CN101513994A - 一种铋基储氢材料及其制备方法 - Google Patents
一种铋基储氢材料及其制备方法 Download PDFInfo
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- CN101513994A CN101513994A CNA2009100473396A CN200910047339A CN101513994A CN 101513994 A CN101513994 A CN 101513994A CN A2009100473396 A CNA2009100473396 A CN A2009100473396A CN 200910047339 A CN200910047339 A CN 200910047339A CN 101513994 A CN101513994 A CN 101513994A
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- bismuth
- hydrogen storage
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- storage material
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- 229910052739 hydrogen Inorganic materials 0.000 title claims abstract description 43
- 239000001257 hydrogen Substances 0.000 title claims abstract description 43
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 title claims abstract description 37
- 238000002360 preparation method Methods 0.000 title claims abstract description 36
- 229910052797 bismuth Inorganic materials 0.000 title claims abstract description 35
- JCXGWMGPZLAOME-UHFFFAOYSA-N bismuth atom Chemical compound [Bi] JCXGWMGPZLAOME-UHFFFAOYSA-N 0.000 title claims abstract description 35
- 239000011232 storage material Substances 0.000 title claims abstract description 22
- 239000011669 selenium Substances 0.000 claims abstract description 35
- 238000006243 chemical reaction Methods 0.000 claims abstract description 27
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 26
- 238000003860 storage Methods 0.000 claims abstract description 24
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 22
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 claims abstract description 13
- 238000000034 method Methods 0.000 claims abstract description 13
- 229910052711 selenium Inorganic materials 0.000 claims abstract description 10
- 229910052714 tellurium Inorganic materials 0.000 claims abstract description 10
- PORWMNRCUJJQNO-UHFFFAOYSA-N tellurium atom Chemical compound [Te] PORWMNRCUJJQNO-UHFFFAOYSA-N 0.000 claims abstract description 10
- 235000019154 vitamin C Nutrition 0.000 claims abstract description 10
- 239000011718 vitamin C Substances 0.000 claims abstract description 10
- 239000007791 liquid phase Substances 0.000 claims abstract description 6
- 150000001621 bismuth Chemical class 0.000 claims abstract description 5
- MGFYIUFZLHCRTH-UHFFFAOYSA-N nitrilotriacetic acid Chemical compound OC(=O)CN(CC(O)=O)CC(O)=O MGFYIUFZLHCRTH-UHFFFAOYSA-N 0.000 claims abstract description 5
- 239000012279 sodium borohydride Substances 0.000 claims abstract description 5
- 229910000033 sodium borohydride Inorganic materials 0.000 claims abstract description 5
- 239000002904 solvent Substances 0.000 claims abstract description 5
- FXADMRZICBQPQY-UHFFFAOYSA-N orthotelluric acid Chemical compound O[Te](O)(O)(O)(O)O FXADMRZICBQPQY-UHFFFAOYSA-N 0.000 claims abstract description 3
- MCAHWIHFGHIESP-UHFFFAOYSA-N selenous acid Chemical compound O[Se](O)=O MCAHWIHFGHIESP-UHFFFAOYSA-N 0.000 claims abstract description 3
- SITVSCPRJNYAGV-UHFFFAOYSA-N tellurous acid Chemical compound O[Te](O)=O SITVSCPRJNYAGV-UHFFFAOYSA-N 0.000 claims abstract description 3
- FBGGJHZVZAAUKJ-UHFFFAOYSA-N bismuth selenide Chemical compound [Se-2].[Se-2].[Se-2].[Bi+3].[Bi+3] FBGGJHZVZAAUKJ-UHFFFAOYSA-N 0.000 claims abstract 7
- 239000000843 powder Substances 0.000 claims description 14
- 230000002829 reductive effect Effects 0.000 claims description 13
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 12
- 235000011114 ammonium hydroxide Nutrition 0.000 claims description 12
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 10
- 239000002086 nanomaterial Substances 0.000 claims description 10
- 239000011734 sodium Substances 0.000 claims description 8
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims description 6
- 229910017604 nitric acid Inorganic materials 0.000 claims description 6
- 229910001451 bismuth ion Inorganic materials 0.000 claims description 5
- 238000003756 stirring Methods 0.000 claims description 4
- YGDVXSDNEFDTGV-UHFFFAOYSA-N 2-[6-[bis(carboxymethyl)amino]hexyl-(carboxymethyl)amino]acetic acid Chemical compound OC(=O)CN(CC(O)=O)CCCCCCN(CC(O)=O)CC(O)=O YGDVXSDNEFDTGV-UHFFFAOYSA-N 0.000 claims description 3
