CN101518505A - Anti-acne facial cleanser composition - Google Patents
Anti-acne facial cleanser composition Download PDFInfo
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- CN101518505A CN101518505A CN200910038307A CN200910038307A CN101518505A CN 101518505 A CN101518505 A CN 101518505A CN 200910038307 A CN200910038307 A CN 200910038307A CN 200910038307 A CN200910038307 A CN 200910038307A CN 101518505 A CN101518505 A CN 101518505A
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- cleanser composition
- acne facial
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Abstract
The invention relates to an anti-acne facial cleanser composition. Besides water, the anti-acne facial cleanser composition also comprises the following components by weight percentage: (A) 0.5 to 30.0 percent of fatty acid; (B) 0.05 to 6.0 percent of neutralizing agent; (C) 0.1 to 20.0 percent of surfactant; (D) 0.05 to 8.0 percent of wet storage agent; and (E) 0.01 to 1.5 percent of disinfectant. The anti-acne facial cleanser composition is mild, does not affect the skin, and has good anti-acne effect.
Description
Technical field
The present invention relates to a kind of cleansing milk, be specifically related to a kind of facial cleanser composition with acne-removing.
Background technology
Comedo is a kind of hair follicle, sebaceous gland chronic inflammation of tissue dermatoses, claims acne or seat skin ulcer again, and pilosity is born in puberty stage, also abscess, ulceration can occur when serious, and then forms cicatrix, brings endless worry for the adolescence men and women who likes to be beautiful.Bacterial infection is the most important reason that comedo takes place, and therefore can play the effect of alleviation, treatment comedo by kill bacteria.The early stage antibacterial that uses mainly contains: sulfur, Benasept, benzethonium chloride, fruit acid, salicylic acid, benzoyl peroxide etc., also have and use antibiotic as chloromycetin, erythromycin etc., this series bactericidal agent or antibiotic adding, though certain anti-acne effect is arranged, but also have certain counter productive simultaneously, can cause problems such as skin allergy.The another one key factor that comedo produces is that sebaceous gland is grown vigorous, the sebum secretion amount increases, the sebum that increases can not in time be got rid of, through oxidation, pollution and become comedo, so keep the cleaning of skin also to help the control and the treatment of comedo, but only depend on cleaning skin can't reach acne-removing.Therefore the clean skin Products Development with acne-removing of function admirable has realistic meaning.
Summary of the invention
The purpose of this invention is to provide a kind of facial cleanser composition, to solve the problem that the cleansing milk acne-removing is poor, zest is big in the prior art with acne-removing.
Anti-acne facial cleanser composition of the present invention outside dewatering, also contains: the fatty acid that (A) accounts for composition weight 0.5% to 30.0%; (B) account for the nertralizer of composition weight 0.05% to 6.0%; (C) account for the surfactant of composition weight 0.1% to 20.0%; (D) account for the wetting agent of composition weight 0.05% to 8.0%; (E) account for the antibacterial of composition weight 0.01% to 1.5%.
Anti-acne facial cleanser composition of the present invention, described fatty acid are at least a in dodecoic acid, tetradecylic acid, hexadecylic acid, the stearic acid.
Anti-acne facial cleanser composition of the present invention, described nertralizer are a kind of in sodium hydroxide, potassium hydroxide, the triethanolamine.
Anti-acne facial cleanser composition of the present invention, described surfactant are at least a in aliphatic alcohol sulfate, fatty alcohol polyoxyethylene ether sulfate, alkylolamides, the betaines amphoteric surfactant.
Anti-acne facial cleanser composition of the present invention, described wetting agent are at least a in glycerol, propylene glycol, Oleum Ricini maleic acid glyceride, olein, the cocos nucifera oil polyethyleneglycol glyceride.
Anti-acne facial cleanser composition of the present invention, described antibacterial are isethionic acid six amidines, the own amidine of two isethionic acids, 3,4, at least a in 4-trichlorine diphenylurea, tea tree oil, the Aloe extraction solution.
Anti-acne facial cleanser composition of the present invention can also contain the pearling agent that accounts for composition weight 0.0% to 5.0%.
Anti-acne facial cleanser composition of the present invention, preferred prescription is:
Constituent content (weight %)
Tetradecylic acid 8.0
Hexadecylic acid 5.0
Potassium hydroxide 2.1
Glycerol 3.0
Polyoxyethylene lauryl ether sodium sulfate 10
Cocos nucifera oil diglycollic amide 3.0
Oleum Ricini maleic acid glyceride 1.0
Isethionic acid six amidines 0.2
Pearlescent flake 3.0
Disodiumedetate 0.2
Antiseptic, essence, coloring agent are an amount of
Water adds 100%
To be elaborated to component selection of the present invention and effect below.
