CH89680A - Process for the preparation of a water-soluble blue dye of the anthraquinone series. - Google Patents

Process for the preparation of a water-soluble blue dye of the anthraquinone series.

Info

Publication number
CH89680A
CH89680A CH89680DA CH89680A CH 89680 A CH89680 A CH 89680A CH 89680D A CH89680D A CH 89680DA CH 89680 A CH89680 A CH 89680A
Authority
CH
Switzerland
Prior art keywords
sep
water
preparation
blue dye
anthraquinone series
Prior art date
Application number
Other languages
German (de)
Inventor
Anilin-Fabrikation Actien Fuer
Original Assignee
Anilin Fabrikation Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Anilin Fabrikation Ag filed Critical Anilin Fabrikation Ag
Publication of CH89680A publication Critical patent/CH89680A/en

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Description

  

  
EMI0001.0001     
  
    \'erfahren <SEP> zur <SEP> Darstellung <SEP> eines <SEP> wasserlösliehen <SEP> blauen <SEP> Farbstoff-,
<tb>  der <SEP> <B>Aiitlii'aelliiioiii'1'llie.</B>     
EMI0001.0002     
  
    Durch <SEP> das <SEP> Patent <SEP> Nr. <SEP> 70157 <SEP> und <SEP> die
<tb>  dazugehüAgen <SEP> Zusatzpatente. <SEP> N <SEP> r. <SEP> 7.1G:1-1 <SEP> 1111d
<tb>  <B>71655</B> <SEP> wurde <SEP> bekannt, <SEP> dass <SEP> plan <SEP> 1-:@m@no--1  halogenantbracbinon-2-sulfosiiure <SEP> init <SEP> einem
<tb>  aromatischen <SEP> Amin, <SEP> in <SEP> Gegenwart <SEP> voll <SEP> Wa  sen <SEP> und <SEP> Kupfer <SEP> oder <SEP> einer <SEP> Iiupl'erverl7in  dung, <SEP> zu <SEP> blauen <SEP> Farbstoffen <SEP> umsetzen <SEP> kann.
<tb>  



  Es <SEP> wurde <SEP> nun <SEP> gefunden, <SEP> dass <SEP> durch <SEP> Um  setzen <SEP> von <SEP> 1-Ä.minobalogenantbracbinon-G  sulfosüure <SEP> (Deutselles <SEP> Patent <SEP> Nr. <SEP> 7112G2)
<tb>  .Mit <SEP> 4-Toluidin <SEP> in <SEP> Gegenwart <SEP> voll <SEP>  'assen <SEP> lind
<tb>  Kupfer, <SEP> bezw. <SEP> einer <SEP> ICupferverbbulung <SEP> eile
<tb>  blauer <SEP> Farbstoff <SEP> entsteht, <SEP> der <SEP> Wolle <SEP> grün  stiolüg <SEP> l71au <SEP> färbt <SEP> und <SEP> in <SEP> Forin <SEP> filziger
<tb>  dunkler <SEP> Nadeln <SEP> erhältlich <SEP> ist, <SEP> die <SEP> siele <SEP> in
<tb>  beissein <SEP> Wasser <SEP> mit <SEP> grünblauer <SEP> Farbe <SEP> @üse11.
<tb>  <I>Beispiel</I>
<tb>  45 <SEP> GEL <SEP> bronberte <SEP> 1-Aminoantllracliiiioil  G-sulfosäure <SEP> des <SEP> deutschen <SEP> Patentes <SEP> 113262
<tb>  werden <SEP> mit <SEP> 30 <SEP> T1.

   <SEP> 4-Toluidin, <SEP> 1 <SEP> <B>TI.</B> <SEP> hl'i@a.
<tb>  Kupfersulfat, <SEP> 15 <SEP> TL <SEP> wasserfreier <SEP> Soda <SEP> und
<tb>  1000 <SEP> Tl. <SEP> Wasser <SEP> unter <SEP> lhiiclzfluss <SEP> gekocht.
<tb>  Bereits <SEP> naeli <SEP> wenigen <SEP> Minuten <SEP> wird <SEP> die <SEP> Flii"#-     
EMI0001.0003     
  
