CA3068161A1 - A mechanochemical process to produce exfoliated nanoparticles - Google Patents

A mechanochemical process to produce exfoliated nanoparticles Download PDF

Info

Publication number
CA3068161A1
CA3068161A1 CA3068161A CA3068161A CA3068161A1 CA 3068161 A1 CA3068161 A1 CA 3068161A1 CA 3068161 A CA3068161 A CA 3068161A CA 3068161 A CA3068161 A CA 3068161A CA 3068161 A1 CA3068161 A1 CA 3068161A1
Authority
CA
Canada
Prior art keywords
nanoparticles
hdpe
gnp
mechanochemical process
mechanochemical
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CA3068161A
Other languages
English (en)
French (fr)
Inventor
Apoorva SINHA
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Carbon Upcycling Technologies Inc
Original Assignee
Carbon Upcycling Technologies Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Carbon Upcycling Technologies Inc filed Critical Carbon Upcycling Technologies Inc
Publication of CA3068161A1 publication Critical patent/CA3068161A1/en
Pending legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00Carbon; Compounds thereof
    • C01B32/15Nano-sized carbon materials
    • C01B32/182Graphene
    • C01B32/198Graphene oxide
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G49/00Compounds of iron
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00Carbon; Compounds thereof
    • C01B32/15Nano-sized carbon materials
    • C01B32/182Graphene
    • C01B32/184Preparation
    • C01B32/19Preparation by exfoliation
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00Carbon; Compounds thereof
    • C01B32/15Nano-sized carbon materials
    • C01B32/182Graphene
    • C01B32/184Preparation
    • C01B32/19Preparation by exfoliation
    • C01B32/192Preparation by exfoliation starting from graphitic oxides
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00Use of inorganic substances as compounding ingredients
    • C08K3/02Elements
    • C08K3/04Carbon
    • C08K3/042Graphene or derivatives, e.g. graphene oxides
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2204/00Structure or properties of graphene
    • C01B2204/20Graphene characterized by its properties
    • C01B2204/32Size or surface area
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/80Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
    • C01P2002/88Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by thermal analysis data, e.g. TGA, DTA, DSC
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/20Particle morphology extending in two dimensions, e.g. plate-like
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/51Particles with a specific particle size distribution
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/51Particles with a specific particle size distribution
    • C01P2004/53Particles with a specific particle size distribution bimodal size distribution
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/61Micrometer sized, i.e. from 1-100 micrometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/62Submicrometer sized, i.e. from 0.1-1 micrometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/64Nanometer sized, i.e. from 1-100 nanometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/12Surface area
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00Specific properties of additives
    • C08K2201/002Physical properties
    • C08K2201/005Additives being defined by their particle size in general
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00Specific properties of additives
    • C08K2201/002Physical properties
    • C08K2201/006Additives being defined by their surface area
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00Specific properties of additives
    • C08K2201/011Nanostructured additives

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Nanotechnology (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Carbon And Carbon Compounds (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
CA3068161A 2017-07-13 2018-07-12 A mechanochemical process to produce exfoliated nanoparticles Pending CA3068161A1 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP17181233 2017-07-13
EP17181233.2 2017-07-13
PCT/IB2018/055156 WO2019012474A1 (en) 2017-07-13 2018-07-12 CHEMICAL METHOD FOR PRODUCING EXFOLIATED NANOPARTICLES

Publications (1)

Publication Number Publication Date
CA3068161A1 true CA3068161A1 (en) 2019-01-17

Family

ID=59409159

Family Applications (1)

Application Number Title Priority Date Filing Date
CA3068161A Pending CA3068161A1 (en) 2017-07-13 2018-07-12 A mechanochemical process to produce exfoliated nanoparticles

Country Status (6)

Country Link
US (4) US11772976B2 (enExample)
EP (3) EP3652109A4 (enExample)
JP (1) JP7372239B2 (enExample)
CN (1) CN111148718B (enExample)
CA (1) CA3068161A1 (enExample)
WO (1) WO2019012474A1 (enExample)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2025074250A1 (en) * 2023-10-06 2025-04-10 Carbon Upcycling Technologies Inc. Low energy mechanochemical carbon sequestration of solid feedstocks