Contain the fatty acid that accounts for composition weight 0.5% to 30.0% in the anti-acne facial cleanser composition of the present invention, described fatty acid is at least a in dodecoic acid, tetradecylic acid, hexadecylic acid, the stearic acid, preferred tetradecylic acid and stearic compositions.Described dodecoic acid is a lauric acid, is the white crystalline waxy solid, and described tetradecylic acid is a myristic acid, is white crystalline solid; Described hexadecylic acid is a Palmic acid, is white crystalline solid; Described stearic acid is a stearic acid, is white or little yellow lamellar crystalline solid.Contain the nertralizer that accounts for composition weight 0.05% to 6.0% in the anti-acne facial cleanser composition of the present invention, described nertralizer is a kind of in sodium hydroxide, potassium hydroxide, the triethanolamine, preferred potassium hydroxide, described potassium hydroxide is used for fatty acid soaps is turned to fatty acid soaps, and then playing the effect of cleaning, the saponification rate of described potassium hydroxide good fortune fatty acid is 65% to 100%.
Contain the surfactant that accounts for composition weight 0.1% to 20.0% in the anti-acne facial cleanser composition of the present invention, described surfactant is at least a in aliphatic alcohol sulfate, fatty alcohol polyoxyethylene ether sulfate, alkylolamides, the betaines amphoteric surfactant.Described aliphatic alcohol sulfate comprises: described aliphatic alcohol sulfate structural formula is: ROSO
3M, wherein M=Na
+, K
+, [HN (CH
2CH
2OH)
3]
+, [H
2N (CH
2CH
2OH)
2]
+, [H
2NCH
2CH
2OH]
+, NH
4 +, R=C
12～C
18Alkyl, preferred M=Na
+, R=C
12, i.e. lauryl alcohol sodium sulfate; Described fatty alcohol ether polyoxyethylene sulfate structural formula is RO (CH
2CH
2O)
nSO
3M, wherein M=Na
+, NH
4 +, [H (C
2H
5OH)
3]
+, R=C
12～C
18Alkyl, n are 2～4, and preferred average ethoxyquin degree is n=3, M=Na
+, R=C
12, i.e. lauryl alcohol ether polyoxyethylene sodium sulfate; Described alkylolamides comprises: coconut monoethanol amide and cocos nucifera oil diglycollic amide; Described betaines amphoteric surfactant comprises: coco dimethyl betanin, cocamido propyl betaine, dodecanamide propyl betanin, cocamidopropyl propyl amide hydroxyl sulphur betanin, lauramide hydroxyl sulphur betanin, preferred cocamido propyl betaine.Other are applicable to that amphoteric surfactant of the present invention also has cocoyl both sexes sodium acetate and lauryl both sexes sodium acetate etc.
Contain the wetting agent that accounts for composition weight 0.05% to 8.0% in the anti-acne facial cleanser composition of the present invention, described wetting agent is at least a in glycerol, propylene glycol, Oleum Ricini maleic acid glyceride, olein, the cocos nucifera oil polyethyleneglycol glyceride.The adding of described wetting agent plays and preserves moisture, soft, lubricated effect, makes product with the no tight sense in back.Other are applicable to that wetting agent of the present invention also has: fatty acid esters such as cocoyl glucoside, sad capric acid triglyceride, cocoyl glyceride, isopropyl palmitate, isopropyl myristate, decyl oleate, isostearate.
Contain the antibacterial that accounts for composition weight 0.01% to 1.5% in the anti-acne facial cleanser composition of the present invention, described antibacterial is isethionic acid six amidines, the own amidine of two isethionic acids, 3,4, at least a in 4-trichlorine diphenylurea, tea tree oil, the Aloe extraction solution, at least a in preferred isethionic acid six amidines, the own amidine of two isethionic acids.Other are applicable to that antibacterial of the present invention also has triclosan, Radix Scutellariae extracting solution etc.
Anti-acne facial cleanser composition of the present invention also contains the pearling agent that accounts for composition weight 0.0% to 5.0%.Described pearling agent is selected from: a kind of in ethylene glycol stearate monoesters and dibasic acid esters, the polyglycol distearate.Anti-acne facial cleanser composition of the present invention can also comprise other optional components, comprises chelating agen, antiseptic, coloring agent and spice etc.The non-limiting example of described chelating agen has: ethylenediaminetetraacetic acid, disodiumedetate, tetrasodium ethylenediamine tetraacetate, citric acid, phosphoric acid, ascorbic acid etc., preferred disodiumedetate; Choosing of described antiseptic, essence, coloring agent meets the regulation of hygienic standards for cosmetics, selects safe raw material for use.
