CH165054A - Process for the production of a new vat dye. - Google Patents

Process for the production of a new vat dye.

Info

Publication number
CH165054A
CH165054A CH165054DA CH165054A CH 165054 A CH165054 A CH 165054A CH 165054D A CH165054D A CH 165054DA CH 165054 A CH165054 A CH 165054A
Authority
CH
Switzerland
Prior art keywords
production
new
dye
vat dye
new vat
Prior art date
Application number
Other languages
German (de)
Inventor
Gesellschaft Fuer Chemis Basel
Original Assignee
Chem Ind Basel
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chem Ind Basel filed Critical Chem Ind Basel
Publication of CH165054A publication Critical patent/CH165054A/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B7/00—Indigoid dyes
    • C09B7/10—Bis-thionapthene indigos

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Oxygen Or Sulfur (AREA)
  • Coloring (AREA)

Description

  

  <B>Zusatzpatent</B> zum Hauptpatent Nr.<B>163280.</B>         Verfahren    zur Herstellung eines neuen     Küpenfarbstoifes.       Es wurde gefunden, dass man einen neuen       Küpenfarbstoff    erhält, wenn man das     2-(p-          Dimethylamino-)anil    des     4.7-Dimetbyl-3-oxy-          thionaphthens    mit 2     .1-Naphththioindoxyl     kondensiert.  



  Der neue     Farbstoff    der Formel  
EMI0001.0010     
    stellt ein     rötlichbraunes    Pulver dar, das sich  in konzentrierter Schwefelsäure mit blauer  Farbe löst und Baumwolle aus rotorange  gefärbter     Küpe    in schönen,     gelbstichig    rot  braunen Tönen von sehr guter Chlor-, Wasch-,       Beuch-    und Lichtechtheit färbt.  



  <I>Beispiel:</I>  310 Teile     2-(p-Dimethylamino-)ariil    des  4.     7-Dimethyl-3-oxythionaphthens,    das durch    Einwirkung von     p-Nitrosodimethylanilin    auf       4.7-Dimethyl-3-oxythionaplithen    erhalten  wird und einen Schmelzpunkt von 208   zeigt,  werden mit 200 Teilen 2 .     1-Naphththioindo-          xyl    in 5000 Teilen Alkohol bis zu beendeter  Kondensation gekocht. Dann wird filtriert,  mit Alkohol gewaschen und der     Farbstoff     getrocknet.



  <B> Additional patent </B> to the main patent no. <B> 163280. </B> Process for the production of a new vat dye. It has been found that a new vat dye is obtained if the 2- (p-dimethylamino) anil of 4,7-dimethyl-3-oxythionaphthens is condensed with 2 .1-naphthioindoxyl.



  The new dye in the formula
EMI0001.0010
    is a reddish-brown powder that dissolves in concentrated sulfuric acid with a blue color and dyes cotton from a red-orange vat in beautiful, yellow-tinged red-brown shades of very good fastness to chlorine, washing, touching and light.



  <I> Example: </I> 310 parts of 2- (p-dimethylamino) ariil of 4. 7-dimethyl-3-oxythionaphthene, which is obtained by the action of p-nitrosodimethylaniline on 4,7-dimethyl-3-oxythionapliths and one Melting point of 208 shows, with 200 parts 2. 1-Naphththioindoxyl boiled in 5000 parts of alcohol until condensation has ended. It is then filtered, washed with alcohol and the dye is dried.

Claims (1)

PATENTANSPRUCH: Verfahren zur Herstellung eines neuen Küpenfarbstoffes, dadurch gekennzeichnet, dass man das 2-(p-Dimethylamino-)anil des 4.7-Dimethyl-3-oxythionaphtheus mit 2.1- Naphththioindoxyl kondensiert. PATENT CLAIM: Process for the production of a new vat dye, characterized in that the 2- (p-dimethylamino-) anil of 4.7-dimethyl-3-oxythionaphtheus is condensed with 2.1-naphththioindoxyl. Der neue Farbstoff der Formel EMI0001.0028 stellt ein rötlichbraunes Pulver dar, das sich in konzentrierter Schwefelsäure mit blauer Farbe löst und Baumwolle aus rotorange gefärbter Küpe in schönen, gelbstichig rot- braunen Tönen von sehr guter Chlor-, Wasch-, Beuch- und Lichtechtheit färbt. The new dye in the formula EMI0001.0028 is a reddish-brown powder that dissolves in concentrated sulfuric acid with a blue color and dyes cotton from a red-orange vat in beautiful, yellow-tinged red-brown shades of very good resistance to chlorine, washing, contact and light.
CH165054D 1932-07-15 1932-07-15 Process for the production of a new vat dye. CH165054A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH163280T 1932-07-15
CH165054T 1932-07-15

Publications (1)

Publication Number Publication Date
CH165054A true CH165054A (en) 1933-10-31

Family

ID=25717741

Family Applications (1)

Application Number Title Priority Date Filing Date
CH165054D CH165054A (en) 1932-07-15 1932-07-15 Process for the production of a new vat dye.

Country Status (1)

Country Link
CH (1) CH165054A (en)

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