CN1008104B - 聚倍半硅氧烷水乳浊液的制备方法 - Google Patents

聚倍半硅氧烷水乳浊液的制备方法

Info

Publication number
CN1008104B
CN1008104B CN86106218A CN86106218A CN1008104B CN 1008104 B CN1008104 B CN 1008104B CN 86106218 A CN86106218 A CN 86106218A CN 86106218 A CN86106218 A CN 86106218A CN 1008104 B CN1008104 B CN 1008104B
Authority
CN
China
Prior art keywords
aqueous emulsion
preparation
polysilsesquioxane
hlb value
water
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
CN86106218A
Other languages
English (en)
Chinese (zh)
Other versions
CN86106218A (zh
Inventor
大桥博司
近藤清宏
冈田文夫
田中正喜
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shin-Etsu Chemical Co Ltd
Original Assignee
Shin-Etsu Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shin-Etsu Chemical Co Ltd filed Critical Shin-Etsu Chemical Co Ltd
Publication of CN86106218A publication Critical patent/CN86106218A/zh
Publication of CN1008104B publication Critical patent/CN1008104B/zh
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K3/00—Materials not provided for elsewhere
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00—Processes of treating or compounding macromolecular substances
    • C08J3/02—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques
    • C08J3/03—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in aqueous media
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04—Polysiloxanes
    • C08G77/06—Preparatory processes
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D183/00—Coating compositions based on macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon, with or without sulfur, nitrogen, oxygen, or carbon only; Coating compositions based on derivatives of such polymers
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K23/00—Use of substances as emulsifying, wetting, dispersing, or foam-producing agents
    • C09K23/18—Quaternary ammonium compounds
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K23/00—Use of substances as emulsifying, wetting, dispersing, or foam-producing agents
    • C09K23/42—Ethers, e.g. polyglycol ethers of alcohols or phenols
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2383/00—Characterised by the use of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon with or without sulfur, nitrogen, oxygen, or carbon only; Derivatives of such polymers
    • C08J2383/04—Polysiloxanes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Health & Medical Sciences (AREA)
  • Dispersion Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Silicon Polymers (AREA)
  • Paints Or Removers (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Processes Of Treating Macromolecular Substances (AREA)
CN86106218A 1985-08-20 1986-08-19 聚倍半硅氧烷水乳浊液的制备方法 Expired CN1008104B (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP182738/85 1985-08-20
JP60182738A JPS6243424A (ja) 1985-08-20 1985-08-20 シルセスキオキサン乳濁液の製造方法

Publications (2)

Publication Number Publication Date
CN86106218A CN86106218A (zh) 1987-03-25
CN1008104B true CN1008104B (zh) 1990-05-23

Family

ID=16123572

Family Applications (1)

Application Number Title Priority Date Filing Date
CN86106218A Expired CN1008104B (zh) 1985-08-20 1986-08-19 聚倍半硅氧烷水乳浊液的制备方法

Country Status (4)

Country Link
US (1) US4778624A (enExample)
JP (1) JPS6243424A (enExample)
KR (1) KR900009041B1 (enExample)
CN (1) CN1008104B (enExample)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1331870C (zh) * 2004-10-27 2007-08-15 西北工业大学 一种制备带环氧基倍半硅氧烷的方法

