CA3174159A1 - Processes and methods for production of crystallized metal sulfates - Google Patents

Processes and methods for production of crystallized metal sulfates Download PDF

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Publication number
CA3174159A1
CA3174159A1 CA3174159A CA3174159A CA3174159A1 CA 3174159 A1 CA3174159 A1 CA 3174159A1 CA 3174159 A CA3174159 A CA 3174159A CA 3174159 A CA3174159 A CA 3174159A CA 3174159 A1 CA3174159 A1 CA 3174159A1
Authority
CA
Canada
Prior art keywords
metal
stream
mother liquor
sulfate
plant
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CA3174159A
Other languages
English (en)
French (fr)
Inventor
Robert John FRASER
Matthew Wesley Jones
Andrea Winyen TRAC
Louiza Kahina HARKOUK
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hatch Ltd
Original Assignee
Hatch Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hatch Ltd filed Critical Hatch Ltd
Publication of CA3174159A1 publication Critical patent/CA3174159A1/en
Pending legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00—Sulfur; Compounds thereof
    • C01B17/96—Methods for the preparation of sulfates in general
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G1/00—Methods of preparing compounds of metals not covered by subclasses C01B, C01C, C01D, or C01F, in general
    • C01G1/10—Sulfates
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G3/00—Compounds of copper
    • C01G3/10—Sulfates
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G45/00—Compounds of manganese
    • C01G45/10—Sulfates
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G51/00—Compounds of cobalt
    • C01G51/10—Sulfates
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00—Compounds of nickel
    • C01G53/10—Sulfates
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B23/00—Obtaining nickel or cobalt
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B23/00—Obtaining nickel or cobalt
    • C22B23/04—Obtaining nickel or cobalt by wet processes
    • C22B23/0453—Treatment or purification of solutions, e.g. obtained by leaching
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/26—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/42—Treatment or purification of solutions, e.g. obtained by leaching by ion-exchange extraction
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B47/00—Obtaining manganese
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/50—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese
    • H01M4/505—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese of mixed oxides or hydroxides containing manganese for inserting or intercalating light metals, e.g. LiMn2O4 or LiMn2OxFy
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/52—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron
    • H01M4/525—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron of mixed oxides or hydroxides containing iron, cobalt or nickel for inserting or intercalating light metals, e.g. LiNiO2, LiCoO2 or LiCoOxFy
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M2004/026—Electrodes composed of, or comprising, active material characterised by the polarity
    • H01M2004/028—Positive electrodes
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Geology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Manufacture And Refinement Of Metals (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Electrolytic Production Of Metals (AREA)
  • Battery Electrode And Active Subsutance (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
CA3174159A 2020-11-12 2021-11-12 Processes and methods for production of crystallized metal sulfates Pending CA3174159A1 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US202063112891P 2020-11-12 2020-11-12
US63/112,891 2020-11-12
PCT/CA2021/051614 WO2022099422A1 (en) 2020-11-12 2021-11-12 Processes and methods for production of crystallized metal sulfates

Publications (1)

Publication Number Publication Date
CA3174159A1 true CA3174159A1 (en) 2022-05-19

Family

ID=81600741

Family Applications (1)

Application Number Title Priority Date Filing Date
CA3174159A Pending CA3174159A1 (en) 2020-11-12 2021-11-12 Processes and methods for production of crystallized metal sulfates

Country Status (11)

Country Link
US (2) US12281027B2 (https=)
EP (1) EP4244410A4 (https=)
JP (1) JP2023549374A (https=)
KR (1) KR20230110285A (https=)
CN (1) CN116648425A (https=)
AU (1) AU2021378828A1 (https=)
CA (1) CA3174159A1 (https=)
CL (1) CL2023001379A1 (https=)
CU (1) CU20230022A7 (https=)
PH (1) PH12023551304A1 (https=)
WO (1) WO2022099422A1 (https=)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20250313491A1 (en) * 2022-06-10 2025-10-09 Umicore Process for metal sulphidation

