CN100381130C - Bee pollen nutrition oral liquid and preparation method thereof - Google Patents
Bee pollen nutrition oral liquid and preparation method thereof Download PDFInfo
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- CN100381130C CN100381130C CNB2006100838692A CN200610083869A CN100381130C CN 100381130 C CN100381130 C CN 100381130C CN B2006100838692 A CNB2006100838692 A CN B2006100838692A CN 200610083869 A CN200610083869 A CN 200610083869A CN 100381130 C CN100381130 C CN 100381130C
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Abstract
The present invention provides a nutritive oral bee pollen liquid with the advantages of security, high nutritive value and convenient eating and a preparation method thereof. The preparation method comprises: firstly extracting fat from bee pollen by supercutical liquid, processing bee pollen meal through exsolution after extraction, and then compressing solvents for reutilization to obtain the bee pollen meal; extracting the bee pollen meal by water, and then processing the extracted bee pollen meal through centrifugation or filtration to obtain raw bee pollen liquid; processing the raw bee pollen liquid through clarification and membrane separation to obtain penetrant bee pollen liquid; compounding the penetrant bee pollen liquid with supplementary materials comprising the water, high fructose syrup, honey, sucrose, citric acid and essence; then processing the mixture through vacuum degasification, instantaneous ultrahigh temperature sterilization and sterile can pack to obtain the nutritive oral bee pollen liquid. In the present invention, the operation of supercutical liquid extraction is used for extracting the fat from the bee pollen firstly, which is favourable to the operation of clarification in later stages, and the appearance of the nutritive oral bee pollen liquid is clear and bright, and meanwhile, an advanced membrane separation technology (microfiltration and ultrafiltration) is used to remove substances bringing on turbidity easily so as to avoid the non-biological turbidity of the nutritive oral bee pollen liquid.
Description
Technical field
The present invention relates to a kind of bee pollen nutrition oral liquid and preparation method thereof, belong to the nutrition oral administration technical field.
Background technology
Bee pollen is exactly that Apis utilizes self special tectonic from phanerogam---the pollen grain of gathering in the flower pesticide of the sources of nectar and pollen, sneak into nectar and saliva through Apis to it, and be processed into irregular oblateness, carry back the dough of nest by the pollen basket on the Apis hind leg.Bee pollen contains the multiple nutrients material, comprise 22 seed amino acids, 14 kinds of vitamin and 30 various trace elements and a large amount of active protease, nucleic acid, hormone, flavone compound and other active substances, wherein protein 20～25%, total amino acid content is more than 20%, free amino acid 1～2%, carbohydrate 40～50%, fat 5～10%, the content of pollen rich in proteins surpasses milk, egg 5～7 times, ascorbic content is higher than fresh fruit and vegetable, is called as the king of natural complex.Particularly the content of vitamin B group is very abundant, than the high Radix Achyranthis Bidentatae of Mel.Contain thiamine 600 μ g in every 100g pollen, riboflavin 1670 μ g, pyridoxol 900 μ g, pantothenic acid 2700 μ g, nicotinic acid 10000 μ g.It contains several mineral materials: potassium, magnesium, calcium, ferrum, silicon, phosphorus, iodine, copper, strontium, zinc, manganese, cobalt, molybdenum, chromium, nickel, stannum, boron, vanadium, aluminum, barium, gallium, titanium, zirconium, beryllium, lead, arsenic, uranium.Bee pollen is described as " optimal natural nutrition source ", " miniature nutrition library ", human really natural nutrient food in a rarity.