    <B>R1</B>gbr<B>7t. <SEP> f?'1'lllll1I</B>n<B>11. <SEP> \71#1177</B> <SEP> eine <SEP> <B>/.II17il,1LnLE-'</B> <SEP> der
<tb>  I'arli@tlil'I'lülllllli <SEP> niolitmehr <SEP> st-aflfindet,
<tb>  fiillt <SEP> 111:1n <SEP> den <SEP> Farhsoff <SEP> i77 <SEP> fat <SEP> reiner <SEP> Worin <SEP>   dllrtl <SEP> S:

  l.lzsaili'e <SEP> alle. <SEP> Er <SEP> bildet. <SEP> lial-ll <SEP> 11e111
<tb>  t@nllü@lli <SEP> aiilieitiem <SEP> @@'as@er <SEP> filzige <SEP> (1111111.e
<tb>  Nadeln, <SEP> die <SEP> fleh <SEP> 111 <SEP> <B>heissen</B> <SEP> IV ,r <SEP> 1177t <SEP> grLln  1;h1111'1' <SEP> 7,(11'11e <SEP> lösen.



  
EMI0001.0001
  
    \ 'learn <SEP> for <SEP> representation <SEP> of a <SEP> water-soluble <SEP> blue <SEP> dye,
<tb> the <SEP> <B> Aiitlii'aelliiioiii'1'llie. </B>
EMI0001.0002
  
    By <SEP> the <SEP> patent <SEP> no. <SEP> 70157 <SEP> and <SEP> die
<tb> associated <SEP> additional patents. <SEP> N <SEP> r. <SEP> 7.1G: 1-1 <SEP> 1111d
<tb> <B> 71655 </B> <SEP> became <SEP> known, <SEP> that <SEP> plan <SEP> 1 -: @ m @ no - 1 halogenantbracbinon-2-sulfosiiure <SEP> init <SEP> one
<tb> aromatic <SEP> amine, <SEP> in <SEP> presence <SEP> full <SEP> water <SEP> and <SEP> copper <SEP> or <SEP> of a <SEP> Iiupl'er connection, <SEP> can convert <SEP> to <SEP> blue <SEP> dyes <SEP>.
<tb>



  <SEP> was found <SEP> now <SEP>, <SEP> that <SEP> by <SEP> to set <SEP> from <SEP> 1-Ä.minobalogenantbracbinon-G sulfosüure <SEP> (German <SEP> Patent <SEP> No. <SEP> 7112G2)
<tb>. With <SEP> 4-toluidine <SEP> in <SEP> presence <SEP> full <SEP> 'ate <SEP> lind
<tb> copper, <SEP> resp. <SEP> of a <SEP> ICupfer bulge <SEP> hurry
<tb> blue <SEP> dye <SEP> is created, <SEP> the <SEP> wool <SEP> green stiolüg <SEP> l71au <SEP> dyes <SEP> and <SEP> in <SEP> Forin <SEP> tomentose
<tb> darker <SEP> needles <SEP> available <SEP> is, <SEP> the <SEP> siele <SEP> in
<tb> beissein <SEP> water <SEP> with <SEP> green-blue <SEP> color <SEP> @ üse11.
<tb> <I> Example </I>
<tb> 45 <SEP> GEL <SEP> bronberte <SEP> 1-Aminoantllracliiiioil G-sulfonic acid <SEP> of the <SEP> German <SEP> patent <SEP> 113262
<tb> become <SEP> with <SEP> 30 <SEP> T1.

   <SEP> 4-toluidine, <SEP> 1 <SEP> <B> TI. </B> <SEP> hl'i @ a.
<tb> copper sulphate, <SEP> 15 <SEP> TL <SEP> anhydrous <SEP> soda <SEP> and
<tb> 1000 <SEP> teaspoons <SEP> water <SEP> under <SEP> hot flow <SEP> boiled.
<tb> <SEP> naeli <SEP> already a few <SEP> minutes <SEP> will <SEP> the <SEP> Flii "# -
EMI0001.0003
  