Family Cites Families (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR1597569A (https=) 1968-10-21 1970-06-29
FI58354C (fi) * 1977-11-28 1981-01-12 Outokumpu Oy Foerfarande foer behandling av raomaterial innehaollande arsenik och metall
US4157943A (en) * 1978-07-14 1979-06-12 The International Nickel Company, Inc. Composite electrode for electrolytic processes
US4314876A (en) 1980-03-17 1982-02-09 The Diversey Corporation Titanium etching solution
US4314976A (en) * 1980-07-18 1982-02-09 Southwire Company Purification of nickel sulfate
FI68422C (fi) 1983-10-21 1985-09-10 Outokumpu Oy Hydrometallurgiskt foerfarande foer behandling av klorider ochfluorider innehaollande raoaemnen av vaerdefulla metaller
US20020035486A1 (en) 2000-07-21 2002-03-21 Huyn Nam Q. Computerized clinical questionnaire with dynamically presented questions
JP5904459B2 (ja) * 2011-11-22 2016-04-13 住友金属鉱山株式会社 高純度硫酸ニッケルの製造方法
US10522884B2 (en) 2012-04-04 2019-12-31 Worcester Polytechnic Institute Method and apparatus for recycling lithium-ion batteries
JP2014024688A (ja) * 2012-07-25 2014-02-06 Sumitomo Metal Mining Co Ltd 硫酸ニッケルの晶析方法
JP6337708B2 (ja) * 2014-09-12 2018-06-06 住友金属鉱山株式会社 ニッケルスラッジからのニッケルの分離方法
JP6613954B2 (ja) * 2016-02-25 2019-12-04 住友金属鉱山株式会社 ニッケル水溶液の製造方法
CN108002408B (zh) 2016-10-31 2021-06-04 湖南金源新材料股份有限公司 电池废料制备硫酸镍、锰、锂、钴及四氧化三钴的方法
US10246343B2 (en) 2016-11-11 2019-04-02 Rocher Manganese, Inc. Processing of cobaltous sulpha/dithionate liquors derived from cobalt resource
CA3076688C (en) 2017-09-28 2021-01-19 Dominique Morin Lithium-ion batteries recycling process
WO2019090389A1 (en) * 2017-11-10 2019-05-16 Bhp Billiton Nickel West Pty Ltd Production of high purity nickel sulfate
KR102820068B1 (ko) 2018-09-27 2025-06-12 이고 리미티드 고순도 수화 황산 니켈의 제조 방법
CN109279667A (zh) 2018-10-09 2019-01-29 金川集团股份有限公司 一种以氧化镍为原料生产电池级硫酸镍的方法
CN109626448B (zh) * 2018-11-09 2021-07-06 浙江科菲科技股份有限公司 一种以废印花镍网生产高纯硫酸镍的方法
EP3670686A1 (en) 2018-12-21 2020-06-24 A.C.N. 630 589 507 Pty Ltd Battery recycling process
CN109734107A (zh) 2018-12-28 2019-05-10 池州西恩新材料科技有限公司 一种锂电池废正极材料的资源化回收方法
CN110203975A (zh) * 2019-04-25 2019-09-06 宁波行殊新能源科技有限公司 锰元素的浸出方法及电池级硫酸锰的制备方法
US10995014B1 (en) 2020-07-10 2021-05-04 Northvolt Ab Process for producing crystallized metal sulfates
JP2023551108A (ja) 2020-11-03 2023-12-07 ハッチ リミテッド 金属硫酸塩を結晶化するための処理方法

Also Published As

Publication number Publication date
PH12023551304A1 (en) 2023-11-20
EP4244410A1 (en) 2023-09-20
US20260103396A1 (en) 2026-04-16
CL2023001379A1 (es) 2023-11-17
AU2021378828A9 (en) 2024-08-08
EP4244410A4 (en) 2025-08-13
US20230048939A1 (en) 2023-02-16
WO2022099422A1 (en) 2022-05-19
CU20230022A7 (es) 2023-12-07
JP2023549374A (ja) 2023-11-24
CN116648425A (zh) 2023-08-25
KR20230110285A (ko) 2023-07-21
US12281027B2 (en) 2025-04-22
AU2021378828A1 (en) 2023-06-22

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