In the anti-acne facial cleanser composition of the present invention, except the above component, water is mended to aequum.
Compared with prior art, the present invention has the following advantages:
(1) anti-acne facial cleanser composition of the present invention to the skin action temperature and, do not stimulate eyes, and good antimicrobial effect, product used 5 days continuously, can obviously take effect.
(2) anti-acne facial cleanser composition of the present invention has the effect of good cleaning skin, washes the back skin moisturizing, does not have tight sense.
Preparation method
Anti-acne facial cleanser composition of the present invention can by any known or other effectively be applicable to the technology preparation that clean compositions is provided, the method for preparing anti-acne facial cleanser composition of the present invention comprises conventional preparation and hybrid technology.
Embodiment
Be the non-limiting example of anti-acne facial cleanser composition of the present invention below.Providing of these embodiment only is for illustrative purposes, can not be interpreted as limitation of the invention, because without departing from the spirit and scope of the present invention, can carry out many changes to the present invention.In these embodiments, unless stated otherwise, all concentration all is percentage by weight.Used term " small amount of matter " refers to those optional materials, and as antiseptic, essence, coloring agent etc., the selection of these small amount of matter will change in order to the physics for preparing special component of the present invention and chemical characteristic along with selected.Preparation example I-XV
The suitable method for preparing anti-acne facial cleanser composition described in example I-XV is as follows: suitable quantity of water is joined in the retort, under slowly stirring, add disodiumedetate, fatty acid, glycerol, be heated with stirring to 75 ℃, add the potassium hydroxide saponification, after finishing, saponification adds surfactant, pearlescent flake and wetting agent, stir the back cooling, treat that temperature reduces to 50 ℃, add antibacterial, add antiseptic, essence, coloring agent etc. after continuing to reduce to room temperature, randomly can add low amounts of water at last and supply.
Example I-V
Content (weight %)
Component
I II III IV V
Tetradecylic acid 4.0 6.0 8.0 9.0 10.0
Hexadecylic acid 8.0 7.0 8.0 6.0 5.0
Potassium hydroxide 2.0 2.3 2.8 2.6 2.7
Glycerol 3.0 3.0 3.0 3.0 3.0
Polyoxyethylene lauryl ether sodium sulfate 12.0 12.0 12.0 12.0 12.0
Cocos nucifera oil diglycollic amide 2.5 2.5 2.5 2.5 2.5
Isethionic acid six amidines 0.1 0.2 0.3 0.4 0.5
Oleum Ricini maleic acid glyceride 1.0 1.0 1.0 1.0 1.0
Pearlescent flake 0.0 3.0 3.0 3.0 3.0
Disodiumedetate 0.1 0.1 0.1 0.1 0.1
Antiseptic, essence, coloring agent are an amount of
Water adds to 100%
Example VI-X
Content (weight %)
Component
VI VII VIII IX X
Dodecoic acid 2.0 2.0 2.5 2.5 3.0
Tetradecylic acid 5.0 8.0 8.0 10.0 12.0
Hexadecylic acid 8.0 6.0 8.0 6.0 4.0
Potassium hydroxide 2.6 2.8 3.2 3.5 3.6
Glycerol 3.0 3.0 3.0 3.0 3.0
Polyoxyethylene lauryl ether sodium sulfate 10.0 10.0 10.0 10.0 10.0
Cocos nucifera oil diglycollic amide 2.5 2.5 2.5 2.5 2.5
The own amidine 0.02 0.04 0.06 0.08 0.1 of two isethionic acids
Cocos nucifera oil polyethyleneglycol glyceride 1.0 1.0 1.0 1.0 1.0
Pearlescent flake 0.0 3.0 3.0 3.0 3.0
Disodiumedetate 0.1 0.1 0.1 0.1 0.1
Antiseptic, essence, coloring agent are an amount of
Water adds to 100%
Optimum embodiment of the present invention is:
Constituent content (weight %)
Tetradecylic acid 8.0
Hexadecylic acid 5.0
Potassium hydroxide 2.1
Glycerol 3.0
Polyoxyethylene lauryl ether sodium sulfate 10
Cocos nucifera oil diglycollic amide 3.0
Oleum Ricini maleic acid glyceride 1.0
Isethionic acid six amidines 0.2
Pearlescent flake 3.0
Disodiumedetate 0.2
Antiseptic, essence, coloring agent are an amount of
Water adds to 100%
The optimum embodiment of the present invention is detected assessment.
