—Chemistry: analytical and immunological testing
    • Y10T436/25—Chemistry: analytical and immunological testing including sample preparation
    • Y10T436/25625—Dilution

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  • Life Sciences & Earth Sciences (AREA)
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  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
CN2007800509715A 2006-12-07 2007-12-07 固相及催化实现的自动同位素稀释和物种化同位素稀释质谱法 Active CN101600954B (zh)

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PCT/US2007/086795 WO2008112032A2 (en) 2006-12-07 2007-12-07 Solid phase and catalyzed enabled automated isotope dilution and speciated isotope dilution mass spectrometry

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US20120205533A1 (en) * 2009-08-19 2012-08-16 Ariya Parisa A Methods and systems for the quantitative chemical speciation of heavy metals and other toxic pollutants
CN103913534B (zh) * 2014-02-11 2016-08-17 中国科学院地质与地球物理研究所兰州油气资源研究中心 一种天然气中系列烃类化合物碳同位素分析方法
CN103837593B (zh) * 2014-03-18 2016-11-23 中国计量科学研究院 一种人血清蛋白质电泳后同位素稀释质谱定量方法
CN104006993B (zh) * 2014-05-26 2016-08-24 中国兵器工业集团第五三研究所 Id-icp-ms法燃油中硫含量的测试样品制备方法
US9443708B2 (en) * 2014-09-10 2016-09-13 Battelle Memorial Institute Ion implantation system and process for ultrasensitive determination of target isotopes
CN104897766B (zh) * 2015-04-27 2017-08-08 北京市医疗器械检验所 一种用同位素稀释质谱法测定样品中痕量元素的校正方法
WO2017154083A1 (ja) * 2016-03-07 2017-09-14 株式会社日立ハイテクノロジーズ 分析装置
US11099165B1 (en) 2016-03-08 2021-08-24 United States Of America As Represented By The Secretary Of The Air Force Focusing agents and methods of using same
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JP7109374B2 (ja) * 2016-04-14 2022-07-29 エフ．ホフマン－ラ ロシュ アーゲー 体液の試料中の標的分析物の濃度を決定するための方法
CN107576748B (zh) * 2016-09-29 2019-07-12 宁波大学 一种应用超声辅助-顶空-固相微萃取技术测定土壤中七种多氯联苯的方法
USD827308S1 (en) 2017-03-07 2018-09-04 Paris Presents Incorporated Makeup brush
USD827309S1 (en) 2017-03-07 2018-09-04 Paris Presents Incorporated Makeup brush
CN108624516B (zh) * 2017-03-20 2022-08-26 华东理工大学 一种提高发酵细胞中的代谢产物量及制备idms标准品的方法
CN108303457B (zh) * 2018-02-11 2023-12-29 中国科学院地质与地球物理研究所 一种用于电离层H、He同位素测量的仪器和方法
EP3576129B1 (en) * 2018-06-01 2023-05-03 Thermo Fisher Scientific (Bremen) GmbH Method for detecting the isotopic labelling state of unknown species of molecules
CN111089969B (zh) * 2018-10-24 2023-08-22 复旦大学 一种n-糖链快速酶解释放和固相富集并质谱分析的方法
US11022593B2 (en) 2018-10-25 2021-06-01 Savannah River Nuclear Solutions, Llc Solid phase sampling device and methods for point-source sampling of polar organic analytes
CN111257098A (zh) * 2018-11-30 2020-06-09 中国科学院大连化学物理研究所 一种催化剂重积碳物种结构的定性检测方法
JP7584418B2 (ja) * 2018-12-04 2024-11-15 ブリストル－マイヤーズ スクイブ カンパニー 多重反応同位体分子種反応モニタリングによる、サンプル内検量線を用いた分析方法
CN110243919A (zh) * 2019-05-14 2019-09-17 中国石油天然气股份有限公司 一种利用钒同位素对油气成因与来源进行分析的方法
CN112683986B (zh) * 2021-03-18 2021-06-15 裕菁科技(上海)有限公司 一种用于定量样品中目标分析物的天然同位素校准曲线法
CN114487202B (zh) * 2022-02-14 2024-11-26 宁夏医科大学 中药材中SUHs的检测方法
CN115060808A (zh) * 2022-02-24 2022-09-16 上海大学 固相萃取结合气相色谱-质谱同时检测水环境介质中多种有机磷酸酯的方法
CN115754103B (zh) * 2022-11-09 2025-09-26 国科大杭州高等研究院 金属离子的富集材料、富集柱及富集方法
CN115859632B (zh) * 2022-12-07 2023-05-26 中科三清科技有限公司 在线源解析模型不确定度调节方法、装置与可读存储介质
CN119355189A (zh) * 2024-10-18 2025-01-24 中国科学院大连化学物理研究所 一种复杂液体样品的质谱检测方法
CN119086941B (zh) * 2024-11-05 2025-02-28 融致丰生制药有限公司 一种多肽提取物的质谱检测分析方法

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WO2008112032A2 (en) 2008-09-18
JP2010512515A (ja) 2010-04-22
CA2671859A1 (en) 2008-09-18
AU2007349186B2 (en) 2014-03-06
AU2007349186A1 (en) 2008-09-18
WO2008112032A3 (en) 2008-12-31
HK1138908A1 (en) 2010-09-03
CA2671859C (en) 2016-07-12
CN101600954A (zh) 2009-12-09
EP2108111A2 (en) 2009-10-14
JP5412288B2 (ja) 2014-02-12
US20120142545A1 (en) 2012-06-07
DK2108111T3 (da) 2019-07-15
EP2108111B1 (en) 2019-04-24
CN103257070A (zh) 2013-08-21
US8383420B2 (en) 2013-02-26

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