CH143223A - Process for the preparation of a compound with a hydrogenated ring system. - Google Patents

Process for the preparation of a compound with a hydrogenated ring system.

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Publication number
CH143223A
CH143223A CH143223DA CH143223A CH 143223 A CH143223 A CH 143223A CH 143223D A CH143223D A CH 143223DA CH 143223 A CH143223 A CH 143223A
Authority
CH
Switzerland
Prior art keywords
preparation
compound
ring system
hydrogenated ring
crotonaldehyde
Prior art date
Application number
Other languages
German (de)
Inventor
Aktiengesellsc Farbenindustrie
Original Assignee
Ig Farbenindustrie Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ig Farbenindustrie Ag filed Critical Ig Farbenindustrie Ag
Publication of CH143223A publication Critical patent/CH143223A/en

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  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Description

  

      Verfahren    zur Darstellung einer Verbindung mit hydriertem Ringsystem.    Gegenstand dieses Zusatzpatentes ist ein  Verfahren zur Darstellung eines     Dimethyl-          tetrahydro    -     benzaldehyds,    welches dadurch  gekennzeichnet ist, dass man     Isopren    und       Crotonaldehyd    kondensiert. Die neue Ver  bindung soll zur Herstellung von Farbstoffen,  pharmazeutischen Produkten und     Riechstoffen     verwendet werden.    <I>Beispiel:</I>    8 Gewichtsteile     Isopren    und 12 Gewichts  teile     Crotonaldehyd    werden im     Autoklaven     einige Stunden auf 150' erhitzt.

   Bei der  Destillation im Vakuum geht der entstandene         Dimethyltetrahydrobenzaldehyd    nach einem  aus     Crotonaldehyd    bestehenden Vorlauf nahezu  rein über und wird durch nochmalige Destil  lation ganz rein erhalten. Kp. 92-93  , 25 mm.



      Process for the preparation of a compound with a hydrogenated ring system. The subject of this additional patent is a process for the preparation of a dimethyl tetrahydro-benzaldehyde, which is characterized in that isoprene and crotonaldehyde are condensed. The new connection is intended to be used in the manufacture of dyes, pharmaceutical products and fragrances. <I> Example: </I> 8 parts by weight of isoprene and 12 parts by weight of crotonaldehyde are heated to 150 ° for a few hours in an autoclave.

   During the distillation in vacuo, the dimethyltetrahydrobenzaldehyde formed is almost pure after a first run consisting of crotonaldehyde and is obtained completely pure by repeated distillation. Bp 92-93, 25 mm.

 

Claims (1)

PATENTANSPRUCH: Verfahren zur Darstellung eines Dimethyl- tetrahydrobenzaldehyds, dadurch gekennzeich net, dass man Isopren mit Crotonaldehyd kon densiert. Der neue Aldehyd siedet bei 25 mm Druck bei 92-93 . PATENT CLAIM: Process for the preparation of a dimethyl tetrahydrobenzaldehyde, characterized in that isoprene is condensed with crotonaldehyde. The new aldehyde boils at 92-93 at 25 mm pressure.
CH143223D 1927-11-05 1928-11-02 Process for the preparation of a compound with a hydrogenated ring system. CH143223A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE143223X 1927-11-05
CH141523T 1930-08-15

Publications (1)

Publication Number Publication Date
CH143223A true CH143223A (en) 1930-10-31

Family

ID=25713744

Family Applications (1)

Application Number Title Priority Date Filing Date
CH143223D CH143223A (en) 1927-11-05 1928-11-02 Process for the preparation of a compound with a hydrogenated ring system.

Country Status (1)

Country Link
CH (1) CH143223A (en)

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