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JPH0618879B2 (ja) * 1988-02-26 1994-03-16 東芝シリコーン株式会社 ポリオルガノシルセスキオキサン微粒子
JP2607118B2 (ja) * 1988-04-19 1997-05-07 日本化学工業株式会社 球状有機珪酸および球状シリカ粉末の製造法
JPH0655828B2 (ja) * 1988-12-15 1994-07-27 信越化学工業株式会社 表面変性ポリメチルシルセスキオキサン球状微粒子及びその製造方法
JP2753043B2 (ja) * 1989-05-29 1998-05-18 株式会社東芝 電気車制御装置
US5268126A (en) * 1989-08-04 1993-12-07 Huels Aktiengesellschaft Emulsifiers for the preparation of aqueous polysiloxane emulsions and aqueous polysiloxane-paraffin oil emulsions with long shelf lives
DE3925846A1 (de) * 1989-08-04 1991-02-14 Huels Chemische Werke Ag Emulgatoren zur herstellung von lagerstabilen, waessrigen polysiloxan- bzw. polysiloxan-paraffinoel-emulsionen
JP2783627B2 (ja) * 1989-12-25 1998-08-06 株式会社トクヤマ 被膜用組成物
CA2041599A1 (en) 1990-06-01 1991-12-02 Michael Gee Method for making polysiloxane emulsions
JPH0742180B2 (ja) * 1991-12-20 1995-05-10 東洋インキ製造株式会社 水性有機珪素系組成物
DE4309971A1 (de) * 1993-03-26 1994-09-29 Bayer Ag Imprägnierungsemulsion für mineralische Baustoffe
US5393330A (en) * 1993-06-30 1995-02-28 Osi Specialties, Inc. Cationic emulsions of alkylalkoxysilanes
DE4415062B4 (de) * 1994-04-29 2004-04-01 Stockhausen Gmbh & Co. Kg Mittel und Verfahren zur Hydrophobierung von Ledern und Pelzen
US6627682B1 (en) 1995-04-12 2003-09-30 Crompton Corporation Epoxy compositions
US6127462A (en) 1995-04-12 2000-10-03 Osi Specialities, Inc. Compositions of epoxysilane and reactive polymer with cure catalyst and methods of preparation
US6369139B1 (en) 1995-04-12 2002-04-09 Crompton Corporation Compositions of epoxysilane emulsion additives in waterbased reactive polymer dispersions and methods of preparation
US5686523A (en) * 1995-05-26 1997-11-11 Osi Specialties, Inc. Aqueous curable silane/polymer compositions
US5827922A (en) * 1995-05-26 1998-10-27 Osi Specialties, Inc. Aqueous silylated polymer curable compositions with tin catalysts
US6069200A (en) * 1995-05-26 2000-05-30 Ck Witco Corporation Aqueous silylated polymer curable compositions
US5661215A (en) * 1995-07-26 1997-08-26 Dow Corning Corporation Microemulsions of gel-free polymers
CA2239163C (en) * 1996-10-02 2006-09-05 Osi Specialties, Inc. Compositions of epoxysilane emulsion additives in waterbased reactive polymer dispersions and methods of preparation
US5801262A (en) * 1997-06-30 1998-09-01 General Electric Company Process for preparing polysiloxane microspheres with a narrow size distribution
US6319982B1 (en) 1998-09-08 2001-11-20 Ck Witco Corporation Waterborne silicone adhesives, sealants and coatings
US6037008A (en) * 1998-09-08 2000-03-14 Ck Witco Corporation Use of emulsified silane coupling agents as primers to improve adhesion of sealants, adhesives and coatings
US6013683A (en) * 1998-12-17 2000-01-11 Dow Corning Corporation Single phase silicone and water compositions
JP4610712B2 (ja) * 2000-10-05 2011-01-12 花王株式会社 水性エマルジョン
US7030066B1 (en) 2001-11-12 2006-04-18 Charles Piskoti Wetting composition for high temperature metal surfaces, and method of making the same
WO2005037907A1 (en) * 2003-10-07 2005-04-28 Honeywell International Inc. Coatings and hard mask compositions for integrated circuit applications, methods of production and uses thereof
US7875673B2 (en) * 2004-07-07 2011-01-25 Dow Corning Corporation Emulsions of organopolysiloxane resins produced by emulsion polymerization
US8901268B2 (en) 2004-08-03 2014-12-02 Ahila Krishnamoorthy Compositions, layers and films for optoelectronic devices, methods of production and uses thereof
JP4775543B2 (ja) 2005-01-24 2011-09-21 信越化学工業株式会社 オルガノシリコーンレジンエマルジョン組成物及びその製造方法、ならびに該組成物の被膜が形成された物品
US20080221263A1 (en) * 2006-08-31 2008-09-11 Subbareddy Kanagasabapathy Coating compositions for producing transparent super-hydrophobic surfaces
JP4239030B2 (ja) * 2006-07-13 2009-03-18 信越化学工業株式会社 光硬化性樹脂組成物及びその硬化皮膜を有する物品
KR100756676B1 (ko) * 2006-11-23 2007-09-07 제일모직주식회사 실리콘계 미립자, 그 제조 방법, 및 그 미립자가 함유된열가소성 수지 조성물
CN101668822B (zh) * 2007-04-26 2013-02-06 陶氏康宁公司 赋予防水性的含水硅氧烷乳液
DE102007047907A1 (de) 2007-11-30 2009-06-04 Wacker Chemie Ag Wässrige Dispersionen von Organosiliciumverbindungen
WO2010062674A1 (en) * 2008-11-03 2010-06-03 Dow Corning Corporation Film forming silicone emulsions
US8557877B2 (en) 2009-06-10 2013-10-15 Honeywell International Inc. Anti-reflective coatings for optically transparent substrates
CN103003333A (zh) 2010-07-22 2013-03-27 道康宁公司 用于制备聚硅氧烷乳液的方法
US8864898B2 (en) 2011-05-31 2014-10-21 Honeywell International Inc. Coating formulations for optical elements
WO2013019752A1 (en) * 2011-07-29 2013-02-07 Sun Color Corporation Dispersions and related coatings and cured articles
JP5607001B2 (ja) * 2011-08-11 2014-10-15 信越化学工業株式会社 シリコーン微粒子及びその製造方法
CN102926212B (zh) * 2012-10-31 2014-09-03 辽宁恒星精细化工有限公司 一种用于棉、麻面料的水性高弹涂层胶及制备方法
WO2016167892A1 (en) 2015-04-13 2016-10-20 Honeywell International Inc. Polysiloxane formulations and coatings for optoelectronic applications
CN106916529B (zh) * 2017-03-07 2018-12-21 陕西科技大学 一种耐久性聚倍半硅氧烷纳米杂化超疏水皮革涂层及其制备方法
WO2020185511A1 (en) * 2019-03-12 2020-09-17 Rohm And Haas Company Aqueous dispersion of (meth)acrylic polymer and polysilsesquioxane nano particles

