CH166082A - Process for the production of a new metal-containing dye. - Google Patents

Process for the production of a new metal-containing dye.

Info

Publication number
CH166082A
CH166082A CH166082DA CH166082A CH 166082 A CH166082 A CH 166082A CH 166082D A CH166082D A CH 166082DA CH 166082 A CH166082 A CH 166082A
Authority
CH
Switzerland
Prior art keywords
containing dye
production
new metal
dye
metal
Prior art date
Application number
Other languages
German (de)
Inventor
Gesellschaft Fuer Chemis Basel
Original Assignee
Chem Ind Basel
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chem Ind Basel filed Critical Chem Ind Basel
Publication of CH166082A publication Critical patent/CH166082A/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B45/00—Complex metal compounds of azo dyes
    • C09B45/02—Preparation from dyes containing in o-position a hydroxy group and in o'-position hydroxy, alkoxy, carboxyl, amino or keto groups
    • C09B45/14—Monoazo compounds
    • C09B45/16—Monoazo compounds containing chromium

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Coloring (AREA)

Description

  

      Zusatzpatent    zum Hauptpatent Nr. 163542.    Verfahren zur Herstellung eines neuen metallhaltigen Farbstoffes.    Es wurde gefunden, dass man einen neuen       metallhaltigen        Farbstoff'    erhalten kann, wenn  man den     Azofarbstoff    aus     diazotierter        4-Sulfo-          2-aminobettzol-l-karbonsäure    und     1-Phenyl-3-          methyl    - 5 -     pyrazolon    mit     chromabgebenden     Mitteln behandelt.  



  Der erhaltene metallhaltige     Farbstoff    stellt  ein dunkelgelbes Pulver dar, das sich in  Wasser mit gelber Farbe löst und Wolle aus  saurem Bade in     rotstichigen    Gelbtönen von  guten Echtheitseigenschaften färbt.  



  <I>Beispiel:</I>  18,9 Teile des     Azofarbstoffes    aus     dia7o-          tierter        4-Sulfo-2-aminobenzol-l-karbonsäure     und     1-Pltenyl-3-methyl-5-pyrazol <  i    werden in  <B>500</B> Teilen Wasser gelöst und mit 4,6 Teilen  Chromoxyd in Form von     Chlorfluorid    mehrere    Stunden rückfliessend gekocht. Man scheidet  sodann den     chromierten        Farbstoff    mit Koch  salz aus, filtriert und trocknet.



      Additional patent to main patent No. 163542. Process for the production of a new metal-containing dye. It has been found that a new metal-containing dye can be obtained by treating the azo dye from diazotized 4-sulfo-2-aminobettzole-1-carboxylic acid and 1-phenyl-3-methyl-5-pyrazolone with chromium-donating agents.



  The metal-containing dye obtained is a dark yellow powder which dissolves in water with a yellow color and dyes wool from an acid bath in reddish yellow shades with good fastness properties.



  <I> Example: </I> 18.9 parts of the azo dye from dia7otated 4-sulfo-2-aminobenzene-1-carboxylic acid and 1-pltenyl-3-methyl-5-pyrazole are used in 500 </B> Parts of water dissolved and refluxed for several hours with 4.6 parts of chromium oxide in the form of chlorofluoride. The chromized dye is then separated out with sodium chloride, filtered and dried.

Claims (1)

PATENTANSPRUCH: Verfahren zur Herstellung eines neuen metallhaltigen Farbstoffes, dadurch gekenn zeichnet, dass man den Azofarbstoff aus di- azotierter 4-Sulfo-2-aminobenzol-l-karbon- säure und 1-Phenyl-3-methyl-5-pyrazolon mit chromabgebenden Mitteln behandelt. Der erhaltene metallhaltige Farbstoff stellt ein dunkelgelbes Pulver dar, das sich in Wasser mit gelber Farbe löst und Wolle aus saurem Bade in rotstichigen Gelbtönen von guten Echtheitseigenschaften färbt. PATENT CLAIM: Process for the production of a new metal-containing dye, characterized in that the azo dye from diazo-4-sulfo-2-aminobenzene-1-carbonic acid and 1-phenyl-3-methyl-5-pyrazolone with chromium-releasing agents treated. The metal-containing dye obtained is a dark yellow powder which dissolves in water with a yellow color and dyes wool from an acid bath in reddish yellow shades with good fastness properties.
CH166082D 1932-07-20 1932-07-20 Process for the production of a new metal-containing dye. CH166082A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH163542T 1932-07-20
CH166082T 1932-07-20

Publications (1)

Publication Number Publication Date
CH166082A true CH166082A (en) 1933-12-15

Family

ID=25717799

Family Applications (1)

Application Number Title Priority Date Filing Date
CH166082D CH166082A (en) 1932-07-20 1932-07-20 Process for the production of a new metal-containing dye.

Country Status (1)

Country Link
CH (1) CH166082A (en)

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