CN101031538B - 对苯二甲酸的优化纯化生产 - Google Patents

对苯二甲酸的优化纯化生产 Download PDF

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Publication number
CN101031538B
CN101031538B CN2005800290037A CN200580029003A CN101031538B CN 101031538 B CN101031538 B CN 101031538B CN 2005800290037 A CN2005800290037 A CN 2005800290037A CN 200580029003 A CN200580029003 A CN 200580029003A CN 101031538 B CN101031538 B CN 101031538B
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CN
China
Prior art keywords
mixture
liquid
solids
solid
solids content
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
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CN2005800290037A
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English (en)
Chinese (zh)
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CN101031538A (zh
Inventor
林鑫
R·S·奥米德拉
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Grupo Petrotemex SA de CV
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Eastman Chemical Co
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Publication of CN101031538A publication Critical patent/CN101031538A/zh
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/0018—Evaporation of components of the mixture to be separated
    • B01D9/0022—Evaporation of components of the mixture to be separated by reducing pressure
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/0018—Evaporation of components of the mixture to be separated
    • B01D9/0031—Evaporation of components of the mixture to be separated by heating
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/0059—General arrangements of crystallisation plant, e.g. flow sheets
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/255—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting
    • C07C51/265—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting having alkyl side chains which are oxidised to carboxyl groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/487—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
CN2005800290037A 2004-09-02 2005-08-29 对苯二甲酸的优化纯化生产 Expired - Lifetime CN101031538B (zh)

Applications Claiming Priority (7)

Application Number Priority Date Filing Date Title
US60680704P 2004-09-02 2004-09-02
US60673504P 2004-09-02 2004-09-02
US60/606,807 2004-09-02
US60/606,735 2004-09-02
US11/191,766 2005-07-28
US11/191,766 US7615663B2 (en) 2004-09-02 2005-07-28 Optimized production of aromatic dicarboxylic acids
PCT/US2005/030661 WO2006028773A2 (en) 2004-09-02 2005-08-29 Optimized purification production of terephthalic acid

Publications (2)

Publication Number Publication Date
CN101031538A CN101031538A (zh) 2007-09-05
CN101031538B true CN101031538B (zh) 2012-03-28

Family

ID=35613863

Family Applications (1)

Application Number Title Priority Date Filing Date
CN2005800290037A Expired - Lifetime CN101031538B (zh) 2004-09-02 2005-08-29 对苯二甲酸的优化纯化生产

Country Status (9)

Country Link
US (1) US7615663B2 (https=)
EP (1) EP1861350A2 (https=)
CN (1) CN101031538B (https=)
BR (1) BRPI0514767A (https=)
CA (1) CA2576323A1 (https=)
IN (1) IN2014DN08961A (https=)
MX (1) MX2007002505A (https=)
TW (1) TW200621702A (https=)
WO (1) WO2006028773A2 (https=)