- XHGGEBRKUWZHEK-UHFFFAOYSA-L tellurate Chemical compound [O-][Te]([O-])(=O)=O XHGGEBRKUWZHEK-UHFFFAOYSA-L 0.000 claims description 2
- 230000001105 regulatory effect Effects 0.000 claims 1
- 239000007772 electrode material Substances 0.000 abstract description 6
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 abstract description 5
- 229910052744 lithium Inorganic materials 0.000 abstract description 5
- 239000000463 material Substances 0.000 abstract description 5
- 230000015572 biosynthetic process Effects 0.000 abstract description 4
- 238000003786 synthesis reaction Methods 0.000 abstract description 4
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 239000002994 raw material Substances 0.000 abstract description 2
- 229940091258 selenium supplement Drugs 0.000 abstract 3
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 abstract 2
- 239000013078 crystal Substances 0.000 abstract 2
- NAQMVNRVTILPCV-UHFFFAOYSA-N hexane-1,6-diamine Chemical compound NCCCCCCN NAQMVNRVTILPCV-UHFFFAOYSA-N 0.000 abstract 2
- XSOKHXFFCGXDJZ-UHFFFAOYSA-N telluride(2-) Chemical compound [Te-2] XSOKHXFFCGXDJZ-UHFFFAOYSA-N 0.000 abstract 2
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 abstract 1
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical class [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 abstract 1
- 229930003268 Vitamin C Natural products 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- JHXKRIRFYBPWGE-UHFFFAOYSA-K bismuth chloride Chemical compound Cl[Bi](Cl)Cl JHXKRIRFYBPWGE-UHFFFAOYSA-K 0.000 abstract 1
- 239000003638 chemical reducing agent Substances 0.000 abstract 1
- BVTBRVFYZUCAKH-UHFFFAOYSA-L disodium selenite Chemical class [Na+].[Na+].[O-][Se]([O-])=O BVTBRVFYZUCAKH-UHFFFAOYSA-L 0.000 abstract 1
- RXPAJWPEYBDXOG-UHFFFAOYSA-N hydron;methyl 4-methoxypyridine-2-carboxylate;chloride Chemical compound Cl.COC(=O)C1=CC(OC)=CC=N1 RXPAJWPEYBDXOG-UHFFFAOYSA-N 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
- 150000003342 selenium Chemical class 0.000 abstract 1
- 125000003748 selenium group Chemical group *[Se]* 0.000 abstract 1
- 229960001471 sodium selenite Drugs 0.000 abstract 1
- 239000011781 sodium selenite Chemical class 0.000 abstract 1
- 235000015921 sodium selenite Nutrition 0.000 abstract 1
- 229910052938 sodium sulfate Inorganic materials 0.000 abstract 1
- 235000011152 sodium sulphate Nutrition 0.000 abstract 1
- VOADVZVYWFSHSM-UHFFFAOYSA-L sodium tellurite Chemical compound [Na+].[Na+].[O-][Te]([O-])=O VOADVZVYWFSHSM-UHFFFAOYSA-L 0.000 abstract 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 12
- OMEPJWROJCQMMU-UHFFFAOYSA-N selanylidenebismuth;selenium Chemical compound [Se].[Bi]=[Se].[Bi]=[Se] OMEPJWROJCQMMU-UHFFFAOYSA-N 0.000 description 9
- -1 bismuthino compound Chemical class 0.000 description 7
- 238000005119 centrifugation Methods 0.000 description 7
- 239000004698 Polyethylene Substances 0.000 description 6
- 239000003125 aqueous solvent Substances 0.000 description 6
- 239000012153 distilled water Substances 0.000 description 6
- 238000001704 evaporation Methods 0.000 description 6
- 230000008020 evaporation Effects 0.000 description 6
- 150000002431 hydrogen Chemical class 0.000 description 6
- 238000009413 insulation Methods 0.000 description 6
- 229920000573 polyethylene Polymers 0.000 description 6
- 238000007789 sealing Methods 0.000 description 6
- 238000001291 vacuum drying Methods 0.000 description 6
- 150000001875 compounds Chemical class 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 3
- 239000013543 active substance Substances 0.000 description 3
- 238000004458 analytical method Methods 0.000 description 3
- 238000011161 development Methods 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 238000011056 performance test Methods 0.000 description 3
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 description 2
- 238000002441 X-ray diffraction Methods 0.000 description 2
- 230000003321 amplification Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 238000003199 nucleic acid amplification method Methods 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 239000004065 semiconductor Substances 0.000 description 2
- 238000007704 wet chemistry method Methods 0.000 description 2
