CA3122582A1 - Plasma processing of lithium transition metal oxides for lithium ion batteries - Google Patents

Plasma processing of lithium transition metal oxides for lithium ion batteries Download PDF

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Publication number
CA3122582A1
CA3122582A1 CA3122582A CA3122582A CA3122582A1 CA 3122582 A1 CA3122582 A1 CA 3122582A1 CA 3122582 A CA3122582 A CA 3122582A CA 3122582 A CA3122582 A CA 3122582A CA 3122582 A1 CA3122582 A1 CA 3122582A1
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CA
Canada
Prior art keywords
plasma processing
lithium
nmc
hours
lithium ion
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Pending
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CA3122582A
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English (en)
French (fr)
Inventor
Richard K. Holman
Kamal Hadidi
Gregory Wrobel
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6K Inc
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6K Inc
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Publication of CA3122582A1 publication Critical patent/CA3122582A1/en
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    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00Secondary cells; Manufacture thereof
    • H01M10/05Accumulators with non-aqueous electrolyte
    • H01M10/052Li-accumulators
    • H01M10/0525Rocking-chair batteries, i.e. batteries with lithium insertion or intercalation in both electrodes; Lithium-ion batteries
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00Compounds of nickel
    • C01G53/40Complex oxides containing nickel and at least one other metal element
    • C01G53/42Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2
    • C01G53/44Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2 containing manganese
    • C01G53/50Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2 containing manganese of the type (MnO2)n-, e.g. Li(NixMn1-x)O2 or Li(MyNixMn1-x-y)O2
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/04Processes of manufacture in general
    • H01M4/0438Processes of manufacture in general by electrochemical processing
    • H01M4/0469Electroforming a self-supporting electrode; Electroforming of powdered electrode material
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/04Processes of manufacture in general
    • H01M4/0471Processes of manufacture in general involving thermal treatment, e.g. firing, sintering, backing particulate active material, thermal decomposition, pyrolysis
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/13Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
    • H01M4/139Processes of manufacture
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/13Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
    • H01M4/139Processes of manufacture
    • H01M4/1391Processes of manufacture of electrodes based on mixed oxides or hydroxides, or on mixtures of oxides or hydroxides, e.g. LiCoOx
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/60Compounds characterised by their crystallite size
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/01Particle morphology depicted by an image
    • C01P2004/03Particle morphology depicted by an image obtained by SEM
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/30Particle morphology extending in three dimensions
    • C01P2004/32Spheres
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/51Particles with a specific particle size distribution
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/61Micrometer sized, i.e. from 1-100 micrometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/62Submicrometer sized, i.e. from 0.1-1 micrometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/12Surface area
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/40Electric properties
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M2004/026Electrodes composed of, or comprising, active material characterised by the polarity
    • H01M2004/028Positive electrodes
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10Energy storage using batteries

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Battery Electrode And Active Subsutance (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
CA3122582A 2018-12-20 2019-12-19 Plasma processing of lithium transition metal oxides for lithium ion batteries Pending CA3122582A1 (en)

Applications Claiming Priority (7)

Application Number Priority Date Filing Date Title
US201862782982P 2018-12-20 2018-12-20
US201862782845P 2018-12-20 2018-12-20
US201862782828P 2018-12-20 2018-12-20
US62/782,845 2018-12-20
US62/782,828 2018-12-20
US62/782,982 2018-12-20
PCT/US2019/067637 WO2020132343A1 (en) 2018-12-20 2019-12-19 Plasma processing of lithium transition metal oxides for lithium ion batteries

Publications (1)

Publication Number Publication Date
CA3122582A1 true CA3122582A1 (en) 2020-06-25

Family

ID=71097875

Family Applications (1)

Application Number Title Priority Date Filing Date
CA3122582A Pending CA3122582A1 (en) 2018-12-20 2019-12-19 Plasma processing of lithium transition metal oxides for lithium ion batteries

Country Status (9)

Country Link
US (1) US20200203706A1 (https=)
EP (1) EP3897963A4 (https=)
JP (1) JP2022514676A (https=)
KR (1) KR20210102427A (https=)
CN (1) CN113423497A (https=)
AU (1) AU2019405960A1 (https=)
CA (1) CA3122582A1 (https=)
TW (1) TW202031596A (https=)
WO (1) WO2020132343A1 (https=)