At present, the existing Chinese patent of having declared of pollen beverage and production technology.(1) maize pollen drink and production method, CN 1104066A, its production method is for to put into the water lixiviate with Pollen Maydis, and becomes Pollen Maydis stock solution, add antiseptic, freezing and filtering and make maize pollen drink in stock solution, this method adopts flooding, freezing method to carry out breaking cellular wall; (2) pollen beverage and preparation method thereof, CN 1095561A, its production method is for to pulverize pollen on colloid mill, add in the acid solution and the pollen beverage of making, and this method adopts mechanical breaking-wall method.(3) pollen beverage and production technology thereof, CN 1165637A.Flos Camelliae Japonicae powder through inoculation, breaking cellular wall fermentation, enzymolysis, fine straining remove the gred the Flos Camelliae Japonicae powder extracting solution, extracting solution stirs through allotment Mel, vitamin, even matter, vacuum outgas, sterilization, fill, re-pasteurization, vanning and make pollen beverage.(4) processing method of pollen fruit squash and product, CN 1089809A.Its key is in the allotment, to add a certain amount of bee pollen before the sterilization of fruit squash homogenizing, and artificial tea powder or the pollen extract of gathering stirs, and carries out homogenizing, sterilization, fill, cooling again, promptly obtains this product.(5) contain the health beverage of pollen, fruit juice, CN97112270.9.The aqueous extract, fruit juice 10～30% weight, sugar 0～12% weight, Mel 0～3.0% weight and the water that contain natural pollen 0.005～0.02% weight and natural flower 0.5～2% weight in this health beverage.The natural dry flower powder of 1 part of weight or natural dried flower with the hot-water soak of 30～100 times of weight at least once, temperature is 50～80 ℃, the time is 30～60 minutes, the elimination residue and aqueous extract.(6) preparation method of nutritive corn pollen liquid, CN01116463.8 (authorizing).Its production method be with Pollen Maydis fermentation tank Nei Jialushi yeast and fermentation of Aspergillus niger through heat, stir, leach, process such as filtration can be made into nutritive corn pollen liquid.This method makes Pollen Maydis broken shell desensitization with microbe fermentation method, and extraction ratio can reach 94%.More than except that the 6th patent is authorized, remaining is unauthorized still up to now.Basically there is not above production marketing on the market at present.Bee pollen content is low in the above patented beverage, and brown stain and back muddiness take place easily, influences outward appearance.The present invention is applied to advanced person's membrane separation technique (microfiltration and ultrafiltration) in this nutrition oral administration, has solved muddy and brown stain problem behind the inanimate.
Summary of the invention
One of purpose of the present invention provides a kind of bee pollen nutrition oral liquid.
With the bee pollen is base stock, and it consists of bee pollen 4～20%, high fructose syrup, Mel or sucrose 4～10%, and vitamin C 0.02-0.1%, citric acid concentration 1～1.5 ‰, the essence consumption is 0.75～1.5g/L, all the other are water.
Above-mentioned bee pollen is selected from Pollen Brassicae campestris, Pollen Maydis, Pollen Helianthi, Pollen Pini, Pollen Astragali Melilotoidis (Pollen Astragali Sinici), pollen of Semen Fagopyri Esculenti, Semen Sesami pollen, Sorghum vulgare Pers. pollen, Flos Camelliae Japonicae powder, Flos Nelumbinis pollen etc.
Two of purpose of the present invention provides a kind of production technology of bee pollen nutrition oral liquid.
Two of purpose of the present invention can reach by the following technical programs:
(1) earlier bee pollen is joined in the extractor, in extractor, feed propane, butane or mixture (liquefied petroleum gas) then, continuous extraction is 1～10 hour under 10～60 ℃ of extraction temperature, extracting pressure 0.1～1Mpa condition, in extraction process, suitably stirs.
(2) carry out bee pollen dregs of rice precipitation and miscella precipitation after having extracted, the solvent compression is recycled, and obtains the bee pollen dregs of rice and bee pollen grease, and extraction times is 1～4 time.Bee pollen dregs of rice precipitation is a kind of endothermic process, therefore when precipitation, can replenish certain heat in the pollen dregs of rice, and the control heating-up temperature, stirs at a slow speed in the precipitation process below 60 ℃, helps solvent evaporates and heat transmission.Miscella precipitation condition: vacuum is 0.05～0.1Mpa, and temperature is 35～60 ℃, keeps both can obtain bee pollen grease in 0.5～2 hour.Bee pollen wherein: solvent=1: 1～4 (W/W).Wherein the charge of bee pollen accounts in the extractor volumetrical 3/4.
Moisture 2～10% in the above-mentioned bee pollen, the granularity of bee pollen is 5～100 orders.Wherein bee pollen is selected from Pollen Brassicae campestris, Pollen Maydis, Pollen Helianthi, Pollen Pini, Pollen Astragali Melilotoidis (Pollen Astragali Sinici), pollen of Semen Fagopyri Esculenti, Semen Sesami pollen, Sorghum vulgare Pers. pollen, Flos Camelliae Japonicae powder or Flos Nelumbinis pollen.
(3) bee pollen dregs of rice water is carried afterwards centrifugal or filtered and obtain bee pollen stock solution, wherein extract 10～50 ℃ of temperature, extraction time is 0.5～6 hour, water is carried and is added citric acid or vitamin C in the process, concentration is 0.5～1 ‰, bee pollen: (W: W), the bee pollen water-insoluble is developed other products and is used in water=1: 4～15.