1. basic the detection
Measure every physical and chemical index of anti-acne facial cleanser according to QB/T 1645-2004 prescriptive procedure.Testing result is as follows:
Product stability is by cold-resistant, heat-resistant experiment.
2. zest test
Skin irritation test repeatedly: earlier the hair of spinal column both sides, laboratory animal back skin is cut or shaved off, the unhairing scope respectively is 2.5cm * 2.5cm; Get and tried thing 0.1～0.5g and spread upon on the side skin, opposite side is coated with excipient in contrast, smears every day 1～2 time, smears continuously 14 days; Answer cropping before each coating, must not injured skin, guarantee that being tried thing fully contacts with skin.Observe dermoreaction and scoring every day.Test result: every day, every animal skin irritant reaction average product score value was 0.2, belonged to nonirritant.
Acute eye irritation experiment: liquid state or ointment 0.1g are tried thing be coated with in the laboratory animal one side conjunctival sac, another branch hole splashes into normal saline in contrast, make the passive closed 5～10s of eye after dripping medicine, record drips behind the medicine 6,24,48 and the local response of 72h eye, observes recovery situation on the the 4th, 7 day.Test result: it is 10.0 that the 6h eye stimulates the total mark meansigma methods, and it is 6.0 that the 24h eye stimulates the total mark meansigma methods, and it is 3.0 that the 48h eye stimulates the total mark meansigma methods, and it is 1.0 that the 72h eye stimulates the total mark meansigma methods, is slight stimulation.
3. anti-acne measure of merit
Select 25 experimenters of 19～25 years old that comedo is arranged, inform test objective, in detail explain anti-acne facial cleanser using method, follow up a case by regular visits to the untoward reaction that may occur in condition etc. and the test, the experimenter is be to enter this test after principle is signed Informed Consent Form voluntarily.Finish patch test before the test, the experimenter does not re-use other product for resolving poxes at duration of test.At the 0th day of test, the 5th day, the 10th day, the 20th day and the 30th day of including test in assessed the anti-acne effect of anti-acne facial cleanser.Test result: among 25 experimenters, 15 experimenters comedo in 5 days on probation is obviously controlled, and 8 experimenters obviously took effect in 5～10 days on probation, and 2 experimenters obviously took effect in 10～20 days on probation.Untoward reaction such as allergy, zest all do not appear in 25 experimenters.
Claims (8)
1. anti-acne facial cleanser composition, contain following:
(A) account for the fatty acid of composition weight 0.5% to 30.0%;
(B) account for the nertralizer of composition weight 0.05% to 6.0%;
(C) account for the surfactant of composition weight 0.1% to 20.0%;
(D) account for the wetting agent of composition weight 0.05% to 8.0%;
(E) account for the antibacterial of composition weight 0.01% to 1.5%; With
(F) surplus is a water.
2. anti-acne facial cleanser composition according to claim 1, described fatty acid are at least a in dodecoic acid, tetradecylic acid, hexadecylic acid, the stearic acid.
3. according to the anti-acne facial cleanser composition of aforementioned each claim, described nertralizer is a kind of in sodium hydroxide, potassium hydroxide, the triethanolamine.
4. according to the anti-acne facial cleanser composition of aforementioned each claim, described surfactant is at least a in aliphatic alcohol sulfate, fatty alcohol polyoxyethylene ether sulfate, alkylolamides, the betaines amphoteric surfactant.
5. according to the anti-acne facial cleanser composition of aforementioned each claim, described wetting agent is at least a in glycerol, propylene glycol, Oleum Ricini maleic acid glyceride, olein, the cocos nucifera oil polyethyleneglycol glyceride.
6. according to the anti-acne facial cleanser composition of aforementioned each claim, described antibacterial is isethionic acid six amidines, the own amidine of two isethionic acids, 3,4, at least a in 4-trichlorine diphenylurea, tea tree oil, the Aloe extraction solution.
7. according to the anti-acne facial cleanser composition of aforementioned each claim, can also contain the pearling agent that accounts for composition weight 0.0% to 5.0%.