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US10987735B2 (en) 2015-12-16 2021-04-27 6K Inc. Spheroidal titanium metallic powders with custom microstructures
HUE065423T2 (hu) 2015-12-16 2024-05-28 6K Inc Eljárás szferoidális dehidrogénezett titánötvözet részecskék elõállítására
AU2019290663B2 (en) 2018-06-19 2023-05-04 6K Inc. Process for producing spheroidized powder from feedstock materials
CN112909238B (zh) 2018-12-29 2022-04-22 宁德时代新能源科技股份有限公司 正极活性材料、正极极片及电化学储能装置
CN110233247B (zh) * 2018-12-29 2021-01-01 宁德时代新能源科技股份有限公司 正极活性材料、正极极片及电化学储能装置
KR20240036705A (ko) 2019-04-30 2024-03-20 6케이 인크. 리튬 란타넘 지르코늄 산화물(llzo) 분말
CA3134573A1 (en) 2019-04-30 2020-11-05 Sunil Bhalchandra BADWE Mechanically alloyed powder feedstock
US12183912B2 (en) * 2019-05-09 2024-12-31 A123 Systems Llc Methods and systems for dry surface doping of cathode materials
CN112786949B (zh) * 2019-11-06 2022-06-07 宁德时代新能源科技股份有限公司 二次电池及含有该二次电池的电池模组、电池包、装置
WO2021118762A1 (en) 2019-11-18 2021-06-17 6K Inc. Unique feedstocks for spherical powders and methods of manufacturing
US11590568B2 (en) 2019-12-19 2023-02-28 6K Inc. Process for producing spheroidized powder from feedstock materials
US12469838B2 (en) 2020-05-03 2025-11-11 Sparkz Inc. Systems and methods involving use of nitrogen-containing plasma to treat lithium iron phosphate cathodes
US12015142B2 (en) * 2020-05-03 2024-06-18 Venkatraman Prabhakar Methods involving use of nitrogen-containing plasma to treat liquid electrolyte lithium-ion cathode materials
AU2021297476A1 (en) 2020-06-25 2022-12-15 6K Inc. Microcomposite alloy structure
AU2021349358A1 (en) 2020-09-24 2023-02-09 6K Inc. Systems, devices, and methods for starting plasma
EP4237174A1 (en) 2020-10-30 2023-09-06 6K Inc. Systems and methods for synthesis of spheroidized metal powders
EP4275239A4 (en) * 2021-01-11 2024-12-18 6K Inc. METHODS AND SYSTEMS FOR RECLAIMING LI-ION CATHODE MATERIALS USING MICROWAVE PLASMA TREATMENT
EP4281215A4 (en) * 2021-01-19 2025-04-30 6K Inc. SINGLE CRYSTAL CATHODE MATERIALS USING MICROWAVE PLASMA PROCESSING
AU2022246797A1 (en) 2021-03-31 2023-10-05 6K Inc. Systems and methods for additive manufacturing of metal nitride ceramics
WO2022269429A1 (en) * 2021-06-25 2022-12-29 Advanced Potash Technologies, Ltd. Multi-step methods of making a high temperature multi-phase material and related materials, compositions and methods of use
WO2023229928A1 (en) 2022-05-23 2023-11-30 6K Inc. Microwave plasma apparatus and methods for processing materials using an interior liner
US12040162B2 (en) 2022-06-09 2024-07-16 6K Inc. Plasma apparatus and methods for processing feed material utilizing an upstream swirl module and composite gas flows
CN115394976B (zh) * 2022-08-04 2026-03-10 广东邦普循环科技有限公司 一种正极材料的制备方法及其应用
WO2024044498A1 (en) 2022-08-25 2024-02-29 6K Inc. Plasma apparatus and methods for processing feed material utilizing a powder ingress preventor (pip)
EP4608776A1 (en) * 2022-10-28 2025-09-03 The Regents of the University of California Solid-state microwave route to cation-disordered rocksalt oxide and oxyfluoride cathodes
US12195338B2 (en) 2022-12-15 2025-01-14 6K Inc. Systems, methods, and device for pyrolysis of methane in a microwave plasma for hydrogen and structured carbon powder production

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US838072A (en) * 1905-04-19 1906-12-11 Benner Mfg Company Baby-jumper.
JPH10172564A (ja) * 1996-12-04 1998-06-26 Mitsubishi Electric Corp 活物質及びその製造方法並びにその活物質を用いたリチウムイオン二次電池
JP2007238402A (ja) * 2006-03-10 2007-09-20 Chugai Ro Co Ltd 粉体製造装置および粉体製造方法
CN102782176B (zh) * 2009-08-24 2014-10-15 应用材料公司 通过热喷涂原位沉积电池活性锂材料
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Also Published As

Publication number Publication date
TW202031596A (zh) 2020-09-01
EP3897963A4 (en) 2022-09-14
KR20210102427A (ko) 2021-08-19
WO2020132343A1 (en) 2020-06-25
EP3897963A1 (en) 2021-10-27
JP2022514676A (ja) 2022-02-14
AU2019405960A1 (en) 2021-06-24
US20200203706A1 (en) 2020-06-25
CN113423497A (zh) 2021-09-21

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