CN100537031C - 有机化合物的制备方法 - Google Patents

有机化合物的制备方法 Download PDF

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Publication number
CN100537031C
CN100537031C CNB028262352A CN02826235A CN100537031C CN 100537031 C CN100537031 C CN 100537031C CN B028262352 A CNB028262352 A CN B028262352A CN 02826235 A CN02826235 A CN 02826235A CN 100537031 C CN100537031 C CN 100537031C
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compound
group
compounds
reaction
groups
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CN1607980A (zh
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石井康敬
平井成尚
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Daicel Corp
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Daicel Chemical Industries Ltd
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
    • B01J31/0234—Nitrogen-, phosphorus-, arsenic- or antimony-containing compounds
    • B01J31/0235—Nitrogen containing compounds
    • B01J31/0245—Nitrogen containing compounds being derivatives of carboxylic or carbonic acids
    • B01J31/0249—Ureas (R2N-C(=O)-NR2)
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/26—Catalysts comprising hydrides, coordination complexes or organic compounds containing in addition, inorganic metal compounds not provided for in groups B01J31/02 - B01J31/24
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06—Preparation of nitro compounds
    • C07C201/08—Preparation of nitro compounds by substitution of hydrogen atoms by nitro groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06—Preparation of nitro compounds
    • C07C201/12—Preparation of nitro compounds by reactions not involving the formation of nitro groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles
    • C07C253/30—Preparation of carboxylic acid nitriles by reactions not involving the formation of cyano groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/48—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by oxidation reactions with formation of hydroxy groups
    • C07C29/50—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by oxidation reactions with formation of hydroxy groups with molecular oxygen only
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/32—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen
    • C07C45/33—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties
    • C07C45/34—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties in unsaturated compounds
    • C07C45/36—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties in unsaturated compounds in compounds containing six-membered aromatic rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
    • C07C49/385—Saturated compounds containing a keto group being part of a ring
    • C07C49/417—Saturated compounds containing a keto group being part of a ring polycyclic
    • C07C49/423—Saturated compounds containing a keto group being part of a ring polycyclic a keto group being part of a condensed ring system
    • C07C49/453—Saturated compounds containing a keto group being part of a ring polycyclic a keto group being part of a condensed ring system having three rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
    • C07C49/587—Unsaturated compounds containing a keto groups being part of a ring
    • C07C49/657—Unsaturated compounds containing a keto groups being part of a ring containing six-membered aromatic rings
    • C07C49/665—Unsaturated compounds containing a keto groups being part of a ring containing six-membered aromatic rings a keto group being part of a condensed ring system
    • C07C49/675—Unsaturated compounds containing a keto groups being part of a ring containing six-membered aromatic rings a keto group being part of a condensed ring system having three rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/255—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting
    • C07C51/265—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting having alkyl side chains which are oxidised to carboxyl groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/31—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation of cyclic compounds with ring-splitting
    • C07C51/313—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation of cyclic compounds with ring-splitting with molecular oxygen
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/28—Preparation of carboxylic acid esters by modifying the hydroxylic moiety of the ester, such modification not being an introduction of an ester group
    • C07C67/29—Preparation of carboxylic acid esters by modifying the hydroxylic moiety of the ester, such modification not being an introduction of an ester group by introduction of oxygen-containing functional groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D251/00—Heterocyclic compounds containing 1,3,5-triazine rings
    • C07D251/02—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
    • C07D251/12—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
    • C07D251/26—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
    • C07D251/30—Only oxygen atoms
    • C07D251/34—Cyanuric or isocyanuric esters
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2231/00—Catalytic reactions performed with catalysts classified in B01J31/00
    • B01J2231/30—Addition reactions at carbon centres, i.e. to either C-C or C-X multiple bonds
    • B01J2231/32—Addition reactions to C=C or C-C triple bonds
    • B01J2231/323—Hydrometalation, e.g. bor-, alumin-, silyl-, zirconation or analoguous reactions like carbometalation, hydrocarbation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2231/00—Catalytic reactions performed with catalysts classified in B01J31/00
    • B01J2231/40—Substitution reactions at carbon centres, e.g. C-C or C-X, i.e. carbon-hetero atom, cross-coupling, C-H activation or ring-opening reactions
    • B01J2231/42—Catalytic cross-coupling, i.e. connection of previously not connected C-atoms or C- and X-atoms without rearrangement
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14—The ring being saturated
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2603/00—Systems containing at least three condensed rings
    • C07C2603/56—Ring systems containing bridged rings
    • C07C2603/58—Ring systems containing bridged rings containing three rings
    • C07C2603/70—Ring systems containing bridged rings containing three rings containing only six-membered rings
    • C07C2603/74—Adamantanes
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/55—Design of synthesis routes, e.g. reducing the use of auxiliary or protecting groups

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
CNB028262352A 2001-12-25 2002-12-05 有机化合物的制备方法 Expired - Fee Related CN100537031C (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2001392863 2001-12-25
JP392863/2001 2001-12-25

Publications (2)

Publication Number Publication Date
CN1607980A CN1607980A (zh) 2005-04-20
CN100537031C true CN100537031C (zh) 2009-09-09

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US (2) US7091342B2 (enExample)
EP (1) EP1459804B1 (enExample)
JP (2) JP4413009B2 (enExample)
CN (1) CN100537031C (enExample)
AU (1) AU2002361079A1 (enExample)
DE (1) DE60236619D1 (enExample)
MY (1) MY134799A (enExample)
SA (1) SA02230481B1 (enExample)
TW (1) TW200301158A (enExample)
WO (1) WO2003055600A1 (enExample)

