CN100384572C - 一种无机物载纳米银溶胶的制备方法 - Google Patents
一种无机物载纳米银溶胶的制备方法 Download PDFInfo
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- CN100384572C CN100384572C CNB2005100623198A CN200510062319A CN100384572C CN 100384572 C CN100384572 C CN 100384572C CN B2005100623198 A CNB2005100623198 A CN B2005100623198A CN 200510062319 A CN200510062319 A CN 200510062319A CN 100384572 C CN100384572 C CN 100384572C
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- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 title claims abstract description 36
- 239000004332 silver Substances 0.000 title claims abstract description 30
- 229910052709 silver Inorganic materials 0.000 title claims abstract description 30
- 238000002360 preparation method Methods 0.000 title claims abstract description 25
- 239000006185 dispersion Substances 0.000 claims abstract description 29
- SQGYOTSLMSWVJD-UHFFFAOYSA-N silver(1+) nitrate Chemical compound [Ag+].[O-]N(=O)=O SQGYOTSLMSWVJD-UHFFFAOYSA-N 0.000 claims abstract description 22
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 22
- 239000000843 powder Substances 0.000 claims abstract description 14
- 229910001961 silver nitrate Inorganic materials 0.000 claims abstract description 11
- 239000008367 deionised water Substances 0.000 claims abstract description 10
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 10
- 239000003638 chemical reducing agent Substances 0.000 claims abstract description 8
- 239000002270 dispersing agent Substances 0.000 claims abstract description 7
- 239000003223 protective agent Substances 0.000 claims abstract description 5
- 239000007864 aqueous solution Substances 0.000 claims description 18
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 17
- VTYYLEPIZMXCLO-UHFFFAOYSA-L calcium carbonate Substances [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims description 16
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims description 10
- 229910000019 calcium carbonate Inorganic materials 0.000 claims description 10
- 238000003756 stirring Methods 0.000 claims description 10
- 238000005303 weighing Methods 0.000 claims description 8
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 5
- 229960005070 ascorbic acid Drugs 0.000 claims description 5
- 235000010323 ascorbic acid Nutrition 0.000 claims description 5
- 239000011668 ascorbic acid Substances 0.000 claims description 5
- 230000008014 freezing Effects 0.000 claims description 5
- 238000007710 freezing Methods 0.000 claims description 5
- 230000010355 oscillation Effects 0.000 claims description 5
- 239000011591 potassium Substances 0.000 claims description 5
- 229910052700 potassium Inorganic materials 0.000 claims description 5
- 239000012279 sodium borohydride Substances 0.000 claims description 5
- 229910000033 sodium borohydride Inorganic materials 0.000 claims description 5
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 claims description 5
- 238000000108 ultra-filtration Methods 0.000 claims description 5
- 229910052500 inorganic mineral Inorganic materials 0.000 claims description 4
- 239000011707 mineral Substances 0.000 claims description 4
- 239000005543 nano-size silicon particle Substances 0.000 claims description 4
- RCEAADKTGXTDOA-UHFFFAOYSA-N OS(O)(=O)=O.CCCCCCCCCCCC[Na] Chemical compound OS(O)(=O)=O.CCCCCCCCCCCC[Na] RCEAADKTGXTDOA-UHFFFAOYSA-N 0.000 claims description 3
- 239000004372 Polyvinyl alcohol Substances 0.000 claims description 3
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 claims description 3
- -1 polyethylene pyrrolidone Polymers 0.000 claims description 3
- 229920002451 polyvinyl alcohol Polymers 0.000 claims description 3
- GCLGEJMYGQKIIW-UHFFFAOYSA-H sodium hexametaphosphate Chemical compound [Na]OP1(=O)OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])O1 GCLGEJMYGQKIIW-UHFFFAOYSA-H 0.000 claims description 3
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims description 2
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 claims description 2
- CEYULKASIQJZGP-UHFFFAOYSA-L disodium;2-(carboxymethyl)-2-hydroxybutanedioate Chemical compound [Na+].[Na+].[O-]C(=O)CC(O)(C(=O)O)CC([O-])=O CEYULKASIQJZGP-UHFFFAOYSA-L 0.000 claims description 2
- 239000008103 glucose Substances 0.000 claims description 2
- 239000000203 mixture Substances 0.000 claims description 2
- 239000000126 substance Substances 0.000 claims description 2
- 239000001648 tannin Substances 0.000 claims description 2
- 235000018553 tannin Nutrition 0.000 claims description 2
