CA3011743C - Methods of deoxygenating metals having oxygen dissolved therein in a solid solution - Google Patents
Methods of deoxygenating metals having oxygen dissolved therein in a solid solution Download PDFInfo
- Publication number
- CA3011743C CA3011743C CA3011743A CA3011743A CA3011743C CA 3011743 C CA3011743 C CA 3011743C CA 3011743 A CA3011743 A CA 3011743A CA 3011743 A CA3011743 A CA 3011743A CA 3011743 C CA3011743 C CA 3011743C
- Authority
- CA
- Canada
- Prior art keywords
- metal
- deoxygenation
- powder
- oxygen
- deoxygenated
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F9/00—Making metallic powder or suspensions thereof
- B22F9/16—Making metallic powder or suspensions thereof using chemical processes
- B22F9/18—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds
- B22F9/20—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds starting from solid metal compounds
- B22F9/22—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds starting from solid metal compounds using gaseous reductors
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
- B22F1/06—Metallic powder characterised by the shape of the particles
- B22F1/065—Spherical particles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
- B22F1/14—Treatment of metallic powder
- B22F1/142—Thermal or thermo-mechanical treatment
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
- B22F1/14—Treatment of metallic powder
- B22F1/145—Chemical treatment, e.g. passivation or decarburisation
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- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/10—Obtaining titanium, zirconium or hafnium
- C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
- C22B34/1263—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction
- C22B34/1268—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction using alkali or alkaline-earth metals or amalgams
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/10—Obtaining titanium, zirconium or hafnium
- C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
- C22B34/1295—Refining, melting, remelting, working up of titanium
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B9/00—General processes of refining or remelting of metals; Apparatus for electroslag or arc remelting of metals
- C22B9/14—Refining in the solid state
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22F—CHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
- C22F1/00—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
- C22F1/16—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of other metals or alloys based thereon
- C22F1/18—High-melting or refractory metals or alloys based thereon
- C22F1/183—High-melting or refractory metals or alloys based thereon of titanium or alloys based thereon
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F2301/00—Metallic composition of the powder or its coating
- B22F2301/20—Refractory metals
- B22F2301/205—Titanium, zirconium or hafnium
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F2998/00—Supplementary information concerning processes or compositions relating to powder metallurgy
- B22F2998/10—Processes characterised by the sequence of their steps
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F2999/00—Aspects linked to processes or compositions used in powder metallurgy
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C14/00—Alloys based on titanium
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/25—Process efficiency
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Metallurgy (AREA)
- Mechanical Engineering (AREA)
- Materials Engineering (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Manufacturing & Machinery (AREA)
- Geology (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Crystallography & Structural Chemistry (AREA)
- Nanotechnology (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Powder Metallurgy (AREA)
- Manufacture Of Metal Powder And Suspensions Thereof (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
Applications Claiming Priority (5)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US201662293667P | 2016-02-10 | 2016-02-10 | |
US62/293,667 | 2016-02-10 | ||