Families Citing this family (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10468674B2 (en) 2018-01-09 2019-11-05 South Dakota Board Of Regents Layered high capacity electrodes
EP3997047A4 (en) 2019-07-08 2023-08-02 Alter Biota Inc. PREPARATION OF HYDRATED GRAPHENE OXIDE FOR USE AS A CONCRETE ADMIXTURE
JP2021031328A (ja) * 2019-08-22 2021-03-01 高彰 岡本 グラフェン前駆体の製造システム、グラフェン前駆体の製造方法およびグラフェン前駆体
US20210104720A1 (en) * 2019-10-08 2021-04-08 South Dakota Board Of Regents Electrode materials comprising cold spray doped compositions
JP7410165B2 (ja) * 2019-10-29 2024-01-09 株式会社クレハ 炭素量子ドット含有組成物、およびその製造方法
WO2021084825A1 (ja) * 2019-10-29 2021-05-06 株式会社クレハ 炭素量子ドット含有組成物、およびその製造方法
CN118145918A (zh) * 2019-11-05 2024-06-07 碳循环技术有限公司 包含机械化学羧化矿物填料和水泥和/或沥青粘合剂的组合物
WO2021087605A1 (en) * 2019-11-05 2021-05-14 Carbon Upcycling Technologies Inc. A mechanically carboxylated fly ash, methods of its production and uses thereof
US20230034630A1 (en) * 2021-07-23 2023-02-02 Chromaflo Technologies Corporation Graphene dispersion and functionalization
ES2933047B2 (es) * 2021-07-26 2023-09-14 Fundacion Instituto De Investig Marques De Valdecilla Material compuesto de poliacrilonitrilo y nanoplaquetas de grafeno, procedimiento de obtención y uso como sustrato de cultivos in vitro de células cancerosas
WO2023200905A1 (en) 2022-04-12 2023-10-19 Carbonbuilt Process for production of hydraulic-carbonating binder systems through mechanochemical activation of minerals
US20230399517A1 (en) 2022-06-13 2023-12-14 Carbon Upcycling Technologies Inc. Mechanochemically carbonated magnesium silicate, methods of its production and uses thereof
GB202208582D0 (en) 2022-06-13 2022-07-27 Groundtruth Global Ltd A mechanochemically carbonated magnesium silicate, methods of its production and uses thereof
PL4410759T3 (pl) * 2022-08-17 2025-09-15 Carbon Upcycling Technologies Inc. Mechanochemicznie karbonizowana glina, sposoby jej wytwarzania i jej zastosowania
ES2994883T3 (en) * 2022-08-17 2025-02-03 Carbon Upcycling Tech Inc A mechanochemically carbonated natural pozzolan, methods of its production and uses thereof
PL4324803T3 (pl) * 2022-08-17 2024-11-04 Carbon Upcycling Technologies Inc. Mechanochemicznie karbonizowany żużel, sposób jego wytwarzania i jego zastosowania