Families Citing this family (36)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7741515B2 (en) 2004-09-02 2010-06-22 Eastman Chemical Company Optimized liquid-phase oxidation
US7586000B2 (en) * 2004-09-02 2009-09-08 Eastman Chemical Company Optimized liquid-phase oxidation
US7381836B2 (en) 2004-09-02 2008-06-03 Eastman Chemical Company Optimized liquid-phase oxidation
US7482482B2 (en) * 2004-09-02 2009-01-27 Eastman Chemical Company Optimized liquid-phase oxidation
US7399882B2 (en) * 2004-09-02 2008-07-15 Eastman Chemical Company Optimized liquid-phase oxidation
US7507857B2 (en) * 2004-09-02 2009-03-24 Eastman Chemical Company Optimized liquid-phase oxidation
US7361784B2 (en) * 2004-09-02 2008-04-22 Eastman Chemical Company Optimized liquid-phase oxidation
US7390921B2 (en) * 2004-09-02 2008-06-24 Eastman Chemical Company Optimized liquid-phase oxidation
US7568361B2 (en) * 2004-09-02 2009-08-04 Eastman Chemical Company Optimized liquid-phase oxidation
US7683210B2 (en) * 2004-09-02 2010-03-23 Eastman Chemical Company Optimized liquid-phase oxidation
US7589231B2 (en) * 2004-09-02 2009-09-15 Eastman Chemical Company Optimized liquid-phase oxidation
US7910769B2 (en) * 2004-09-02 2011-03-22 Eastman Chemical Company Optimized liquid-phase oxidation
US20060047153A1 (en) * 2004-09-02 2006-03-02 Wonders Alan G Optimized liquid-phase oxidation
US7572936B2 (en) * 2004-09-02 2009-08-11 Eastman Chemical Company Optimized liquid-phase oxidation
US7692036B2 (en) 2004-11-29 2010-04-06 Eastman Chemical Company Optimized liquid-phase oxidation
US7608733B2 (en) * 2004-09-02 2009-10-27 Eastman Chemical Company Optimized liquid-phase oxidation
US7608732B2 (en) * 2005-03-08 2009-10-27 Eastman Chemical Company Optimized liquid-phase oxidation
US7504535B2 (en) * 2004-09-02 2009-03-17 Eastman Chemical Company Optimized liquid-phase oxidation
US7495125B2 (en) * 2004-09-02 2009-02-24 Eastman Chemical Company Optimized liquid-phase oxidation
US7582793B2 (en) 2004-09-02 2009-09-01 Eastman Chemical Company Optimized liquid-phase oxidation
US7371894B2 (en) * 2004-09-02 2008-05-13 Eastman Chemical Company Optimized liquid-phase oxidation
US7563926B2 (en) * 2004-09-02 2009-07-21 Eastman Chemical Company Optimized liquid-phase oxidation
US7572932B2 (en) * 2004-09-02 2009-08-11 Eastman Chemical Company Optimized liquid-phase oxidation
US7692037B2 (en) 2004-09-02 2010-04-06 Eastman Chemical Company Optimized liquid-phase oxidation
US7884232B2 (en) * 2005-06-16 2011-02-08 Eastman Chemical Company Optimized liquid-phase oxidation
US7358389B2 (en) * 2006-01-04 2008-04-15 Eastman Chemical Company Oxidation system employing internal structure for enhanced hydrodynamics
US7355068B2 (en) * 2006-01-04 2008-04-08 Eastman Chemical Company Oxidation system with internal secondary reactor
US20070155987A1 (en) * 2006-01-04 2007-07-05 O'meadhra Ruairi S Oxidative digestion with optimized agitation
US7772424B2 (en) * 2006-03-01 2010-08-10 Eastman Chemical Company Polycarboxylic acid production system employing enhanced evaporative concentration downstream of oxidative digestion
US7501537B2 (en) * 2006-03-01 2009-03-10 Eastman Chemical Company Polycarboxylic acid production system employing oxidative digestion with reduced or eliminated upstream liquor exchange
US20070208194A1 (en) 2006-03-01 2007-09-06 Woodruff Thomas E Oxidation system with sidedraw secondary reactor
US7816556B2 (en) * 2006-03-01 2010-10-19 Eastman Chemical Company Polycarboxylic acid production system employing enhanced multistage oxidative digestion
US7714094B2 (en) * 2007-11-15 2010-05-11 Eastman Chemical Company Simplified isophthalic acid process for modifying PET
GB2489684A (en) * 2011-03-31 2012-10-10 Haifa Chemicals Ltd Crystallisation Apparatus
CN105218358B (zh) * 2015-09-29 2017-09-12 江西科苑生物药业有限公司 一种粗均苯三甲酸的精制方法
US20180050930A1 (en) * 2016-08-16 2018-02-22 Naveed Aslam Crystallizer for water reclamation

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4835307A (en) * 1984-12-13 1989-05-30 Amoco Corporation Method and apparatus for controlling the manufacture of terephthalic acid to control the level and variability of the contaminant content and the optical density
US6307099B1 (en) * 1997-02-27 2001-10-23 E. I. Du Pont De Nemours And Company Production of terephthalic acid
WO2004052821A1 (en) * 2002-12-09 2004-06-24 Eastman Chemical Company Process for the oxidative purification of terephthalic acid