    <B> R1 </B> gbr <B> 7t. <SEP> f? '1'lllll1I </B> n <B> 11. <SEP> \ 71 # 1177 </B> <SEP> a <SEP> <B> /.II17il,1LnLE- '</B> <SEP> the
<tb> I'arli @ tlil'I'lülllllli <SEP> niolitmehr <SEP> st-aflfinds,
<tb> fills <SEP> 111: 1n <SEP> the <SEP> Farhsoff <SEP> i77 <SEP> fat <SEP> pure <SEP> where <SEP> dllrtl <SEP> S:

  l.lzsaili'e <SEP> all. <SEP> He <SEP> forms. <SEP> lial-ll <SEP> 11e111
<tb> t @ nllü @ lli <SEP> aiilieitiem <SEP> @@ 'as @ er <SEP> felty <SEP> (1111111.e
<tb> needles, <SEP> which are called <SEP> fleh <SEP> 111 <SEP> <B> </B> <SEP> IV, r <SEP> 1177t <SEP> grLln 1; h1111'1 '<SEP > 7, (11'11e <SEP> solve.

Claims (1)

EMI0001.0004 P_\Tr\Ta-NSt'R<B>U</B>C71 <tb> Vorf:ibren <SEP> zier <SEP> Dara-ellmig <SEP> eines <SEP> wassc#r lüsliefcil <SEP> fLmen <SEP> Farl)toffeder <SEP> A.ntbraelli nonreilie, <SEP> der <SEP> Molle <SEP> @rünstiehi@; <SEP> 171a11 <SEP> fiii'171: <tb> imd <SEP> in <SEP> Form <SEP> filziger <SEP> dunkler <SEP> tadeln. <SEP> erlillt lieb <SEP> i4. <SEP> die <SEP> sieh <SEP> in <SEP> beisseni <SEP> @@"asser <SEP> mit <SEP> grün 1dalic'r <SEP> <I>AM</I> <SEP> 111#c.11. <SEP> daduruh <SEP> @Zehennzeicbnet, <tb> fliess <SEP> 111t111 <SEP> 1-,@.lnlllOllalll@,'(llall@b@aeblilllll-(i-3LLl fosül <SEP> 'e <SEP> in <SEP> C,-egnnlrai t- <SEP> von <SEP> Wasser <SEP> 11n(1 <SEP> lsnp fer <SEP> oller <SEP> e111('1' <SEP> Illlpfe7.'l"el'b@lld.1111@' <SEP> mit <SEP> 1-To lnidili <SEP> ninselzt. EMI0001.0004 P_ \ Tr \ Ta-NSt'R <B> U </B> C71 <tb> Vorf: ibren <SEP> zier <SEP> Dara-ellmig <SEP> of a <SEP> wassc # r lüsliefcil <SEP> fLmen <SEP> Farl) toffeder <SEP> A.ntbraelli nonreilie, <SEP> der < SEP> Molle <SEP> @ rünstiehi @; <SEP> 171a11 <SEP> fiii'171: <tb> imd <SEP> in <SEP> form <SEP> felty <SEP> darker <SEP> blame. <SEP> is loving <SEP> i4. <SEP> the <SEP> see <SEP> in <SEP> beisseni <SEP> @@ "asser <SEP> with <SEP> green 1dalic'r <SEP> <I> AM </I> <SEP> 111 # c.11. <SEP> daduruh <SEP> @Zehennzeicbnet, <tb> fliess <SEP> 111t111 <SEP> 1 -, @. lnlllOllalll @, '(llall @ b @ aeblilllll- (i-3LLl fosül <SEP>' e <SEP> in <SEP> C, -egnnlrai t- <SEP> from <SEP> water <SEP> 11n (1 <SEP> lsnp fer <SEP> oller <SEP> e111 ('1' <SEP> Illlpfe7.'l "el'b @ lld.1111 @ '<SEP > with <SEP> 1-To lnidili <SEP> ninselzt.
CH89680D 1914-06-22 1920-07-01 Process for the preparation of a water-soluble blue dye of the anthraquinone series. CH89680A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE73007X 1914-06-22
CH70157T 1914-07-04

Publications (1)

Publication Number Publication Date
CH89680A true CH89680A (en) 1921-06-01

Family

ID=25700583

Family Applications (1)

Application Number Title Priority Date Filing Date
CH89680D CH89680A (en) 1914-06-22 1920-07-01 Process for the preparation of a water-soluble blue dye of the anthraquinone series.

Country Status (1)

Country Link
CH (1) CH89680A (en)

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