CN101265130A - Process for preparing kelp holdfast and oyster shell composite biological preparation by microwave technique - Google Patents
Process for preparing kelp holdfast and oyster shell composite biological preparation by microwave technique Download PDFInfo
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- CN101265130A CN101265130A CNA200810015600XA CN200810015600A CN101265130A CN 101265130 A CN101265130 A CN 101265130A CN A200810015600X A CNA200810015600X A CN A200810015600XA CN 200810015600 A CN200810015600 A CN 200810015600A CN 101265130 A CN101265130 A CN 101265130A
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
- Y02A40/10—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in agriculture
- Y02A40/20—Fertilizers of biological origin, e.g. guano or fertilizers made from animal corpses
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Abstract
The invention relates to a method for producing a liquid extract capable of promoting growth and development of plants, more particularly to a method for extracting effective components for regulating and promoting growth and development of plants, from wastes after sea tangle and oyster processing, and producing leaf surface biological preparations easily absorbed by plants. The method comprises the following steps: 1. raw material treatment; 2. alcoholization in a sea tangle fixer; 3. addition of oyster shell in the sea tangle fixe; 4. microwave treatment; 5. material filtration; and 6. sterilization. The inventive compound biological preparation is widely used as foliage spray fertilizer for industrial crops such as rape, tomato, coriander, cabbage, garland chrysanthemum, enteromorpha linza, cucumber, white gourd, potato, peanut, wheat and maize; fruit trees and flowers; and also used for seed soaking treatment of various crops. The biological preparation can promote seed germination, improve the resistance in seedlings, promote the growth and development of seedlings, improve the related physiological indexes, and increase the yield and quality of economic plants.
Description
Technical field:
The present invention relates to a kind of production technique that promotes plant-growth, grows required extracting solution, particularly from the processing waste material of marine organisms sea-tangle and oyster, extract and to regulate, promote plant-growth, grow required effective constituent and be prepared into the method for the blade face biotechnological formulation that is fit to plant absorbing.
Background technology:
As everyone knows, marine organisms green manure (composite biological agent) is meant and utilizes marine organisms (waste material that mainly utilizes the course of processing to produce) to be main raw material, the biotechnological formulation that adopts up-to-date biotechnology, physical technique and special chemical industry technology to produce.It contains farm crop, fruit tree, flowers and reproducting tree species such as nitrogen, phosphorus, potassium, calcium, magnesium, iron, zinc, manganese, silicon, boron, the molybdenum useful element that grows; Contain compositions such as the necessary biologically active substance of a large amount of plant metabolisms, organic substance, amino acid, humic acid simultaneously.
The use of composite biological agent can be regulated Soil structure, improves the soil permeability energy, reduce interionic antagonistic action, realizes the eubiosis; Solve because the soil compaction problem that long-term a large amount of single administration chemical fertilizer causes improves the soil biochemistry activity; Eliminate chemical decomposition fertilizer residual in soil, improve effective specific absorption of fertilizer; Can suppress the harmful microorganism in the soil, thereby improve the diseases and insect pests resistance of farm crop; Reduce the pollution of chemical fertilizer, reduce and drop into, can also improve output and crop quality environment.Composite biological agent has the incomparable advantage of general chemical fertilizer.
In view of its all advantage, the scholar who is engaged in biotechnology, applied chemistry and association area both at home and abroad inquires into the production technology of green fertilizer, has done many exploitations and research work.Consult documents and materials and domestic and international part is shown with investigation biological, that chemistry is the enterprise of technical support by us: this field work now mainly lays particular emphasis on the following aspects: 1. bacterial manure and bush mycorrhizal fungi combine the production composite biological fertilizer; 2. using the biotechnology means, is the raw material production green fertilizer with non-economy organs such as stalk of farm crop etc.; 3. the part scholar produces starting material, exploitation composite biological agent, but complex process; The raw material resources of being utilized simultaneously are not suitable for the structure of marine industries; The fertilizer of 4. most research work exploitation, to edaphic factor consider not enough, directly have influence on the extensive popularization of composite biological agent; 5. in addition, the composite biological agent of research is not considered the difference between species of farm crop, fruit tree, flowers and the concrete species of reproducting tree species comprehensively.
