CH144192A - Process for the preparation of 1-phenoxy-3-isobutyryloxy-propane. - Google Patents
Process for the preparation of 1-phenoxy-3-isobutyryloxy-propane.Info
- Publication number
- CH144192A CH144192A CH144192DA CH144192A CH 144192 A CH144192 A CH 144192A CH 144192D A CH144192D A CH 144192DA CH 144192 A CH144192 A CH 144192A
- Authority
- CH
- Switzerland
- Prior art keywords
- propane
- phenoxy
- isobutyryloxy
- preparation
- oxy
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 3
- CKNQCZOAGZXQIN-UHFFFAOYSA-N 3-phenoxypropyl 2-methylpropanoate Chemical compound CC(C)C(=O)OCCCOC1=CC=CC=C1 CKNQCZOAGZXQIN-UHFFFAOYSA-N 0.000 title description 2
- 239000001294 propane Substances 0.000 claims description 3
- 239000003795 chemical substances by application Substances 0.000 claims description 2
- 239000007788 liquid Substances 0.000 claims description 2
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N dimethylmethane Natural products CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 claims 1
- KQNPFQTWMSNSAP-UHFFFAOYSA-N isobutyric acid Chemical compound CC(C)C(O)=O KQNPFQTWMSNSAP-UHFFFAOYSA-N 0.000 description 2
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Description
Verfahren zur Darstellung von 1-Phenogy-3-isobutyryloay-propan. Nach vorliegender Erfindung gewinnt man das bisher unbekannte 1-Phenoxy 3-isobuty- ryloxy-propan, eine fruchtigsüss riechende farblose Flüssigkeit, D150 =1. 023, Kp.sn,m = 138-141<B>0</B>; indem man 1-Phenoxy-3-oxy-propan mit Iso- butyrylierungsmitteln behandelt. Die Ver bindung soll als Riechstoff Verwendung finden.
<I>Beispiel:</I> 1 Mol 1-Pherioxy-3-oxy-propari wird mit 1 Mol Isobuttersäure 8 Stunden langsam bis auf 205 erhitzt, wobei das freiwerdende Wasser übergeht. Das Reaktionsprodukt wird neutral gewaschen und im Vakuum fraktioniert.
Process for the preparation of 1-phenogy-3-isobutyryloyl-propane. According to the present invention, the previously unknown 1-phenoxy 3-isobutyryloxy-propane, a fruity-sweet smelling colorless liquid, D150 = 1, is obtained. 023, Kp.sn, m = 138-141 <B> 0 </B>; by treating 1-phenoxy-3-oxy-propane with isobutyrylating agents. The connection is intended to be used as a fragrance.
<I> Example: </I> 1 mole of 1-pherioxy-3-oxy-propariate is slowly heated to 205 for 8 hours with 1 mole of isobutyric acid, with the released water passing over. The reaction product is washed neutral and fractionated in vacuo.
Claims (1)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE144192X | 1928-11-06 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH144192A true CH144192A (en) | 1930-12-15 |
Family
ID=5670091
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH144192D CH144192A (en) | 1928-11-06 | 1929-03-18 | Process for the preparation of 1-phenoxy-3-isobutyryloxy-propane. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH144192A (en) |
-
1929
- 1929-03-18 CH CH144192D patent/CH144192A/en unknown
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