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DE2701724C2 (de) * 1977-01-18 1984-09-20 Bayer Ag, 5090 Leverkusen Stabile Alkylwasserstoffpolysiloxan- Emulsionen
DE3173441D1 (en) * 1980-08-26 1986-02-20 Japan Synthetic Rubber Co Ltd Ladder-like lower alkylpolysilsesquioxanes and process for their preparation
JPS57111354A (en) * 1980-12-29 1982-07-10 Toray Silicone Co Ltd Organopolysiloxane composition
EP0076656B1 (en) * 1981-10-03 1988-06-01 Japan Synthetic Rubber Co., Ltd. Solvent-soluble organopolysilsesquioxanes, processes for producing the same, and compositions and semiconductor devices using the same
DE3216585C2 (de) * 1982-05-04 1984-07-26 Th. Goldschmidt Ag, 4300 Essen Verfahren zur Herstellung von feinteiligen, stabilen O/W-Emulsionen von Organopolysiloxanen
JPS6013813A (ja) * 1983-07-05 1985-01-24 Toshiba Silicone Co Ltd ポリメチルシルセスキオキサンの製造方法
US4670299A (en) * 1984-11-01 1987-06-02 Fujitsu Limited Preparation of lower alkyl polysilsesquioxane and formation of insulating layer of silylated polymer on electronic circuit board
US4648904A (en) * 1986-02-14 1987-03-10 Scm Corporation Aqueous systems containing silanes for rendering masonry surfaces water repellant

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1331870C (zh) * 2004-10-27 2007-08-15 西北工业大学 一种制备带环氧基倍半硅氧烷的方法

Also Published As

Publication number Publication date
JPH0114250B2 (enExample) 1989-03-10
US4778624A (en) 1988-10-18
JPS6243424A (ja) 1987-02-25
KR870002225A (ko) 1987-03-30
KR900009041B1 (ko) 1990-12-17
CN86106218A (zh) 1987-03-25

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