Summary of the invention:
The objective of the invention is to overcome above-mentioned the deficiencies in the prior art, a kind of marine biotechnology means of utilizing are provided, obtain the composite biological agent and the production technique thereof that promote growth and development of plants.
The present invention can reach by following measure:
Microwave technology prepares the technology of sea-tangle holdfast and oyster shell composite biological preparation, and step comprises:
1, the starting material that are used for production technique are handled,
1.1 sea-tangle holdfast (Radix Laminariae) pre-treatment:
The sea-tangle holdfast has two kinds of treatment processs as starting material:
Fresh holdfast can promptly get standby raw material by cryopreservation → thaw → wash → quantitatively, add 1-2 times of water through organizing Mechanical Crushing,
Drying holdfast can promptly get standby raw material by washing → purification → drying → grind → sieve (200-400 order),
1.2 oyster shells pre-treatment:
Oyster shells → impurity elimination thing → 800-1200 ℃ pyroprocessing → fragmentation → standby raw material,
2, sea-tangle holdfast alcoholization,
In the sea-tangle holdfast raw material with the pre-treatment gained, low mass molecule alcohol classes such as the ethanol of interpolation 70%-85%, Virahol, mechanical stirring 0.5-2 hour,
3, add oyster shells in the sea-tangle holdfast,
Take by weighing oyster shells through the pre-treatment gained, dissolving in oyster shells takes by weighing in the weight 50-100 pure water doubly and dissolves in the pure water, heat 100 ℃-150 ℃ and stirring, filtration residue gets the oyster shells treatment solution, pH value is stabilized between 13.0-14.0, get the oyster shells treatment solution, regulate its pH value 8.0-9.5, stirring at normal temperature in the liquid of adding step 2 gained, standby
4, microwave treatment,
Microwave treatment radiated time 5-10min, microwave power 800-1200W, solvent load 1/4-1/2,
5, filtration of material,
With the cooling of the substance solution of microwave treatment gained, adding with the kelp is the acid fermentation liquid neutralization of main matrix, and the potential of hydrogen of regulator solution is to neutral, filter the thick liquid of composite biological agent,
6, underpressure distillation,
Adopt reduced pressure distillation process to concentrate thick liquid, temperature is controlled between 45-60 ℃,
7, add tensio-active agent,
Increase the tensio-active agent-polyoxyethylene sorbitan monooleate to biological growth and development, product quality, Environmental indicators, the no any negative impact of import and export quarantine, addition is the 1/1000-1/500 of leaf dressing amount concentration,
8, sterilization
Adopt ultraviolet or chemical process sterilization.
Composite biological agent of the present invention can be widely used in the foliage application of cash crop, fruit tree and flowers (particularly watch leaf flower) such as rape, tomato, coriander, Chinese cabbage, crowndaisy chrysanthemum, green moss, cucumber, wax gourd, potato, peanut, wheat, corn.Simultaneously, composite biological agent of the present invention can be used for the seed soaking of various crop to be handled, and not only promotes the sprouting of seed, and obviously improves the resistance of seedling, promotes growth of seedlings to grow, and improves the relevant physiological index, improves output and the quality of economic plants.
The using method of composite biological agent of the present invention is: the general dilute with water 400-600 that soaks seed doubly; The general dilute with water 500-1000 of leaf dressing doubly; The consumption that general cash crop are every mu is 15-30ml.
