CH191142A - Process for the production of an anthraquinone derivative. - Google Patents
Process for the production of an anthraquinone derivative.Info
- Publication number
- CH191142A CH191142A CH191142DA CH191142A CH 191142 A CH191142 A CH 191142A CH 191142D A CH191142D A CH 191142DA CH 191142 A CH191142 A CH 191142A
- Authority
- CH
- Switzerland
- Prior art keywords
- production
- anthraquinone derivative
- product
- derivative
- orange
- Prior art date
Links
- 238000004519 manufacturing process Methods 0.000 title claims description 5
- 238000000034 method Methods 0.000 title claims description 3
- RZVHIXYEVGDQDX-UHFFFAOYSA-N 9,10-anthraquinone Chemical compound C1=CC=C2C(=O)C3=CC=CC=C3C(=O)C2=C1 RZVHIXYEVGDQDX-UHFFFAOYSA-N 0.000 title description 3
- 239000000047 product Substances 0.000 claims description 4
- HDZGCSFEDULWCS-UHFFFAOYSA-N monomethylhydrazine Chemical compound CNN HDZGCSFEDULWCS-UHFFFAOYSA-N 0.000 claims description 3
- 239000013078 crystal Substances 0.000 claims description 2
- 239000000975 dye Substances 0.000 claims description 2
- 239000013067 intermediate product Substances 0.000 claims description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 2
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B5/00—Dyes with an anthracene nucleus condensed with one or more heterocyclic rings with or without carbocyclic rings
- C09B5/02—Dyes with an anthracene nucleus condensed with one or more heterocyclic rings with or without carbocyclic rings the heterocyclic ring being only condensed in peri position
- C09B5/04—Pyrazolanthrones
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Description
<B>Zusatzpatent</B> zum Hauptpatent Nr.189137. Verfahren zur Herstellung eines Anthrachinonderivates. Es wurde gefunden, dass man ein Anthra- chinonderivat herstellen kann, wenn man auf 1 - Amno - 5 - halogenanthrachinon Methyl- hydrazin einwirken lässt.
Das erhaltene Produkt der Formel
EMI0001.0015
bildet orangegefärbte Kristalle, die bei 2434 bis 235 schmelzen und sich in konzentrier ter Schwefelsäure mit oranger Färbe lösen. Das neue Produkt stellt ein wertvolles Zwi schenprodukt für die Herstellung von Farb stoffen dar.
<I>Beispiel:</I> 1,3 Teile 1,5-Aminochloranthrachinon, 18 Teile etwa 30prozentige wässerige Methyl- hydrazinlösung, 5 Teile .Soda und 150 Teile Pyridin werden 10 Stunden zum Sieden er- hitzt. Nach Erkalten wird abfiltriert, mit heissem Wasser gewaschen und ,getrocknet.
<B> Additional patent </B> to main patent number 189137. Process for the production of an anthraquinone derivative. It has been found that an anthraquinone derivative can be produced if 1 - amno - 5 - halogenanthraquinone methylhydrazine is allowed to act.
The product of the formula obtained
EMI0001.0015
forms orange-colored crystals that melt at 2434 to 235 and dissolve in concentrated sulfuric acid with an orange color. The new product is a valuable intermediate product for the manufacture of dyes.
<I> Example: </I> 1.3 parts of 1,5-aminochloranthraquinone, 18 parts of about 30 percent aqueous methylhydrazine solution, 5 parts of soda and 150 parts of pyridine are heated to the boil for 10 hours. After cooling, it is filtered off, washed with hot water and dried.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH189137T | 1936-02-07 | ||
| CH191142T | 1936-02-07 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH191142A true CH191142A (en) | 1937-05-31 |
Family
ID=25721740
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH191142D CH191142A (en) | 1936-02-07 | 1936-02-07 | Process for the production of an anthraquinone derivative. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH191142A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1257149B (en) * | 1963-06-04 | 1967-12-28 | Bayer Ag | Process for the preparation of 4, -5- or 8-amino-1, 9-pyrazole anthrones |
| EP0103381A1 (en) * | 1982-07-23 | 1984-03-21 | Warner-Lambert Company | Substituted anthra(1,9-cd)pyrazol-6(2H)-ones |
| US4556654A (en) * | 1983-06-28 | 1985-12-03 | Warner-Lambert Company | Antimicrobial substituted anthra[1,9-cd]pyrazol-6(2H)-ones |
-
1936
- 1936-02-07 CH CH191142D patent/CH191142A/en unknown
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1257149B (en) * | 1963-06-04 | 1967-12-28 | Bayer Ag | Process for the preparation of 4, -5- or 8-amino-1, 9-pyrazole anthrones |
| EP0103381A1 (en) * | 1982-07-23 | 1984-03-21 | Warner-Lambert Company | Substituted anthra(1,9-cd)pyrazol-6(2H)-ones |
| US4556654A (en) * | 1983-06-28 | 1985-12-03 | Warner-Lambert Company | Antimicrobial substituted anthra[1,9-cd]pyrazol-6(2H)-ones |
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