- 229920001864 tannin Polymers 0.000 claims description 2
- 239000002245 particle Substances 0.000 abstract description 6
- 238000000034 method Methods 0.000 abstract description 2
- 230000006641 stabilisation Effects 0.000 abstract description 2
- 238000011105 stabilization Methods 0.000 abstract description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 12
- 239000004408 titanium dioxide Substances 0.000 description 6
- 239000000377 silicon dioxide Substances 0.000 description 4
- 229960001866 silicon dioxide Drugs 0.000 description 2
- 235000012239 silicon dioxide Nutrition 0.000 description 2
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- SOQBVABWOPYFQZ-UHFFFAOYSA-N oxygen(2-);titanium(4+) Chemical compound [O-2].[O-2].[Ti+4] SOQBVABWOPYFQZ-UHFFFAOYSA-N 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
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- Manufacture Of Metal Powder And Suspensions Thereof (AREA)
Abstract
Description
Claims (5)
Priority Applications (1)
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CNB2005100623198A CN100384572C (zh) | 2005-12-29 | 2005-12-29 | 一种无机物载纳米银溶胶的制备方法 |
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CNB2005100623198A CN100384572C (zh) | 2005-12-29 | 2005-12-29 | 一种无机物载纳米银溶胶的制备方法 |
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CN1803351A CN1803351A (zh) | 2006-07-19 |
CN100384572C true CN100384572C (zh) | 2008-04-30 |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102120265B (zh) * | 2010-01-07 | 2013-04-10 | 中国科学院化学研究所 | 单分散的银纳米粒子的胶体、纳米银粉的制备方法及其导电油墨 |
CN103170642A (zh) * | 2013-03-22 | 2013-06-26 | 北京航空航天大学 | 非正二十面体金纳米材料的制备方法 |
Families Citing this family (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US7968008B2 (en) | 2006-08-03 | 2011-06-28 | Fry's Metals, Inc. | Particles and inks and films using them |
US9615463B2 (en) | 2006-09-22 | 2017-04-04 | Oscar Khaselev | Method for producing a high-aspect ratio conductive pattern on a substrate |
CN100528427C (zh) * | 2007-09-14 | 2009-08-19 | 北京首创纳米科技有限公司 | 一种纳米银复合溶胶的制备方法 |
CN102897883B (zh) * | 2012-10-10 | 2014-03-19 | 盐城工学院 | 一种腐殖酸降解材料Ag-TiO2的制备方法 |
CN103055800A (zh) * | 2013-02-05 | 2013-04-24 | 华北电力大学(保定) | 一种高效吸附气态元素汞的纳米修饰材料及制备方法 |
CN103461381B (zh) * | 2013-07-05 | 2015-08-05 | 北京中科东亚纳米材料科技有限公司 | 除甲醛、除异味复合消毒剂的制备方法 |
CN103737014B (zh) * | 2013-12-23 | 2015-12-30 | 暨南大学 | 一种纳米硫银复合溶胶及其制备方法与应用 |
CN104259481A (zh) * | 2014-10-14 | 2015-01-07 | 钱景 | 一种纳米银的制备方法 |
CN105970618A (zh) * | 2016-07-01 | 2016-09-28 | 潘明华 | 一种抗静电耐磨水溶胶整理剂及其制备方法 |
CN109021360B (zh) * | 2018-08-01 | 2021-03-05 | 福州市长乐区三互信息科技有限公司 | 一种抗菌汽车坐垫及其制备方法 |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1583332A (zh) * | 2004-06-08 | 2005-02-23 | 陈丽琼 | 一种纳米银溶胶及其制备方法 |
JP2005054223A (ja) * | 2003-08-01 | 2005-03-03 | Mitsui Mining & Smelting Co Ltd | ロッド状銀粒子の製造方法 |
CN1623897A (zh) * | 2004-11-19 | 2005-06-08 | 中国乐凯胶片集团公司 | 载纳米银的二氧化硅制备方法 |
CN1686646A (zh) * | 2005-04-26 | 2005-10-26 | 四川大学 | 一种粒径可控的单分散纳米银粉的制备方法 |
-
2005
- 2005-12-29 CN CNB2005100623198A patent/CN100384572C/zh not_active Expired - Fee Related
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2005054223A (ja) * | 2003-08-01 | 2005-03-03 | Mitsui Mining & Smelting Co Ltd | ロッド状銀粒子の製造方法 |
CN1583332A (zh) * | 2004-06-08 | 2005-02-23 | 陈丽琼 | 一种纳米银溶胶及其制备方法 |
CN1623897A (zh) * | 2004-11-19 | 2005-06-08 | 中国乐凯胶片集团公司 | 载纳米银的二氧化硅制备方法 |
CN1686646A (zh) * | 2005-04-26 | 2005-10-26 | 四川大学 | 一种粒径可控的单分散纳米银粉的制备方法 |
Non-Patent Citations (2)
Title |
---|
含纳米棒银溶胶的制备及其光谱性质研究. 刘霞,何天敬,刘凡镇,陈东明.化学物理学报,第18卷第1期. 2005 |
含纳米棒银溶胶的制备及其光谱性质研究. 刘霞,何天敬,刘凡镇,陈东明.化学物理学报,第18卷第1期. 2005 * |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102120265B (zh) * | 2010-01-07 | 2013-04-10 | 中国科学院化学研究所 | 单分散的银纳米粒子的胶体、纳米银粉的制备方法及其导电油墨 |
CN103170642A (zh) * | 2013-03-22 | 2013-06-26 | 北京航空航天大学 | 非正二十面体金纳米材料的制备方法 |
CN103170642B (zh) * | 2013-03-22 | 2016-03-23 | 北京航空航天大学 | 非正二十面体金纳米材料的制备方法 |
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Owner name: SHANGHAI HUASHI NANO MATERIALS CO., LTD. Free format text: FORMER OWNER: HUANG DEHUAN Effective date: 20080801 |
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Effective date of registration: 20080801 Address after: A building, Xin Mei Industrial Zone, No. 260 Lian Cao Road, Shanghai, Minhang District Patentee after: Shanghai Huashi Nano Material Co., Ltd. Address before: Room 13, No. 288, Lane 301, Macao Road, Shanghai, Putuo District Patentee before: Huang Dehuan |
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