Embodiment:
Below the present invention is further described:
Composite biological agent production technique of the present invention mainly comprises:
1, the starting material that are used for production technique are handled,
1.1 sea-tangle holdfast (Radix Laminariae) pre-treatment,
The sea-tangle holdfast has two kinds of treatment processs as starting material:
Fresh holdfast promptly gets standby raw material by cryopreservation → thaw → wash → quantitatively, add 1-2 times of water through organizing Mechanical Crushing,
Drying holdfast promptly gets standby raw material by washing → purification → drying → grind → sieve (200-400 order),
1.2 oyster shells pre-treatment: oyster shells → impurity elimination thing → 800-1200 ℃ pyroprocessing → fragmentation → standby raw material,
2, sea-tangle holdfast alcoholization
In the sea-tangle holdfast raw material with the pre-treatment gained, low mass molecule alcohol classes such as the ethanol of interpolation 70%-85%, Virahol, mechanical stirring 0.5-2 hour,
3, add oyster shells in the sea-tangle holdfast,
Take by weighing the oyster shells through the pre-treatment gained, dissolve in oyster shells and take by weighing in the weight 50-100 pure water doubly, heat 100 ℃-150 ℃ and stir, filtration residue must the oyster shells treatment solution, and pH value is stabilized between 13.0-14.0.Get the oyster shells treatment solution, add in the liquid of step 2 gained, come the pH value of regulating step 2 gained liquid with the oyster shells treatment solution, pH value is 8.0-9.5, and stirring at normal temperature is standby,
4, microwave treatment,
Microwave processing process is a key problem in technology of the present invention.Microwave-assisted extraction technique has easy quick, few, the rate of recovery advantages of higher of reagent dosage as a kind of novel pre-treatment means.Key factor: microwave irradiation time, microwave power, solvent load are to three indexs: the influence of extraction yield, solvent recovering rate, extracting solution total content, composite biological agent production technique of the present invention, the microwave treatment best of breed of requirement are radiated time 5-10min, microwave power 800-1200W, solvent load 1/4-1/2.
5, filtration of material,
With the substance solution naturally cooling of microwave treatment gained, adding with the kelp is the acid fermentation liquid neutralization of main matrix, and the potential of hydrogen of regulator solution is to neutral; Filter the thick liquid of composite biological agent.
6, underpressure distillation
Composite biological agent adopts reduced pressure distillation process to concentrate thick liquid, and temperature is controlled between 45-60 ℃.
7, add tensio-active agent
The composite biological agent of gained of the present invention can directly carry out foliage application to most economic plants.But for blade wax, the higher plant of siliceous equal size, on the basis of above-mentioned operational path, can increase the tensio-active agent-polyoxyethylene sorbitan monooleate (food grade) to biological growth and development, product quality, Environmental indicators, the no any negative impact of import and export quarantine, addition is the 1/1000-1/500 of leaf dressing amount concentration.
8, sterilization
Adopt ultraviolet or chemical process sterilization to get final product.
Composite biological agent of the present invention can be widely used in the foliage application of cash crop, fruit tree and flowers (particularly watch leaf flower) such as rape, tomato, coriander, Chinese cabbage, crowndaisy chrysanthemum, green moss, cucumber, wax gourd, potato, peanut, wheat, corn.Simultaneously, composite biological agent of the present invention can be used for the seed soaking of various crop to be handled, and not only promotes the sprouting of seed, and obviously improves the resistance of seedling, promotes growth of seedlings to grow, and improves the relevant physiological index, improves output and the quality of economic plants.
The using method of composite biological agent of the present invention is: the general dilute with water 400-600 that soaks seed doubly; The general dilute with water 500-1000 of leaf dressing doubly; The consumption that general cash crop are every mu is 15-30ml.
Claims (3)
1, a kind of microwave technology prepares the technology of sea-tangle holdfast and oyster shell composite biological preparation, and its feature comprises the steps:
(1), starting material handle,
1.1 the pre-treatment of sea-tangle holdfast:
The sea-tangle holdfast has two kinds of treatment processs as starting material:
Fresh holdfast promptly gets standby raw material by cryopreservation → thaw → wash → quantitatively, add 1-2 times of water through organizing Mechanical Crushing;
Drying holdfast promptly gets standby raw material by washing → purification → drying → grind → sieve (200-400 order),
1.2 oyster shells pre-treatment:
Oyster shells → impurity elimination thing → 800-1200 ℃ pyroprocessing → fragmentation → standby raw material.
(2), sea-tangle holdfast alcoholization,
In the sea-tangle holdfast raw material of pre-treatment gained, add the low mass molecule alcohol class of 70%-85%, mechanical stirring 0.5-2 hour,
(3), add oyster shells in the sea-tangle holdfast,
Take by weighing oyster shells through the pre-treatment gained, dissolve in the oyster shells weight 50-100 pure water doubly, heat 100 ℃-150 ℃ and stirring, filtration residue, get the oyster shells treatment solution, pH value is stabilized between 13.0-14.0, gets the oyster shells treatment solution, adds in the liquid of step (2) gained, regulating its pH value with the oyster shells treatment solution is 8.0-9.5, stirring at normal temperature gets reserve liquid
(4), microwave treatment,
Reserve liquid is carried out microwave treatment, radiated time 5-10min, microwave power 800-1200W, solvent load 1/4-1/2,
(5), filtration of material,
With the cooling of the substance solution of microwave treatment gained, adding with the kelp is the acid fermentation liquid neutralization of main matrix, and the potential of hydrogen of regulator solution is to neutral, filter composite biological agent liquid.