(4) clarification: clarifier is gelatin, chitosan, Bentonite, PVPP or above clarifier is united use, concentration is 0.5～4 ‰, and temperature is 0～50 ℃, stirs in clarifying process, mixing speed is 20～200 rev/mins, and settling time is 0.5～24 hour.Clarification finishes afterwards centrifugal or filters and obtains clear liquor, and relative centrifugal force(RCF) is 1500～5000g when wherein centrifugal.
(5) bee pollen is clarified the clear liquor that obtains after finish centrifugal or the filtration and carried out separation and purification through membrance separation.At first with the micro-filtration membrane module of clear liquor by 0.1 μ m, and then by molecular weight is the hyperfiltration membrane assembly of 1000～20000Da, obtains permeate.Film device: membrane module adopts ceramic membrane or hollow-fibre membrane, temperature: 5～50 ℃, and pressure: 0.05～0.1Mpa.
(6) be that base stock is allocated with bee pollen stock solution, it consists of bee pollen 4～20%, high fructose syrup or sucrose 4～10%, and vitamin C 0.02-0.1%, citric acid concentration are 1～1.5 ‰, and the essence consumption is 0.75～1.5 (g/L), and all the other are water.
(7) the bee pollen liquid after will allocating promptly gets bee pollen nutrition oral liquid after through vacuum outgas, instantaneous ultra high temperature sterilization (UHTS), aseptic canning.Wherein vacuum outgas: vacuum is 0.02～0.1Mpa, and the degassing time is 10～60 minutes; Instantaneous ultra high temperature sterilization (UHTS): temperature: 121 ℃, 8～15 seconds time.
The present invention has following advantage than prior art:
(1) at first with bee pollen through the supercritical defat, this helps the later stage must clarify, the product appearance clarification is bright.
(2) adopt normal-temperature water to get to reduce high temperature for the thermal sensitivity loss of nutritive components.
(3) removed the material that causes muddiness easily by advanced membrane separation technique (microfiltration and ultrafiltration),, guaranteed the sensory characteristic of product clear as protein, macromole pigment etc.
(4) by allotment, changed the taste of some pollen stock solutions, make it have good mouthfeel.
(5) thus do not add the pure natural characteristic that any antiseptic and pigment have guaranteed product.
In order to understand essence of an invention better, describe technology contents of the present invention in detail with embodiment below, but content of the present invention is not limited thereto.
Embodiment 1
With 2 kilograms of Pollen Brassicae campestriss (moisture 5%) is raw material, it is joined in the 15L extractor, in extractor, feed liquefied petroleum gas then, carry out bee pollen dregs of rice precipitation and miscella precipitation in extraction under 20 ℃ of extraction temperature, the extracting pressure 0.1Mpa condition after 1 hour, the solvent compression is recycled, and obtains the bee pollen dregs of rice and bee pollen grease.Extract altogether 3 times, the oils and fats yield is 4.0% for the first time; According to the first time extraction conditions carry out second time extraction, the oils and fats yield is 0.5%; According to the first time extraction conditions extract for the third time, the oils and fats yield is 0.3%.The bee pollen dregs of rice are 0.07Mpa in vacuum, and precipitation promptly gets supercritical defat pollen under 40 ℃ of conditions of temperature after 0.5 hour.
0.5 kilogram of supercritical defat pollen joined in 5 liters the extraction pot, the distilled water that adds 2.5 kilograms again, carry 2 hours at 30 ℃ of water, in leaching process, constantly stir, after having extracted extracting solution is obtained supernatant through centrifugal (relative centrifugal force(RCF) is 4000g).In temperature is 40 ℃, adds 2.5 ‰ Bentonite bee pollen liquid is clarified, and stirs in clarifying process, and mixing speed is 140 rev/mins, and settling time is 3 hours.The centrifugal clear liquor that obtains after clarification finishes, relative centrifugal force(RCF) is 3000g when wherein centrifugal.Clear liquor is carried out separation and purification through membrance separation.At first with the micro-filtration membrane module of clear liquor by 0.1 μ m, and then by molecular weight is the hyperfiltration membrane assembly of 10000Da, obtains permeate.Film device: membrane module is adopted hollow-fibre membrane, temperature: 30 ℃, and pressure: 0.05～0.1Mpa.In 1000ml bee pollen permeate, successively add 50g high fructose syrup (F42), 0.25 gram citric acid, 0.25 gram vitamin C and green apple essence 1 gram then.Last deployed getting promptly gets bee pollen nutrition oral liquid after bee pollen liquid passes through vacuum outgas, instantaneous ultra high temperature sterilization (UHTS), aseptic canning.Wherein vacuum outgas: vacuum is 0.05Mpa, and the degassing time is 30 minutes; Instantaneous ultra high temperature sterilization (UHTS): temperature: 121 ℃, 11 seconds time.