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US6769128B1 (en) 1995-06-07 2004-07-27 United Video Properties, Inc. Electronic television program guide schedule system and method with data feed access
BRPI9812104B1 (pt) 1997-07-21 2016-12-27 Guide E Inc método para navegar por um guia de programa interativo
US6898762B2 (en) 1998-08-21 2005-05-24 United Video Properties, Inc. Client-server electronic program guide
CA2870324C (en) 2000-03-31 2017-08-15 United Video Properties, Inc. Systems and methods for improved audience measuring
JPWO2005023784A1 (ja) * 2003-09-02 2006-11-02 ダイセル化学工業株式会社 Ｎ，ｎ′，ｎ″−トリ置換イソシアヌル酸の製造方法
JP2005298380A (ja) * 2004-04-08 2005-10-27 Daicel Chem Ind Ltd 芳香族カルボン酸の製造法
JP4885468B2 (ja) * 2005-03-28 2012-02-29 株式会社ダイセル 有機化合物の製造方法
US7994330B2 (en) * 2005-03-28 2011-08-09 Daicel Chemical Industries, Ltd. Method for producing organic compound and method for decomposing compound having dicarboximide skeleton
JP2006273793A (ja) * 2005-03-30 2006-10-12 Daicel Chem Ind Ltd 環状アシルウレア系触媒を用いた有機化合物の製造方法
US8613024B2 (en) * 2005-12-13 2013-12-17 United Video Properties, Inc. Cross-platform predictive popularity ratings for use in interactive television applications
US7326815B2 (en) * 2005-12-27 2008-02-05 Exxonmobil Chemical Patents Inc. Selective oxidation of alkylbenzenes
US7834217B2 (en) * 2006-12-05 2010-11-16 Daicel Chemical Industries, Ltd. Method for producing oxidation product of cycloalkane
US7801888B2 (en) 2007-03-09 2010-09-21 Microsoft Corporation Media content search results ranked by popularity
JP5091774B2 (ja) * 2008-06-11 2012-12-05 株式会社ダイセル 酸化触媒系
US9014546B2 (en) 2009-09-23 2015-04-21 Rovi Guides, Inc. Systems and methods for automatically detecting users within detection regions of media devices
CN106008193B (zh) * 2016-06-01 2019-12-17 中国矿业大学 一种常压下使用氧气为氧化剂催化氧化褐煤的方法
US10091549B1 (en) 2017-03-30 2018-10-02 Rovi Guides, Inc. Methods and systems for recommending media assets based on the geographic location at which the media assets are frequently consumed
CN107556201B (zh) * 2017-09-08 2020-10-27 山西智创药研科技有限公司 一种制备间氨基苯酚的工艺方法
CN108525670B (zh) * 2018-05-04 2021-03-16 太原理工大学 氧化硅限域镍基催化剂及其制备方法与应用
CN112125795B (zh) * 2019-06-24 2023-08-29 中国石油化工股份有限公司 环己烷氧化制己二酸的方法
WO2021160470A1 (en) 2020-02-13 2021-08-19 Basf Se Preparation of aromatic carbonyl compounds by catalytic oxidation with molecular oxygen
CN112588083B (zh) * 2020-11-20 2022-04-22 绍兴文理学院 一种高效捕集二氧化碳的方法
CN114814065B (zh) * 2022-04-12 2023-12-01 上海交通大学 幽门螺旋杆菌的唾液中voc标志物及其在制备诊断试剂中的应用
CN115057800B (zh) * 2022-07-28 2022-11-01 山东星之联生物科技股份有限公司 对苯乙烯磺酸盐的清洁合成方法

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EP0429701A1 (en) * 1988-06-02 1991-06-05 Showa Highpolymer Co., Ltd. Curable resin composition
WO1993003825A1 (en) * 1991-08-13 1993-03-04 The Dow Chemical Company A composition and method for simultaneous absorption of sulfur dioxide and nitric oxide
JPH06199857A (ja) * 1993-01-07 1994-07-19 Taisho Pharmaceut Co Ltd ５−デアザフラボ−６，９−キノン誘導体及びその製造方法
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EP0429701A1 (en) * 1988-06-02 1991-06-05 Showa Highpolymer Co., Ltd. Curable resin composition
WO1993003825A1 (en) * 1991-08-13 1993-03-04 The Dow Chemical Company A composition and method for simultaneous absorption of sulfur dioxide and nitric oxide
JPH06199857A (ja) * 1993-01-07 1994-07-19 Taisho Pharmaceut Co Ltd ５−デアザフラボ−６，９−キノン誘導体及びその製造方法
JP2000086218A (ja) * 1998-09-05 2000-03-28 Agency Of Ind Science & Technol 超微細カーボンチューブの合成方法及びそれに用いる触媒

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EP1459804A4 (en) 2005-04-06
EP1459804A1 (en) 2004-09-22
TWI300012B (enExample) 2008-08-21
EP1459804B1 (en) 2010-06-02
US7288649B2 (en) 2007-10-30
WO2003055600A1 (en) 2003-07-10
AU2002361079A1 (en) 2003-07-15
JP2009079066A (ja) 2009-04-16
JPWO2003055600A1 (ja) 2005-04-28
US20050020439A1 (en) 2005-01-27
US20060030716A1 (en) 2006-02-09
US7091342B2 (en) 2006-08-15
DE60236619D1 (de) 2010-07-15
SA02230481B1 (ar) 2009-02-07
JP4413009B2 (ja) 2010-02-10
CN1607980A (zh) 2005-04-20
MY134799A (en) 2007-12-31
JP4920024B2 (ja) 2012-04-18
TW200301158A (en) 2003-07-01

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