- 229910005438 FeTi Inorganic materials 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- 229910045601 alloy Inorganic materials 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000009977 dual effect Effects 0.000 description 1
- 238000004134 energy conservation Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229910052987 metal hydride Inorganic materials 0.000 description 1
- 150000004681 metal hydrides Chemical class 0.000 description 1
- 238000000593 microemulsion method Methods 0.000 description 1
- 239000011858 nanopowder Substances 0.000 description 1
- 229910052763 palladium Inorganic materials 0.000 description 1
- 239000012071 phase Substances 0.000 description 1
- 230000005622 photoelectricity Effects 0.000 description 1
- 238000000634 powder X-ray diffraction Methods 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 239000002243 precursor Substances 0.000 description 1
- 239000002594 sorbent Substances 0.000 description 1
- 238000010189 synthetic method Methods 0.000 description 1
- 230000005619 thermoelectricity Effects 0.000 description 1
Images
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
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- Inorganic Compounds Of Heavy Metals (AREA)
Abstract
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Cited By (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102020253A (zh) * | 2010-11-09 | 2011-04-20 | 北京大学 | 一种拓扑绝缘体材料及其制备方法 |
CN101746738B (zh) * | 2009-09-29 | 2011-06-29 | 武汉理工大学 | 纳米片状Bi2Se3热电化合物的制备方法 |
CN103058151A (zh) * | 2013-01-16 | 2013-04-24 | 吉林大学 | 一种分级结构的碲化铋纳米晶及其制备方法 |
CN103086331A (zh) * | 2013-03-01 | 2013-05-08 | 浙江大学 | 一种超薄硒化铋二元化合物纳米片的制备方法 |
CN103896222A (zh) * | 2012-12-24 | 2014-07-02 | 中国科学技术大学 | 超薄纳米片半导体材料及其制备方法和应用 |
CN106450300A (zh) * | 2016-11-01 | 2017-02-22 | 中南大学 | 一种具有花状结构的焦磷酸铁钠材料及其制备方法和应用 |
CN110660898A (zh) * | 2019-10-10 | 2020-01-07 | 中国科学院电工研究所 | 一种柔性热电薄膜的制备方法 |
CN112281183A (zh) * | 2020-09-16 | 2021-01-29 | 华南理工大学 | 团簇状硒化铋及其制备方法与电催化还原二氧化碳的应用 |
CN113755878A (zh) * | 2021-08-31 | 2021-12-07 | 北京大学深圳研究生院 | 一种铋基催化剂的制备方法和应用 |
CN116813347A (zh) * | 2023-05-22 | 2023-09-29 | 合肥睿力工业科技有限公司 | 一种碲化铋复合材料及其制备方法、应用 |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN100560479C (zh) * | 2008-06-17 | 2009-11-18 | 浙江大学 | 一种Bi2Te3纳米薄片的制备方法 |
-
2009
- 2009-03-10 CN CN2009100473396A patent/CN101513994B/zh active Active
Cited By (16)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101746738B (zh) * | 2009-09-29 | 2011-06-29 | 武汉理工大学 | 纳米片状Bi2Se3热电化合物的制备方法 |
CN102020253A (zh) * | 2010-11-09 | 2011-04-20 | 北京大学 | 一种拓扑绝缘体材料及其制备方法 |
CN102020253B (zh) * | 2010-11-09 | 2012-01-25 | 北京大学 | 一种拓扑绝缘体材料及其制备方法 |
CN103896222A (zh) * | 2012-12-24 | 2014-07-02 | 中国科学技术大学 | 超薄纳米片半导体材料及其制备方法和应用 |
CN103896222B (zh) * | 2012-12-24 | 2016-01-20 | 中国科学技术大学 | 超薄纳米片半导体材料的制备方法 |
CN103058151A (zh) * | 2013-01-16 | 2013-04-24 | 吉林大学 | 一种分级结构的碲化铋纳米晶及其制备方法 |
CN103058151B (zh) * | 2013-01-16 | 2015-02-04 | 吉林大学 | 一种分级结构的碲化铋纳米晶及其制备方法 |
CN103086331A (zh) * | 2013-03-01 | 2013-05-08 | 浙江大学 | 一种超薄硒化铋二元化合物纳米片的制备方法 |
CN106450300A (zh) * | 2016-11-01 | 2017-02-22 | 中南大学 | 一种具有花状结构的焦磷酸铁钠材料及其制备方法和应用 |
CN106450300B (zh) * | 2016-11-01 | 2019-05-03 | 中南大学 | 一种具有花状结构的焦磷酸铁钠材料及其制备方法和应用 |
CN110660898A (zh) * | 2019-10-10 | 2020-01-07 | 中国科学院电工研究所 | 一种柔性热电薄膜的制备方法 |
CN110660898B (zh) * | 2019-10-10 | 2023-02-07 | 中国科学院电工研究所 | 一种柔性热电薄膜的制备方法 |
CN112281183A (zh) * | 2020-09-16 | 2021-01-29 | 华南理工大学 | 团簇状硒化铋及其制备方法与电催化还原二氧化碳的应用 |
CN112281183B (zh) * | 2020-09-16 | 2022-01-18 | 华南理工大学 | 团簇状硒化铋及其制备方法与电催化还原二氧化碳的应用 |
CN113755878A (zh) * | 2021-08-31 | 2021-12-07 | 北京大学深圳研究生院 | 一种铋基催化剂的制备方法和应用 |
CN116813347A (zh) * | 2023-05-22 | 2023-09-29 | 合肥睿力工业科技有限公司 | 一种碲化铋复合材料及其制备方法、应用 |
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Publication number | Publication date |
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CN101513994B (zh) | 2011-10-05 |
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Address after: 215400 No.6 Liangfu Road, Taicang City, Suzhou City, Jiangsu Province Patentee after: Jiangsu Institute of advanced inorganic materials Address before: No. 6 Liangfu Road, Taicang City, Jiangsu Province, 215400 Patentee before: SUZHOU Research Institute SHANGHAI INSTITUTE OF CERAMICS CHINESE ACADEMY OF SCIENCES |
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