Family Cites Families (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1579622A (en) * 1925-05-28 1926-04-06 Edna T Rasmussen Vanity cane
IL103641A (en) * 1992-11-04 1996-11-14 Environmental Systems Ltd Expandable graphite compositions for absorption of liquids and method for the manufacture thereof
US6287694B1 (en) 1998-03-13 2001-09-11 Superior Graphite Co. Method for expanding lamellar forms of graphite and resultant product
CN100337742C (zh) * 2003-07-31 2007-09-19 北京化工大学 一种经插层前体制备的高分散铜基氧化催化剂及制备方法
US20060252871A1 (en) * 2005-05-04 2006-11-09 Baird Donald G Process for increasing the exfoliation and dispersion of nanoparticles into polymeric matrices using supercritical carbon dioxide
US7785492B1 (en) 2006-09-26 2010-08-31 Nanotek Instruments, Inc. Mass production of nano-scaled platelets and products
BRPI0705815B1 (pt) * 2007-10-25 2018-03-20 Braskem S.A Processo de polimerização de nanopartículas de carga mineral para obtenção de nanocompósitos poliméricos
US9096736B2 (en) * 2010-06-07 2015-08-04 Kabushiki Kaisha Toyota Chuo Kenkyusho Fine graphite particles, graphite particle-dispersed liquid containing the same, and method for producing fine graphite particles
SG186811A1 (en) * 2010-06-25 2013-02-28 Univ Singapore Methods of forming graphene by graphite exfoliation
EP2647600A4 (en) 2010-11-29 2015-10-28 Sekisui Chemical Co Ltd CARBON MATERIAL, PROCESS FOR PRODUCING CARBON MATERIAL, METHOD FOR PRODUCING GRAPHITE IN SEWERS, AND GRAPHITE IN FLAKES
EA201301031A1 (ru) * 2011-03-15 2014-06-30 ПИРЛЕСС УОРЛДУАЙД, ЛЛСи Простой синтез графена, производных графена и абразивных наночастиц и их различные применения, в том числе в качестве трибологическиполезных присадок к смазочным маслам
KR101910924B1 (ko) 2013-03-08 2018-10-23 유니버시티 오브 센트럴 플로리다 리서치 파운데이션, 인코포레이티드 산업용 대규모 산화 그래핀 제조
US20140272199A1 (en) 2013-03-14 2014-09-18 Yi-Jun Lin Ultrasonic spray coating of conducting and transparent films from combined graphene and conductive nano filaments
GB201304770D0 (en) * 2013-03-15 2013-05-01 Provost Fellows Foundation Scholars And The Other Members Of Board Of A scalable process for producing exfoliated defect-free, non-oxidised 2-dimens ional materials in large quantities
US10886526B2 (en) * 2013-06-13 2021-01-05 Zenlabs Energy, Inc. Silicon-silicon oxide-carbon composites for lithium battery electrodes and methods for forming the composites
ES2534575B1 (es) 2013-09-24 2016-01-14 Consejo Superior De Investigaciones Científicas (Csic) Exfoliación de grafito con disolventes eutécticos profundos
CN103706337B (zh) * 2013-12-30 2015-10-07 成都纺织高等专科学校 一种除甲醛纳米混合物及其制备方法
JPWO2015125740A1 (ja) 2014-02-18 2017-03-30 積水化学工業株式会社 薄片化黒鉛の製造方法、薄片化黒鉛及び薄片化黒鉛−樹脂複合材料
KR101576896B1 (ko) * 2014-04-07 2015-12-14 인하대학교 산학협력단 산화철(β-FeOOH)-그래핀 복합체의 제조방법 및 이에 의해 제조되는 산화철(β-FeOOH)-그래핀 복합체
CN106687512B (zh) * 2014-07-17 2019-02-15 凯诺斯私人有限公司 聚合物树脂组合物和用所述组合物形成的制品
WO2016018995A1 (en) * 2014-07-30 2016-02-04 Rutgers, The State University Of New Jersey Graphene-reinforced polymer matrix composites
CN104763427B (zh) * 2015-02-12 2016-11-02 太原理工大学 一种超临界co2预裂煤矿厚硬难垮顶板的方法
ITUB20159348A1 (it) * 2015-12-21 2017-06-21 Univ Degli Studi Di Roma La Sapienza 00185 Roma / It PRODUZIONE DI NANOSTRUTTURE COMPOSITE A BASE GRAFENE OTTENUTE MEDIANTE CRESCITA IN SOSPENSIONE DI NANOROD E MICROROD DI ZnO SU FIOCCHI DI GNP NON SUPPORTATI
CN107277960B (zh) * 2017-05-24 2020-09-11 方大炭素新材料科技股份有限公司 一种降低石墨电极/接头电阻率的方法

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2025074250A1 (en) * 2023-10-06 2025-04-10 Carbon Upcycling Technologies Inc. Low energy mechanochemical carbon sequestration of solid feedstocks