2, a kind of microwave technology according to claim 1 prepares the technology of sea-tangle holdfast and oyster shell composite biological preparation, it is characterized in that adopting reduced pressure distillation process to concentrate the composite biological agent liquid of gained, temperature is controlled between 45-60 ℃, add tensio-active agent again, addition is the 1/1000-1/500 of leaf dressing amount concentration, and sterilization gets final product then.
3, a kind of microwave technology according to claim 2 prepares the technology of sea-tangle holdfast and oyster shell composite biological preparation, it is characterized in that tensio-active agent is a polyoxyethylene sorbitan monooleate.
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| Application Number | Priority Date | Filing Date | Title |
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| CN200810015600XA CN101265130B (en) | 2008-04-21 | 2008-04-21 | Process for preparing kelp holdfast and oyster shell composite biological preparation by microwave technique |
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| CN200810015600XA CN101265130B (en) | 2008-04-21 | 2008-04-21 | Process for preparing kelp holdfast and oyster shell composite biological preparation by microwave technique |
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| CN101265130A true CN101265130A (en) | 2008-09-17 |
| CN101265130B CN101265130B (en) | 2011-03-16 |
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| CN200810015600XA Expired - Fee Related CN101265130B (en) | 2008-04-21 | 2008-04-21 | Process for preparing kelp holdfast and oyster shell composite biological preparation by microwave technique |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103011971A (en) * | 2012-12-26 | 2013-04-03 | 福建超大集团有限公司 | Manufacturing method of compound organic fertilizer with fertilizer-retaining and loss-controlling functions |
| CN103011972A (en) * | 2012-12-26 | 2013-04-03 | 福建超大集团有限公司 | Manufacture method of synergic type nitrogenous fertilizer with slow release and loss control effect |
| CN103011970A (en) * | 2012-12-26 | 2013-04-03 | 福建超大集团有限公司 | Manufacturing method of multifunctional humic acid fertilizer with water retention and fertilizer retention functions |
| CN106480010A (en) * | 2017-01-04 | 2017-03-08 | 烟台固特丽生物科技股份有限公司 | A kind of preparation of immobilization agricultural microbial agent and application process |
| CN107083847A (en) * | 2017-04-21 | 2017-08-22 | 孙祎 | A kind of method that utilization oyster shell and microorganism repair masonry |
| CN111908982A (en) * | 2020-08-10 | 2020-11-10 | 济南航晨生物科技有限公司 | Method for extracting seaweed by electromagnetic radiation |
-
2008
- 2008-04-21 CN CN200810015600XA patent/CN101265130B/en not_active Expired - Fee Related
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103011971A (en) * | 2012-12-26 | 2013-04-03 | 福建超大集团有限公司 | Manufacturing method of compound organic fertilizer with fertilizer-retaining and loss-controlling functions |
| CN103011972A (en) * | 2012-12-26 | 2013-04-03 | 福建超大集团有限公司 | Manufacture method of synergic type nitrogenous fertilizer with slow release and loss control effect |
| CN103011970A (en) * | 2012-12-26 | 2013-04-03 | 福建超大集团有限公司 | Manufacturing method of multifunctional humic acid fertilizer with water retention and fertilizer retention functions |
| CN106480010A (en) * | 2017-01-04 | 2017-03-08 | 烟台固特丽生物科技股份有限公司 | A kind of preparation of immobilization agricultural microbial agent and application process |
| CN107083847A (en) * | 2017-04-21 | 2017-08-22 | 孙祎 | A kind of method that utilization oyster shell and microorganism repair masonry |
| CN107083847B (en) * | 2017-04-21 | 2019-08-23 | 广州新城建筑设计院有限公司 | A method of masonry is repaired using oyster shell and microorganism |
| CN111908982A (en) * | 2020-08-10 | 2020-11-10 | 济南航晨生物科技有限公司 | Method for extracting seaweed by electromagnetic radiation |
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| CN101265130B (en) | 2011-03-16 |
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Granted publication date: 20110316 Termination date: 20120421 |