Embodiment 2
With 500 kilograms of Pollen Brassicae campestriss (moisture 5%) is raw material, it is joined in the 4000L extractor, in extractor, feed liquefied petroleum gas then, carry out bee pollen dregs of rice precipitation and miscella precipitation in extraction under 50 ℃ of extraction temperature, the extracting pressure 0.8Mpa condition after 3.5 hours, the solvent compression is recycled, and obtains the bee pollen dregs of rice and bee pollen grease.Extract altogether 3 times, the oils and fats yield is 3.6% for the first time; According to the first time extraction conditions carry out second time extraction, the oils and fats yield is 0.8%; According to the first time extraction conditions extract for the third time, the oils and fats yield is 0.4%.The bee pollen dregs of rice are 0.08Mpa in vacuum, and precipitation promptly gets supercritical defat pollen under 40 ℃ of conditions of temperature after 1 hour.
475 kilograms of supercritical defat pollen are joined in 4000 liters the extraction pot, the distilled water that adds 2500 kilograms again, carry 2 hours at 30 ℃ of water, in leaching process, constantly stir, after having extracted extracting solution is obtained supernatant through centrifugal (relative centrifugal force(RCF) is 4000g).In temperature is 40 ℃, adds 2.5 ‰ Bentonite bee pollen liquid is clarified, and stirs in clarifying process, and mixing speed is 140 rev/mins, and settling time is 3 hours.The centrifugal clear liquor that obtains after clarification finishes, relative centrifugal force(RCF) is 3000g when wherein centrifugal.Clear liquor is carried out separation and purification through membrance separation.At first with the micro-filtration membrane module of clear liquor by 0.1 μ m, and then by molecular weight is the hyperfiltration membrane assembly of 10000Da, obtains permeate.Film device: membrane module is adopted hollow-fibre membrane, temperature: 30 ℃, and pressure: 0.05～0.1Mpa.In 1000L bee pollen permeate, successively add 50kg high fructose syrup (F42), 0.25kg citric acid, 0.25kg vitamin C and green apple essence 1kg then.Last deployed getting promptly gets bee pollen nutrition oral liquid after bee pollen liquid passes through vacuum outgas, instantaneous ultra high temperature sterilization (UHTS), aseptic canning.Wherein vacuum outgas: vacuum is 0.05Mpa, and the degassing time is 30 minutes; Instantaneous ultra high temperature sterilization (UHTS): temperature: 121 ℃, 11 seconds time.
Accompanying drawing: the technological process of bee pollen nutrition oral liquid
Claims (8)
1. bee pollen nutrition oral liquid, it is characterized in that: it is made with following method: adopt extracting oil and fat of bee pollen through supercutical fluid, carry out bee pollen dregs of rice precipitation and miscella precipitation after extract, solvent compresses recycling, obtains the bee pollen dregs of rice; It is centrifugal or filter and to obtain bee pollen stock solution that bee pollen dregs of rice water is carried the back; Add clarifier bee pollen stock solution is clarified, the clarification back that finishes is centrifugal or filter and obtain clear liquor, and clear liquor is obtained the bee pollen permeate through membrane filtration; Bee pollen permeate and adjuvant are allocated, afterwards through promptly getting bee pollen nutrition oral liquid behind vacuum outgas, instantaneous ultra high temperature sterilization (UHTS), the aseptic canning.
2. a kind of bee pollen nutrition oral liquid according to claim 1, it is characterized in that: wherein extracting oil and fat of bee pollen through supercutical fluid is earlier bee pollen to be joined in the extractor, in extractor, feed propane, butane or mixture then, continuous extraction is 1～10 hour under 10～60 ℃ of extraction temperature, extracting pressure 0.1～1Mpa condition, in extraction process, suitably stir.
3. a kind of bee pollen nutrition oral liquid according to claim 1 is characterized in that: carry out bee pollen dregs of rice precipitation and miscella precipitation after having extracted, the solvent compression is recycled, and obtains the bee pollen dregs of rice and bee pollen grease, and extraction times is 1～4 time; Bee pollen dregs of rice precipitation is a kind of endothermic process, therefore when precipitation, replenishes certain heat in the pollen dregs of rice, and the control heating-up temperature, stirs at a slow speed in the precipitation process below 50 ℃, helps solvent evaporates and heat transmission; Miscella precipitation condition: vacuum is 0.05～0.1Mpa, and temperature is 35～50 ℃, keeps to obtain bee pollen grease in 0.5～2 hour; Wherein bee pollen is 1: 1～4 with the ratio of shooting flow body weight, and wherein the charge of bee pollen accounts in the extractor volumetrical 3/4; In the above-mentioned bee pollen moisture 2～10%, the granularity of bee pollen is 5～100 orders, and wherein bee pollen is selected from Pollen Brassicae campestris, Pollen Maydis, Pollen Helianthi, Pollen Pini, Pollen Astragali Melilotoidis (Pollen Astragali Sinici), pollen of Semen Fagopyri Esculenti, Semen Sesami pollen, Sorghum vulgare Pers. pollen, Flos Camelliae Japonicae powder or Flos Nelumbinis pollen.