8. according to the anti-acne facial cleanser composition of claim 1, specifically comprise:
Constituent content weight %
Tetradecylic acid 8.0
Hexadecylic acid 5.0
Potassium hydroxide 2.1
Glycerol 3.0
Polyoxyethylene lauryl ether sodium sulfate 10
Cocos nucifera oil diglycollic amide 3.0
Oleum Ricini maleic acid glyceride 1.0
Isethionic acid six amidines 0.2
Pearlescent flake 3.0
Disodiumedetate 0.2
Antiseptic, essence, coloring agent are an amount of
Water adds to 100%
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200910038307A CN101518505A (en) | 2009-03-31 | 2009-03-31 | Anti-acne facial cleanser composition |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200910038307A CN101518505A (en) | 2009-03-31 | 2009-03-31 | Anti-acne facial cleanser composition |
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| Publication Number | Publication Date |
|---|---|
| CN101518505A true CN101518505A (en) | 2009-09-02 |
Family
ID=41079445
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|---|---|---|---|
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101991514A (en) * | 2010-11-29 | 2011-03-30 | 陕西永泰生物工程有限责任公司 | Skin-smoothing and moisturizing sanitizer composition and preparation method thereof |
| CN102727391A (en) * | 2012-07-06 | 2012-10-17 | 澳宝化妆品（惠州）有限公司 | Mild moisturizing soap-based cleaning cream |
| CN103006507A (en) * | 2012-12-06 | 2013-04-03 | 南通市华东润滑设备有限公司 | Aloe facial cleaner |
| CN103142423A (en) * | 2013-04-01 | 2013-06-12 | 珀莱雅化妆品股份有限公司 | Soap-based cleansing cream not generating soap scum |
| CN103655229A (en) * | 2013-12-05 | 2014-03-26 | 青岛海芬海洋生物科技有限公司 | Facial cleanser containing algal polysaccharide |
| CN104224620A (en) * | 2014-09-02 | 2014-12-24 | 青岛永通电梯工程有限公司 | Acne treating facial cleanser |
| CN105213222A (en) * | 2015-06-30 | 2016-01-06 | 朱耀灯 | The oily anti-acne of a kind of control is clean to be showed and preparation method thereof |
| CN106999377A (en) * | 2014-12-18 | 2017-08-01 | 高露洁-棕榄公司 | Liquid cleansing agent |
| CN109666545A (en) * | 2018-12-28 | 2019-04-23 | 中山市天图精细化工有限公司 | A kind of efficient cleaning toilet foam aerosol and preparation method thereof |
-
2009
- 2009-03-31 CN CN200910038307A patent/CN101518505A/en active Pending
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101991514A (en) * | 2010-11-29 | 2011-03-30 | 陕西永泰生物工程有限责任公司 | Skin-smoothing and moisturizing sanitizer composition and preparation method thereof |
| CN101991514B (en) * | 2010-11-29 | 2012-05-30 | 陕西永泰生物工程有限责任公司 | Skin-smoothing and moisturizing sanitizer composition and preparation method thereof |
| CN102727391A (en) * | 2012-07-06 | 2012-10-17 | 澳宝化妆品（惠州）有限公司 | Mild moisturizing soap-based cleaning cream |
| CN103006507A (en) * | 2012-12-06 | 2013-04-03 | 南通市华东润滑设备有限公司 | Aloe facial cleaner |
| CN103142423A (en) * | 2013-04-01 | 2013-06-12 | 珀莱雅化妆品股份有限公司 | Soap-based cleansing cream not generating soap scum |
| CN103655229A (en) * | 2013-12-05 | 2014-03-26 | 青岛海芬海洋生物科技有限公司 | Facial cleanser containing algal polysaccharide |
| CN104224620A (en) * | 2014-09-02 | 2014-12-24 | 青岛永通电梯工程有限公司 | Acne treating facial cleanser |
| CN106999377A (en) * | 2014-12-18 | 2017-08-01 | 高露洁-棕榄公司 | Liquid cleansing agent |
| CN106999377B (en) * | 2014-12-18 | 2020-10-09 | 高露洁-棕榄公司 | Liquid skin cleaning agent |
| CN105213222A (en) * | 2015-06-30 | 2016-01-06 | 朱耀灯 | The oily anti-acne of a kind of control is clean to be showed and preparation method thereof |
| CN109666545A (en) * | 2018-12-28 | 2019-04-23 | 中山市天图精细化工有限公司 | A kind of efficient cleaning toilet foam aerosol and preparation method thereof |
| CN109666545B (en) * | 2018-12-28 | 2020-10-02 | 中山市天图精细化工有限公司 | Efficient toilet cleaning foam aerosol and preparation method thereof |
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Open date: 20090902 |