US15/216,549 US9669464B1 (en) | 2016-02-10 | 2016-07-21 | Methods of deoxygenating metals having oxygen dissolved therein in a solid solution |
US15/216,549 | 2016-07-21 | ||
PCT/US2017/017503 WO2017139665A1 (en) | 2016-02-10 | 2017-02-10 | Methods of deoxygenating metals oxygen dissolved therein in a solid solution |
Publications (2)
Publication Number | Publication Date |
---|---|
CA3011743A1 CA3011743A1 (en) | 2017-08-17 |
CA3011743C true CA3011743C (en) | 2019-11-05 |
Family
ID=58778382
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CA3011743A Active CA3011743C (en) | 2016-02-10 | 2017-02-10 | Methods of deoxygenating metals having oxygen dissolved therein in a solid solution |
Country Status (10)
Country | Link |
---|---|
US (1) | US9669464B1 (zh) |
EP (1) | EP3414035B1 (zh) |
JP (1) | JP6522249B2 (zh) |
KR (1) | KR101965121B1 (zh) |
CN (1) | CN108602120B (zh) |
AU (1) | AU2017217970B2 (zh) |
CA (1) | CA3011743C (zh) |
DK (1) | DK3414035T3 (zh) |
ES (1) | ES2925385T3 (zh) |
WO (1) | WO2017139665A1 (zh) |
Families Citing this family (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US11130175B2 (en) * | 2018-01-18 | 2021-09-28 | The Boeing Company | Spherical metallic powder blends and methods for manufacturing the same |
WO2020091854A1 (en) * | 2018-10-31 | 2020-05-07 | Arconic Inc. | Method and system for processing metal powders, and articles produced therefrom |
CN110484737B (zh) * | 2019-10-08 | 2021-05-18 | 攀枝花学院 | 用高氧钛回收料制备钛锭的方法 |
CN110616340B (zh) * | 2019-10-08 | 2021-06-11 | 攀枝花学院 | 用高氧钛回收料氢化脱氢制备钛锭的方法 |
CN111097915B (zh) * | 2020-02-24 | 2021-05-14 | 北京科技大学 | 一种制备低氧高质量氢化脱氢钛粉的方法 |
CN112247139A (zh) * | 2020-09-25 | 2021-01-22 | 郑州大学 | 一种降低细钛粉氧含量的方法 |
CN112341208B (zh) * | 2021-01-07 | 2021-07-09 | 矿冶科技集团有限公司 | 失氧型氧化物陶瓷球形粉末的制备方法、失氧型氧化物陶瓷球形粉末和燃料电池电解质薄膜 |
CN113000833A (zh) * | 2021-02-23 | 2021-06-22 | 郑州大学 | 用于增材制造的Ti-6Al-4V合金球形粉体及其制备方法 |
KR102300837B1 (ko) * | 2021-04-15 | 2021-09-13 | 한국지질자원연구원 | 마그네슘을 이용한 오프그레이드 타이타늄 스폰지의 탈산법 |
CN113718131A (zh) * | 2021-09-03 | 2021-11-30 | 立中四通轻合金集团股份有限公司 | 一种钛钼中间合金短流程低成本制备方法 |
CN114015954B (zh) * | 2021-09-08 | 2022-07-01 | 先导薄膜材料有限公司 | 一种降低铝合金中氧含量的方法 |
KR102687047B1 (ko) * | 2021-12-27 | 2024-07-23 | 삼화스틸 주식회사 | 구형 금속분말의 제조방법 |
KR20230133491A (ko) * | 2022-03-11 | 2023-09-19 | 전북대학교산학협력단 | 타이타늄계 분말 제조방법 |
CN116237517A (zh) * | 2023-01-12 | 2023-06-09 | 东北大学 | 一种微米金属颗粒球化的方法 |
Family Cites Families (39)
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US2205854A (en) | 1937-07-10 | 1940-06-25 | Kroll Wilhelm | Method for manufacturing titanium and alloys thereof |
US2427338A (en) | 1945-03-26 | 1947-09-16 | Metal Hydrides Inc | Production of titanium hydride |
US2773787A (en) | 1952-12-20 | 1956-12-11 | Du Pont | Production of group iv-a metals |
US2804375A (en) | 1953-05-28 | 1957-08-27 | Nat Distillers Chem Corp | Cyclic process for the beneficiation of titania ores and slags |
US2850379A (en) | 1954-03-15 | 1958-09-02 | Ethyl Corp | Process for production of refractory metals |
DE1016026B (de) | 1956-01-26 | 1957-09-19 | Degussa | Verfahren zur Herstellung von Metallen durch Reduktion |
BE551090A (zh) | 1956-02-17 | |||
US2984560A (en) | 1960-02-08 | 1961-05-16 | Du Pont | Production of high-purity, ductile titanium powder |
US3140170A (en) * | 1962-11-23 | 1964-07-07 | Thomas A Henrie | Magnesium reduction of titanium oxides in a hydrogen atmosphere |
US3472648A (en) | 1968-01-26 | 1969-10-14 | Pullman Inc | Treatment of titanium oxides |
FR2052082A5 (zh) | 1969-07-11 | 1971-04-09 | Commissariat Energie Atomique | |
US3903239A (en) | 1973-02-07 | 1975-09-02 | Ontario Research Foundation | Recovery of titanium dioxide from ores |
US4923531A (en) | 1988-09-23 | 1990-05-08 | Rmi Company | Deoxidation of titanium and similar metals using a deoxidant in a molten metal carrier |
JP2651945B2 (ja) * | 1990-02-20 | 1997-09-10 | 株式会社ジャパンエナジー | チタンの脱酸方法 |
US5503655A (en) | 1994-02-23 | 1996-04-02 | Orbit Technologies, Inc. | Low cost titanium production |
US5460642A (en) | 1994-03-21 | 1995-10-24 | Teledyne Industries, Inc. | Aerosol reduction process for metal halides |
JP3391461B2 (ja) | 1994-08-01 | 2003-03-31 | インターナショナル・タイテイニアム・パウダー・リミテッド・ライアビリティ・カンパニー | 元素材料の製造方法 |
US5830420A (en) | 1995-11-21 | 1998-11-03 | Qit-Fer Et Titane Inc. | Method to upgrade titania slag and resulting product |