Also Published As

Publication number Publication date
WO2019012474A1 (en) 2019-01-17
EP4049976A1 (en) 2022-08-31
US20230339761A1 (en) 2023-10-26
EP3652109A4 (en) 2021-05-05
EP4282819A3 (en) 2024-02-28
CN111148718A (zh) 2020-05-12
US20210147239A1 (en) 2021-05-20
JP7372239B2 (ja) 2023-10-31
US12234152B2 (en) 2025-02-25
EP3652109A1 (en) 2020-05-20
EP4282819A2 (en) 2023-11-29
US20250154009A1 (en) 2025-05-15
US20230312350A1 (en) 2023-10-05
CN111148718B (zh) 2023-06-09
US11772976B2 (en) 2023-10-03
JP2020527534A (ja) 2020-09-10

Similar Documents

Publication Publication Date Title
US12234152B2 (en) Mechanochemical process to produce exfoliated nanoparticles
Istrate et al. Reinforcement in melt-processed polymer–graphene composites at extremely low graphene loading level
Lin et al. Evaluation of the thermal, mechanical and dynamic mechanical characteristics of modified graphite nanoplatelets and graphene oxide high-density polyethylene composites
US7906053B1 (en) Polymer-graphite nanocomposites via solid-state shear pulverization
Verma A perspective on the potential material candidate for railway sector applications: PVA based functionalized graphene reinforced composite
FR2916364A1 (fr) Procede de preparation de pre-composites a base de nanotubes notamment de carbone
CA2963214C (fr) Preparation d'un melange-maitre a base de soufre et de nanocharges carbonees, le melange-maitre obtenu et ses utilisations
Nacas et al. Nano boron nitride/polyurethane adhesives in flexible laminated food packaging: peeling resistance and permeability properties
Suresh et al. A review on the effect of various nano fillers on the mechanical properties and thermal stability of chloroprene rubber composites
Rahmanian et al. Polyethylene nanocomposites with carbon nanofillers: similarities and differences and new insight on cavitation in tensile drawing
JP5432974B2 (ja) 炭素繊維複合材料の製造方法及び炭素繊維複合材料
Razak et al. GRAPHENE NANOPLATELETS-FILLED NR/EPDM RUBBER BLEND: EFFECTS OF GNPS LOADING ON BLEND PROCESS ABILITY, MECHANICAL PROPERTIES AND FRACTURE MORPHOLOGY.
Sriprachuabwong et al. Electrolytically exfoliated graphene–polylactide‐based bioplastic with high elastic performance
Afsharpour et al. Nanofillers in additives for rubbers
JP5735442B2 (ja) 炭素ナノ物質でコーティングされた天然纎維補強材と高分子とを含むナノバイオ複合体
Pantano Carbon nanotube based composites: processing, properties, modelling and application
Bureewong et al. Mechanical and thermal properties of NR/XSBR composite reinforced with rice husk silica
Mural et al. Processing nanocomposites based on commodity polymers
Abbasi et al. Effect of aspect ratio, surface modification and compatibilizer on the mechanical and thermal properties of ldpe-mwcnt nanocomposites
Mardlin Graphene Nanoplatelets Produced by Thermomechanical Exfoliation of Graphite, and their use in Polyamide Composites
Salleh et al. The influences of melt-compounding parameters on the tensile properties of low filler loading of untreated-MWCNTs-polypropylene (PP) nanocomposites
Saji et al. Synthesis, Mechanical Properties and Thermal Stability of Polydimethylsiloxane Nanocomposites.
Colemana Reinforcement in melt-processed polymer-graphene composites at extremely low graphene loading level
Mwafy et al. Fabrication and Characterization of Carbon Nanotubes/PMMA Nanocomposite
Benchikh et al. Cellulose nanocrystals/polyaniline particles’s dispersion in polypropylene nanocomposites

Legal Events

Date Code Title Description
EEER Examination request

Effective date: 20220920

EEER Examination request

Effective date: 20220920

EEER Examination request

Effective date: 20220920

EEER Examination request

Effective date: 20220920

EEER Examination request

Effective date: 20220920

EEER Examination request

Effective date: 20220920