CH144759A - Process for the production of a new metal-containing dye. - Google Patents

Process for the production of a new metal-containing dye.

Info

Publication number
CH144759A
CH144759A CH144759DA CH144759A CH 144759 A CH144759 A CH 144759A CH 144759D A CH144759D A CH 144759DA CH 144759 A CH144759 A CH 144759A
Authority
CH
Switzerland
Prior art keywords
containing dye
production
new metal
metal
dye
Prior art date
Application number
Other languages
German (de)
Inventor
Gesellschaft Fuer Chemis Basel
Original Assignee
Chem Ind Basel
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chem Ind Basel filed Critical Chem Ind Basel
Publication of CH144759A publication Critical patent/CH144759A/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B45/00—Complex metal compounds of azo dyes
    • C09B45/02—Preparation from dyes containing in o-position a hydroxy group and in o'-position hydroxy, alkoxy, carboxyl, amino or keto groups
    • C09B45/14—Monoazo compounds
    • C09B45/16—Monoazo compounds containing chromium

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Coloring (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Description

  

      Zusatzpatent    zum     Hauptpatent    Nr. 143026.    Verfahren zur Herstellung eines neuen metallhaltigen Farbstoffes.    Es wurde gefunden, dass man einen neuen  metallhaltigen     Farbstoff    erhält, wenn man  den     Azofarbstoff    aus     5-Nitro-2-diazo-l-phenol     und     1-(Benzoylainino)-8-oxynaphthalin-4-sulfo-          säure    mit chromabgebenden Mitteln behandelt.  



  Der erhaltene metallhaltige Farbstoff bil  det getrocknet ein dunkles Pulver, das sich  in Wasser mit graublauer Farbe löst und  Naturseide in     rotstichig    grauen Tönen färbt.       Beispiel:     5,08 Teile des durch Kombinieren von       diazotiertem        5-Nitro-2-amino-l-pheiiol    und     1-          (Benzoylamino)-8-oxynaphthalin    - 4 -     sulfosäure     in alkalischer Lösung erhaltenen     Farbstoffes     werden in 400 Teilen Wasser gelöst und mit  20 Teilen einer 7,

  6      /o        Cr2        0s    enthaltenden       Fluorchromlösung    24-30 Stunden am Rück-         flusskühler    zum Kochen erhitzt.     Hierauf    wird  die gebildete Chromverbindung mit Kochsalz  abgeschieden, filtriert und bei mässiger Tem  peratur getrocknet.



      Additional patent to main patent no. 143026. Process for the production of a new metal-containing dye. It has been found that a new metal-containing dye is obtained if the azo dye composed of 5-nitro-2-diazo-1-phenol and 1- (benzoylainino) -8-oxynaphthalene-4-sulfonic acid is treated with chromium donating agents.



  The metal-containing dye obtained forms a dark powder when dried, which dissolves in water with a gray-blue color and dyes natural silk in reddish gray tones. Example: 5.08 parts of the dye obtained by combining diazotized 5-nitro-2-amino-1-phenol and 1- (benzoylamino) -8-oxynaphthalene-4-sulfonic acid in an alkaline solution are dissolved in 400 parts of water and mixed with 20 Split a 7,

  6 / o Cr2 0s containing fluorochrome solution heated to boiling for 24-30 hours on the reflux condenser. The chromium compound formed is then deposited with common salt, filtered and dried at a moderate temperature.

Claims (1)

PATENTANSPRUCH: Verfahren zur Herstellung eines neuen metallhaltigen Farbstoffes, dadurch gekenn zeichnet, dass man den Azofarbstoff aus 5- Nitro-2-diazo-l-phenol und 1-(Benzoylamirio)- 8-oxynaphthalin-4-sulfosäure mit chromabge benden Mitteln behandelt. Der erhaltene metallhaltige Farbstoff bil det getrocknet ein dunkles Pulver, das sich in Wasser mit graublauer Farbe löst und Naturseide in rotstichig grauen Tönen färbt. PATENT CLAIM: Process for the production of a new metal-containing dye, characterized in that the azo dye from 5- nitro-2-diazo-1-phenol and 1- (benzoylamirio) - 8-oxynaphthalene-4-sulfonic acid is treated with chromium-releasing agents. The metal-containing dye obtained forms a dark powder when dried, which dissolves in water with a gray-blue color and dyes natural silk in reddish gray tones.
CH144759D 1929-03-16 1929-03-16 Process for the production of a new metal-containing dye. CH144759A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH143026T 1929-03-16
CH144759T 1929-03-16

Publications (1)

Publication Number Publication Date
CH144759A true CH144759A (en) 1931-01-15

Family

ID=25714184

Family Applications (1)

Application Number Title Priority Date Filing Date
CH144759D CH144759A (en) 1929-03-16 1929-03-16 Process for the production of a new metal-containing dye.

Country Status (1)

Country Link
CH (1) CH144759A (en)

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