CH156316A - Process for the production of a chromium-containing dye. - Google Patents

Process for the production of a chromium-containing dye.

Info

Publication number
CH156316A
CH156316A CH156316DA CH156316A CH 156316 A CH156316 A CH 156316A CH 156316D A CH156316D A CH 156316DA CH 156316 A CH156316 A CH 156316A
Authority
CH
Switzerland
Prior art keywords
chromium
dye
production
containing dye
yellow
Prior art date
Application number
Other languages
German (de)
Inventor
Gesellschaft Fuer Chemis Basel
Original Assignee
Chem Ind Basel
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chem Ind Basel filed Critical Chem Ind Basel
Publication of CH156316A publication Critical patent/CH156316A/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B45/00Complex metal compounds of azo dyes
    • C09B45/02Preparation from dyes containing in o-position a hydroxy group and in o'-position hydroxy, alkoxy, carboxyl, amino or keto groups
    • C09B45/14Monoazo compounds
    • C09B45/16Monoazo compounds containing chromium

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Coloring (AREA)

Description

  

  <B>Zusatzpatent</B> zum Hauptpatent Nr. 152880.         Verfahren    zur     Herstellung        eines        chromhaltigen    Farbstoffes.    Es wurde gefunden, dass ein neuer     chrom-          haltiger    Farbstoff, der auf jede     chromierbare     Gruppe des     Farbstoffmoleküls    1 Atom Chrom  enthält, erhalten wird, wenn man den Farb  stoff aus dianotierter 1-     Aminonaphtalin    - 4     -          sulfosäure    und     1-Oxybenzol-2-carbonsäui,e    mit  Chromsulfat behandelt.  



  Der gebildete Farbstoff stellt ein braun  gelbes Pulver, das sich in Wasser mit braun  stichig gelber Farbe löst und Wolle aus  schwefelsaurem Bade in     rotstichig    gelben  Tönen färbt.    <I>Beispiel:</I>    37 Teile des     Farbstoffes    aus dianotierter       1-Aininonaphtalin-4-sulfosäure    und     1-Oxy-          benzol-2-cai-bonsäure    werden in 1500 Teilen  Wasser gelöst und während einigen     Stunden     mit einer aus 9,1 Teilen     Cr20a    und 14,6 Teilen       H2S04    erhaltenen     Ohromsulfatlösung    zum  Kochen erhitzt.

   Nach Beendigung der Chro-         mierung    wird die gebildete Chromverbindung  durch Zugabe von Kochsalz aus der Lösung  abgeschieden, filtriert und bei mässiger Tem  peratur getrocknet.



  <B> Additional patent </B> to the main patent No. 152880. Process for the production of a chromium-containing dye. It has been found that a new chromium-containing dye, which contains 1 atom of chromium for every chromable group of the dye molecule, is obtained if the dye is obtained from dianotized 1-aminonaphthalene-4-sulfonic acid and 1-oxybenzene-2-carboxylic acid, e treated with chromium sulfate.



  The dye formed is a brown-yellow powder that dissolves in water with a brown-tinged yellow color and dyes wool from sulfuric acid bath in red-tinged yellow shades. <I> Example: </I> 37 parts of the dye from dianotized 1-amino naphthalene-4-sulfonic acid and 1-oxybenzene-2-cai-bonic acid are dissolved in 1500 parts of water and mixed with one of 9.1 for a few hours Parts of Cr20a and 14.6 parts of H2S04 are heated to boiling.

   When the chromium plating has ended, the chromium compound formed is separated out from the solution by adding sodium chloride, filtered and dried at a moderate temperature.

 

Claims (1)

PATENTANSPRUCH: Verfahren zur Herstellung eines chrom haltigen Farbstoffes, der auf jede chromier- bare Gruppe des Farbstoffmoleküls 1 Atom Chrom enthält, dadurch gekennzeichnet, dah man den Farbstoff aus dianotierter 1-Amino- naphtalin-4-sulfosäure und 1-Oxybenzol-2- carbonsäure mit Chromsulfat behandelt. PATENT CLAIM: Process for the production of a chromium-containing dye which contains 1 atom of chromium for every chromable group of the dye molecule, characterized in that the dye is made from dianotated 1-amino-naphthalene-4-sulfonic acid and 1-oxybenzene-2-carboxylic acid treated with chromium sulfate. Der gebildete Farbstoff stellt ein braun gelbes Pulver dar, das sich in Wasser mit braunstichig gelber Farbe löst und Wolle aus schwefelsaurem Bade in rotstichig gelben Tönen färbt. The dye formed is a brown-yellow powder that dissolves in water with a brownish yellow color and dyes wool from sulfuric acid bath in reddish yellow tones.
CH156316D 1929-12-18 1929-12-18 Process for the production of a chromium-containing dye. CH156316A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH152880T 1929-12-18
CH156316T 1929-12-18

Publications (1)

Publication Number Publication Date
CH156316A true CH156316A (en) 1932-07-31

Family

ID=25716050

Family Applications (1)

Application Number Title Priority Date Filing Date
CH156316D CH156316A (en) 1929-12-18 1929-12-18 Process for the production of a chromium-containing dye.

Country Status (1)

Country Link
CH (1) CH156316A (en)

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