CH156312A - Process for the production of a chromium-containing dye. - Google Patents

Process for the production of a chromium-containing dye.

Info

Publication number
CH156312A
CH156312A CH156312DA CH156312A CH 156312 A CH156312 A CH 156312A CH 156312D A CH156312D A CH 156312DA CH 156312 A CH156312 A CH 156312A
Authority
CH
Switzerland
Prior art keywords
dye
chromium
production
containing dye
oxynaphthalene
Prior art date
Application number
Other languages
German (de)
Inventor
Gesellschaft Fuer Chemis Basel
Original Assignee
Chem Ind Basel
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chem Ind Basel filed Critical Chem Ind Basel
Publication of CH156312A publication Critical patent/CH156312A/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B45/00—Complex metal compounds of azo dyes
    • C09B45/02—Preparation from dyes containing in o-position a hydroxy group and in o'-position hydroxy, alkoxy, carboxyl, amino or keto groups
    • C09B45/14—Monoazo compounds
    • C09B45/16—Monoazo compounds containing chromium

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Paper (AREA)
  • Coloring (AREA)

Description

  

  Zusatzpatent zum Hauptpatent Nr. 152880.         -'erfahren    zur     Herstellung    eines     ehromhaltigen        Farbstoffes.       Es wurde gefunden, dass ein neuer     chrom-          haltiger        .Farbstoff,    der auf jede     ehromierbare     Gruppe des     Farbstoffmoleküls    1 Atom Chrom  enthält, erhalten wird, wenn man den Farb  stoff aus     diazotierter        1-Amirio-2-oxynaph-          tlialin-4-sulfosäure    und     1-Oxynaphthalin    mit  Chromsulfat behandelt.  



  Der gebildete Farbstoff stellt ein dunkel  blaues Pulver dar, das sich in     verdünnter     Soda mit     rotstichig    blauer Farbe löst     und     Wolle aus     schwefelsaurem    Bad in     grünstichig     blauen Tönen färbt.  



  <I>Beispiel:</I>  39,4 Teile des Farbstoffes aus     diazotierter          1-Ainino-2-oxynaphthalin-4-sulfosäure    und     1-          Oxynaphthalin    werden in 2000 Teilen Wasser       aufgekocht    und mit einer aus 9,1 Teilen       Cr20s    und 14,6 Teilen     132S04    erhaltenen       Chromsulfatlösung    während 30 Stunden am       Riiel@flufküliler    zum Kochen erhitzt. Die    Chromverbindung scheidet sich nach dem       Erkalten    aus der     Lösung    aus; sie wird ab  filtriert, ausgewaschen und bei mässiger  Temperatur getrocknet.



  Additional patent to the main patent No. 152880. -'erfahren for the production of an Ehrom-containing dye. It has been found that a new chromium-containing dyestuff which contains 1 atom of chromium for every honorable group of the dyestuff molecule is obtained if the dyestuff is obtained from diazotized 1-aminophthalene-4-sulfonic acid and 1 -Oxynaphthalene treated with chromium sulfate.



  The dye formed is a dark blue powder that dissolves in dilute soda with a reddish blue color and dyes wool from a sulfuric acid bath in greenish blue tones.



  <I> Example: </I> 39.4 parts of the dye from diazotized 1-amino-2-oxynaphthalene-4-sulfonic acid and 1-oxynaphthalene are boiled in 2000 parts of water and mixed with one of 9.1 parts of Cr20s and 14, 6 parts of 132S04 obtained chromium sulfate solution heated to boiling on a Riiel @ flufküliler for 30 hours. The chromium compound separates out of the solution after cooling; it is filtered off, washed and dried at a moderate temperature.

Claims (1)

PATENTANSPRUCH: Verfahren zur Herstellung eines chruin- lialtigen Farbstoffes, der auf jede chroinier- bare Gruppe des Farbstoffmoleküls 1 Atom Chrom enthält, dadurch gekennzeichnet, dass nian den Farbstoff aus diazotierter 1-Amino- oxynaphthalin -4- sulfosäure und 1-Oxyiiapli- thalin mit Chromsulfat behandelt. PATENT CLAIM: A process for the production of a chruin-lialtigen dye which contains 1 atom of chromium for each chrominable group of the dye molecule, characterized in that the dye from diazotized 1-amino-oxynaphthalene -4-sulfonic acid and 1-oxyiiapli- thalin with Treated chromium sulfate. Der gebildete Farbstoff stellt ein dunkel- blaues Pulver dar, das sich in verdünnter Soda-mit rotstichig blauer Farbe löst und .Wolle aus schwefelsaurem Bade in grün stichig blauen Tönen färbt. The dye formed is a dark blue powder that dissolves in dilute soda with a reddish blue color and dyes wool from sulfuric acid bath in greenish blue tones.
CH156312D 1929-12-18 1929-12-18 Process for the production of a chromium-containing dye. CH156312A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH152880T 1929-12-18
CH156312T 1929-12-18

Publications (1)

Publication Number Publication Date
CH156312A true CH156312A (en) 1932-07-31

Family

ID=25716046

Family Applications (1)

Application Number Title Priority Date Filing Date
CH156312D CH156312A (en) 1929-12-18 1929-12-18 Process for the production of a chromium-containing dye.

Country Status (1)

Country Link
CH (1) CH156312A (en)

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