US6264719B1 (en) | 1997-08-19 | 2001-07-24 | Titanox Developments Limited | Titanium alloy based dispersion-strengthened composites |
US6231636B1 (en) | 1998-02-06 | 2001-05-15 | Idaho Research Foundation, Inc. | Mechanochemical processing for metals and metal alloys |
US6152982A (en) | 1998-02-13 | 2000-11-28 | Idaho Research Foundation, Inc. | Reduction of metal oxides through mechanochemical processing |
NZ520369A (en) | 2002-07-22 | 2005-03-24 | Titanox Dev Ltd | A separation process for producing titanium rich powder from metal matrix composite |
US6824585B2 (en) | 2002-12-03 | 2004-11-30 | Adrian Joseph | Low cost high speed titanium and its alloy production |
US7410562B2 (en) | 2003-08-20 | 2008-08-12 | Materials & Electrochemical Research Corp. | Thermal and electrochemical process for metal production |
WO2006042360A1 (en) * | 2004-10-20 | 2006-04-27 | Commonwealth Scientific And Industrial Research Organisation | Low temperature industrial process |
DE602006007780D1 (de) * | 2005-10-21 | 2009-08-27 | Sulzer Metco Us Inc | Verfahren zur Herstellung hochreinen fliessfähigen Metalloxidpulvers durch Plasmaschmelzen |
NZ548675A (en) | 2006-07-20 | 2008-12-24 | Titanox Dev Ltd | A process for producing titanium metal alloy powder from titanium dioxide and aluminium |
JP5427452B2 (ja) | 2008-03-31 | 2014-02-26 | 日立金属株式会社 | 金属チタンの製造方法 |
WO2010036131A1 (en) | 2008-09-25 | 2010-04-01 | Titanox Development Limited | Production of titanium alloys in particulate form via solid state reduction process |
US8007562B2 (en) | 2008-12-29 | 2011-08-30 | Adma Products, Inc. | Semi-continuous magnesium-hydrogen reduction process for manufacturing of hydrogenated, purified titanium powder |
JP6034550B2 (ja) | 2009-01-20 | 2016-11-30 | 株式会社Ti | 水素発生触媒、水素発生方法、水素発生装置 |
CN102428195B (zh) | 2009-05-29 | 2014-12-10 | 日立金属株式会社 | 金属钛的制造方法 |
US8388727B2 (en) | 2010-01-11 | 2013-03-05 | Adma Products, Inc. | Continuous and semi-continuous process of manufacturing titanium hydride using titanium chlorides of different valency |
US20130220211A1 (en) * | 2012-02-29 | 2013-08-29 | Indrajit Dutta | Crystal to crystal oxygen extraction |
US9067264B2 (en) | 2012-05-24 | 2015-06-30 | Vladimir S. Moxson | Method of manufacturing pure titanium hydride powder and alloyed titanium hydride powders by combined hydrogen-magnesium reduction of metal halides |
KR101259434B1 (ko) * | 2012-07-27 | 2013-04-30 | 한국지질자원연구원 | 티타늄 합금 스크랩으로부터 저산소 합금 분말의 제조 방법 |
GB201309173D0 (en) * | 2013-05-21 | 2013-07-03 | Roberts Mark P | Novel process and product |
EP3036195B1 (en) | 2013-08-19 | 2020-07-01 | University Of Utah Research Foundation | Producing a titanium product |
WO2015175726A1 (en) * | 2014-05-13 | 2015-11-19 | University Of Utah Research Foundation | Production of substantially spherical metal powers |
-
2016
- 2016-07-21 US US15/216,549 patent/US9669464B1/en active Active
-
2017
- 2017-02-10 KR KR1020187025784A patent/KR101965121B1/ko active IP Right Grant
- 2017-02-10 DK DK17750888.4T patent/DK3414035T3/da active
- 2017-02-10 CA CA3011743A patent/CA3011743C/en active Active
- 2017-02-10 AU AU2017217970A patent/AU2017217970B2/en active Active
- 2017-02-10 JP JP2018537516A patent/JP6522249B2/ja active Active
- 2017-02-10 EP EP17750888.4A patent/EP3414035B1/en active Active
- 2017-02-10 CN CN201780010034.0A patent/CN108602120B/zh active Active
- 2017-02-10 WO PCT/US2017/017503 patent/WO2017139665A1/en active Application Filing
- 2017-02-10 ES ES17750888T patent/ES2925385T3/es active Active
Also Published As
Publication number | Publication date |
---|---|
AU2017217970B2 (en) | 2018-11-22 |
US9669464B1 (en) | 2017-06-06 |
ES2925385T3 (es) | 2022-10-17 |
EP3414035A4 (en) | 2019-07-24 |
KR20180102691A (ko) | 2018-09-17 |
EP3414035A1 (en) | 2018-12-19 |
WO2017139665A1 (en) | 2017-08-17 |
KR101965121B1 (ko) | 2019-08-13 |
CA3011743A1 (en) | 2017-08-17 |
JP2019510873A (ja) | 2019-04-18 |
DK3414035T3 (da) | 2022-07-11 |
CN108602120A (zh) | 2018-09-28 |
JP6522249B2 (ja) | 2019-05-29 |
CN108602120B (zh) | 2021-03-09 |
EP3414035B1 (en) | 2022-04-06 |
AU2017217970A1 (en) | 2018-08-09 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
EEER | Examination request |
Effective date: 20180717 |