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US2794832A (en) 1955-06-20 1957-06-04 Shell Dev Crystallization and separation of crystals
US2962361A (en) 1957-08-12 1960-11-29 Standard Oil Co Continuous oxidation system for producing carboxylic acids
US3629321A (en) * 1969-05-26 1971-12-21 Standard Oil Co Integration of para-xylene oxidation to terephthalic acid and its esterification to dimethyl terephthalate
US3873275A (en) 1969-09-29 1975-03-25 Whiting Corp Crystallization apparatus and method
JPS5518698B1 (https=) 1971-04-03 1980-05-21
FR2413352A1 (fr) 1977-12-28 1979-07-27 Mitsui Petrochemical Ind Procede de preparation de l'acide terephtalique
US4334086A (en) 1981-03-16 1982-06-08 Labofina S.A. Production of terephthalic acid
JPS5993029A (ja) 1982-11-16 1984-05-29 Mitsubishi Chem Ind Ltd 高純度テレフタル酸の製造法
JP2545103B2 (ja) 1987-12-17 1996-10-16 三井石油化学工業株式会社 テレフタル酸スラリ―の分散媒交換方法
DE69104280T2 (de) 1990-06-25 1995-02-16 Mitsubishi Gas Chemical Co Verfahren zur Herstellung von hochreiner Isophthalsäure.
GB9102393D0 (en) 1991-02-05 1991-03-20 Ici Plc Production of terephthalic acid
ES2079967T3 (es) 1992-03-27 1996-01-16 Allied Signal Inc Procedimiento para la cristalizacion en un cristalizador de deflector y tubo de aspiracion.
KR970000136B1 (ko) * 1993-09-28 1997-01-04 브이.피. 유리예프 고순도 벤젠디카르복실산 이성질체의 제조방법
US5712412A (en) 1994-12-26 1998-01-27 Mitsubishi Gas Chemical Co., Inc. Process for producing highly pure terephthalic acid
US6054610A (en) 1995-06-07 2000-04-25 Hfm International, Inc. Method and apparatus for preparing purified terephthalic acid and isophthalic acid from mixed xylenes
JPH1045667A (ja) 1996-07-29 1998-02-17 Mitsubishi Gas Chem Co Inc 分散媒置換装置を用いた高純度テレフタル酸の製造方法
BR0107739A (pt) 2000-01-21 2002-10-22 Bp Corp North America Inc Processos para a produção de ácido carboxìlico aromático, de recuperação de energia, e para a produção de ácido dicarboxìlico aromático, e, processo contìnuo para a produção de um ácido tricarboxìlico aromático
CA2398041A1 (en) 2000-01-25 2001-08-02 Inca International S.P.A. Process for the recovery of crude terephthalic acid (cta)
DE10026619A1 (de) 2000-05-29 2001-12-06 Basf Ag Vorrichtung zur Herstellung von Kristallen
JP2006509044A (ja) 2002-12-09 2006-03-16 イーストマン ケミカル カンパニー 粗製カルボン酸スラリーの精製方法
WO2004058377A1 (en) 2002-12-16 2004-07-15 E.I. Du Pont De Nemours And Company Apparatus and method for forming crystals/precipitate/particles
US20040215036A1 (en) 2003-04-25 2004-10-28 Robert Lin Method for heating a crude carboxylic acid slurry in a post oxidation zone by the addition of steam

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4835307A (en) * 1984-12-13 1989-05-30 Amoco Corporation Method and apparatus for controlling the manufacture of terephthalic acid to control the level and variability of the contaminant content and the optical density
US6307099B1 (en) * 1997-02-27 2001-10-23 E. I. Du Pont De Nemours And Company Production of terephthalic acid
WO2004052821A1 (en) * 2002-12-09 2004-06-24 Eastman Chemical Company Process for the oxidative purification of terephthalic acid

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
全文.

Also Published As

Publication number Publication date
US7615663B2 (en) 2009-11-10
WO2006028773A2 (en) 2006-03-16
MX2007002505A (es) 2007-05-04
EP1861350A2 (en) 2007-12-05
TW200621702A (en) 2006-07-01
CA2576323A1 (en) 2006-03-16
IN2014DN08961A (https=) 2015-07-10
WO2006028773A3 (en) 2006-07-13
US20060047166A1 (en) 2006-03-02
BRPI0514767A (pt) 2008-06-24
CN101031538A (zh) 2007-09-05

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C06 Publication
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C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
ASS Succession or assignment of patent right

Owner name: PEMEX GROUP LLC

Free format text: FORMER OWNER: EASTMAN CHEM CO.

Effective date: 20110907

C41 Transfer of patent application or patent right or utility model
TA01 Transfer of patent application right

Effective date of registration: 20110907

Address after: Nuevo Leon, Mexico

Applicant after: GRUPO PETROTEMEX, S.A. de C.V.

Address before: Tennessee

Applicant before: EASTMAN CHEMICAL Co.

EE01 Entry into force of recordation of patent licensing contract

Assignee: JIAXING PETROCHEMICAL Co.,Ltd.

Assignor: GRUPO PETROTEMEX, S.A. de C.V.

Contract record no.: 2012990000015

Denomination of invention: Optimized purification production of terephthalic acid

License type: Common License

Open date: 20070905

Record date: 20120113

C14 Grant of patent or utility model
GR01 Patent grant
CX01 Expiry of patent term
CX01 Expiry of patent term

Granted publication date: 20120328