CH161841A - Process for the production of a new azo dye. - Google Patents
Process for the production of a new azo dye.Info
- Publication number
- CH161841A CH161841A CH161841DA CH161841A CH 161841 A CH161841 A CH 161841A CH 161841D A CH161841D A CH 161841DA CH 161841 A CH161841 A CH 161841A
- Authority
- CH
- Switzerland
- Prior art keywords
- production
- azo dye
- new azo
- azo
- wool
- Prior art date
Links
- 239000000987 azo dye Substances 0.000 title description 3
- 239000000975 dye Substances 0.000 claims description 5
- 150000003931 anilides Chemical class 0.000 claims description 3
- ZYECOAILUNWEAL-NUDFZHEQSA-N (4z)-4-[[2-methoxy-5-(phenylcarbamoyl)phenyl]hydrazinylidene]-n-(3-nitrophenyl)-3-oxonaphthalene-2-carboxamide Chemical compound COC1=CC=C(C(=O)NC=2C=CC=CC=2)C=C1N\N=C(C1=CC=CC=C1C=1)/C(=O)C=1C(=O)NC1=CC=CC([N+]([O-])=O)=C1 ZYECOAILUNWEAL-NUDFZHEQSA-N 0.000 claims description 2
- 229920002955 Art silk Polymers 0.000 claims description 2
- 229920000742 Cotton Polymers 0.000 claims description 2
- 239000000843 powder Substances 0.000 claims description 2
- 239000000758 substrate Substances 0.000 claims description 2
- 210000002268 wool Anatomy 0.000 claims description 2
- 239000002253 acid Substances 0.000 claims 1
- 125000000956 methoxy group Chemical group [H]C([H])([H])O* 0.000 claims 1
- 239000000126 substance Substances 0.000 claims 1
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- OCISOSJGBCQHHN-UHFFFAOYSA-N 3-hydroxynaphthalene-1-carboxylic acid Chemical compound C1=CC=C2C(C(=O)O)=CC(O)=CC2=C1 OCISOSJGBCQHHN-UHFFFAOYSA-N 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- -1 wool Polymers 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B29/00—Monoazo dyes prepared by diazotising and coupling
- C09B29/10—Monoazo dyes prepared by diazotising and coupling from coupling components containing hydroxy as the only directing group
- C09B29/18—Monoazo dyes prepared by diazotising and coupling from coupling components containing hydroxy as the only directing group ortho-Hydroxy carbonamides
- C09B29/20—Monoazo dyes prepared by diazotising and coupling from coupling components containing hydroxy as the only directing group ortho-Hydroxy carbonamides of the naphthalene series
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Coloring (AREA)
Description
Verfahren zur Herstellung eines neuen Azofarbstoffes. Es wurde gefunden, dass man einen neuen Azofarbstoff der Formel:
EMI0001.0003
erhält, wenn man den 2-Diazo-4.4'-dimeth- oay-5-acetylamino-1.1'-diphenyläther mit dem Anilid der 2.3-Oxynaphtoesäure kuppelt. Der so erhaltene Farbstoff bildet ein rot violettes Pulver. Auf geeigneten Substraten, wie zum Beispiel Baumwolle, Wolle, Kunst seide hergestellt, färbt er diese in leuchten den, sehr echten violetten Tönen.
<I>Beispiel:</I> 30,2 Teile 2-Amino-4.4'-dimethoxy-5- acetylamino-1.1'-diphenyläther werden wie üblich diazotiert und in eine Lösung von 26,3 Teilen des Anilids der 2 . 3-Oxynaphtoe- säure, 60 Teilen 30 o/oiger Natriumhydroxyd- lösung, 15 Teilen Soda und 2000 Teilen Wasser eingetragen. Der gebildete Farbstoff fällt sofort aus. Er wird filtriert; gewaschen und getrocknet.
Process for the production of a new azo dye. It has been found that a new azo dye of the formula:
EMI0001.0003
obtained when the 2-diazo-4.4'-dimeth-oay-5-acetylamino-1.1'-diphenyl ether is coupled with the anilide of 2.3-oxynaphthoic acid. The dye thus obtained forms a red-violet powder. Produced on suitable substrates such as cotton, wool, artificial silk, he dyes them in bright, very real purple tones.
<I> Example: </I> 30.2 parts of 2-amino-4,4'-dimethoxy-5-acetylamino-1,1'-diphenyl ether are diazotized as usual and poured into a solution of 26.3 parts of the anilide of the 2nd 3-Oxynaphthoic acid, 60 parts of 30% sodium hydroxide solution, 15 parts of soda and 2000 parts of water were added. The dye formed precipitates immediately. It is filtered; washed and dried.
Claims (1)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CH161841T | 1932-04-11 |
Publications (1)
Publication Number | Publication Date |
---|---|
CH161841A true CH161841A (en) | 1933-05-31 |
Family
ID=4415122
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CH161841D CH161841A (en) | 1932-04-11 | 1932-04-11 | Process for the production of a new azo dye. |
Country Status (1)
Country | Link |
---|---|
CH (1) | CH161841A (en) |
-
1932
- 1932-04-11 CH CH161841D patent/CH161841A/en unknown
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