4. a kind of bee pollen nutrition oral liquid according to claim 1, it is characterized in that: it is centrifugal or filter and to obtain bee pollen stock solution that bee pollen dregs of rice water is carried the back, wherein extract 10～50 ℃ of temperature, extraction time is 0.5～6 hour, water is carried and is added citric acid or vitamin C in the process, concentration is 0.5～1 ‰, and the weight ratio of bee pollen and water is 1: 4～15.
5. a kind of bee pollen nutrition oral liquid according to claim 1, it is characterized in that: clarification: clarifier is gelatin, chitosan, Bentonite, PVPP or above clarifier is united use, concentration is 0.5～4 ‰, temperature is 0～50 ℃, stir in clarifying process, mixing speed is 20～200 rev/mins, and settling time is 0.5～24 hour, clarification finishes afterwards centrifugal or filters and obtains clear liquor, and relative centrifugal force(RCF) is 1500～5000g when wherein centrifugal.
6. a kind of bee pollen nutrition oral liquid according to claim 1, it is characterized in that: bee pollen is clarified the clear liquor that obtains after finish centrifugal or the filtration carry out separation and purification: at first with the micro-filtration membrane module of clear liquor by 0.1 μ m through membrance separation, and then be the hyperfiltration membrane assembly of 1000～20000Da by molecular weight, obtain permeate; Film device: membrane module adopts ceramic membrane or hollow-fibre membrane, temperature: 5～50 ℃, and pressure: 0.05～0.1Mpa.
7. a kind of bee pollen nutrition oral liquid according to claim 1, it is characterized in that: wherein the composition of bee pollen permeate and adjuvant allotment is a bee pollen 4～20%, high fructose syrup, Mel or sucrose 4～10%, vitamin C 0.02-0.1%, citric acid 1～1.5 ‰, the essence consumption is 0.75～1.5g/L, and surplus is a water.
8. a kind of bee pollen nutrition oral liquid according to claim 1, its feature: promptly get bee pollen nutrition oral liquid after will allocating back bee pollen liquid process vacuum outgas, instantaneous ultra high temperature sterilization (UHTS), aseptic canning, wherein vacuum outgas: vacuum is 0.02～0.1Mpa, and the degassing time is 10～60 minutes; Instantaneous ultra high temperature sterilization (UHTS): temperature: 121 ℃, 8～15 seconds time.
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| CN101332218B (en) * | 2007-06-29 | 2012-12-05 | 浙江海正药业股份有限公司 | Broken pollen extract and extracting method and use thereof |
| CN102389069A (en) * | 2011-11-14 | 2012-03-28 | 西华大学 | Bee pollen cell-wall breaking method, bee pollen oral solution and its preparation method |
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| CN105124675A (en) * | 2015-08-17 | 2015-12-09 | 安徽省天旭茶业有限公司 | Coffee fragrant tea pollen beverage and preparation technology thereof |
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| CN105077443A (en) * | 2015-08-17 | 2015-11-25 | 安徽省天旭茶业有限公司 | Tea pollen beverage capable of tonifying and developing brain and preparation process thereof |
| CN105076434A (en) * | 2015-08-17 | 2015-11-25 | 安徽省天旭茶业有限公司 | Camellia pollen beverage and preparation method thereof |
| CN105077479A (en) * | 2015-08-17 | 2015-11-25 | 安徽省天旭茶业有限公司 | Scented tea pollen beverage and preparation process thereof |
| CN105707801A (en) * | 2016-03-03 | 2016-06-29 | 扬州三邦生物工程有限公司 | Bee pollen and preparing method thereof |
| CN105767997A (en) * | 2016-03-03 | 2016-07-20 | 扬州三邦生物工程有限公司 | Bee pollen and preparation method thereof |
| CN112741321A (en) * | 2021-01-12 | 2021-05-04 | 沈阳荣药堂医药科技有限公司 | Pine pollen oral liquid and preparation method thereof |
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