CH119123A - Process for the production of a new dye. - Google Patents

Process for the production of a new dye.

Info

Publication number
CH119123A
CH119123A CH119123DA CH119123A CH 119123 A CH119123 A CH 119123A CH 119123D A CH119123D A CH 119123DA CH 119123 A CH119123 A CH 119123A
Authority
CH
Switzerland
Prior art keywords
new dye
dye
production
mol
new
Prior art date
Application number
Other languages
German (de)
Inventor
Gesellschaft Fuer Chemis Basel
Original Assignee
Chem Ind Basel
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chem Ind Basel filed Critical Chem Ind Basel
Publication of CH119123A publication Critical patent/CH119123A/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B45/00Complex metal compounds of azo dyes
    • C09B45/02Preparation from dyes containing in o-position a hydroxy group and in o'-position hydroxy, alkoxy, carboxyl, amino or keto groups
    • C09B45/14Monoazo compounds
    • C09B45/16Monoazo compounds containing chromium

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Coloring (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Description

  

  Verfahren zur Herstellung eines neuen Farbstoffes.    Es     wurde    gefunden, dass man einen  neuen, wertvollen Farbstoff erhält, wenn  man den     Azofarbstoff,    den man durch Kup  peln von 1     Mol.        diazotiertem        5-Nitro-2-          amino-l-phenol    mit 1     Mol.        1-Naphthylamin-          5-sulfosäure    erhalten kann, mit     Chromfluo-          rid    behandelt. Der neue Farbstoff stellt ein  schwärzliches Pulver dar und färbt Wolle  aus schwefelsaurem Bade in grünen Tönen  mit vorzüglichen Echtheitseigenschaften.  



  <I>Beispiel:</I>  50 Teile- des     Natriumsalzes    des aus     di-          azotiertem        5-Nitro-2-amino-l-phenol    und     1-          Naphthylamin-5-sulfosäure    erhältlichen Farb  stoffes werden in 900 Teilen Wasser kochend  gelöst, mit 18 Teilen Chromoxyd in Form  von     Chromfluorid    versetzt und in Gegenwart    von Glaspulver längere Zeit rückfliessend  gekocht. Durch Eindampfen und     Aussalzen          wird    der neue chromhaltige Farbstoff ge  wonnen.



  Process for the production of a new dye. It has been found that a new, valuable dye is obtained if the azo dye, which is obtained by coupling 1 mol of diazotized 5-nitro-2-amino-1-phenol with 1 mol. 1-naphthylamine-5-sulfonic acid can be obtained, treated with chromium fluoride. The new dye is a blackish powder and dyes wool from sulfuric acid bath in green shades with excellent fastness properties.



  <I> Example: </I> 50 parts of the sodium salt of the dye obtainable from diacotized 5-nitro-2-amino-1-phenol and 1-naphthylamine-5-sulfonic acid are dissolved in 900 parts of boiling water with 18 parts of chromium oxide are added in the form of chromium fluoride and refluxed for a long time in the presence of glass powder. The new chromium-containing dye is obtained by evaporation and salting out.

 

Claims (1)

PATENTANSPRUCH: Verfahren zur Herstellung eines neuen Farbstoffes, dadurch gekennzeichnet, dass man den Azofarbstoff, den man durch Kup peln von 1 Mol. diazotiertem 5-Nitro-2- amino-l-phenol mit 1 Mol. 1-Naphthylamin- 5-sulfosäüre erhalten kann, mit Chromfluo- rid behandelt. Der neue Farbstoff stellt ein schwärzliches Pulver dar, färbt Wolle aus schwefelsaurem Bade in grünen Tönen mit vorzüglichen Echtheitseigenschaften. Claim: Process for the preparation of a new dye, characterized in that the azo dye obtained by coupling 1 mol of diazotized 5-nitro-2-amino-1-phenol with 1 mol. 1-naphthylamine-5-sulfonic acid can, treated with chromium fluoride. The new dye is a blackish powder, dyes wool from sulfuric acid bath in green shades with excellent fastness properties.
CH119123D 1925-02-14 1925-02-14 Process for the production of a new dye. CH119123A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH119123T 1925-02-14
CH115111T 1926-06-01

Publications (1)

Publication Number Publication Date
CH119123A true CH119123A (en) 1927-02-16

Family

ID=25708452

Family Applications (1)

Application Number Title Priority Date Filing Date
CH119123D CH119123A (en) 1925-02-14 1925-02-14 Process for the production of a new dye.

Country Status (1)

Country Link
CH (1) CH119123A (en)

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