CA2783604C - Process for epoxidation start-up - Google Patents

Process for epoxidation start-up Download PDF

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Publication number
CA2783604C
CA2783604C CA2783604A CA2783604A CA2783604C CA 2783604 C CA2783604 C CA 2783604C CA 2783604 A CA2783604 A CA 2783604A CA 2783604 A CA2783604 A CA 2783604A CA 2783604 C CA2783604 C CA 2783604C
Authority
CA
Canada
Prior art keywords
ethylene
temperature
catalyst
moderator
epoxidation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CA2783604A
Other languages
English (en)
French (fr)
Other versions
CA2783604A1 (en
Inventor
Howard Sachs
Andrzej Rokicki
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Scientific Design Co Inc
Original Assignee
Scientific Design Co Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=44152004&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=CA2783604(C) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Scientific Design Co Inc filed Critical Scientific Design Co Inc
Publication of CA2783604A1 publication Critical patent/CA2783604A1/en
Application granted granted Critical
Publication of CA2783604C publication Critical patent/CA2783604C/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C11/00—Aliphatic unsaturated hydrocarbons
    • C07C11/02—Alkenes
    • C07C11/04—Ethylene
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/02—Synthesis of the oxirane ring
    • C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • C07D301/04—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen
    • C07D301/08—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen in the gaseous phase
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/02—Synthesis of the oxirane ring
    • C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • C07D301/04—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen
    • C07D301/08—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen in the gaseous phase
    • C07D301/10—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen in the gaseous phase with catalysts containing silver or gold
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
    • C07D303/02—Compounds containing oxirane rings
    • C07D303/04—Compounds containing oxirane rings containing only hydrogen and carbon atoms in addition to the ring oxygen atoms

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Epoxy Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
CA2783604A 2009-12-17 2010-12-16 Process for epoxidation start-up Expired - Fee Related CA2783604C (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US28739309P 2009-12-17 2009-12-17
US61/287,393 2009-12-17
PCT/US2010/060769 WO2011084600A2 (en) 2009-12-17 2010-12-16 Process for epoxidation start-up

Publications (2)

Publication Number Publication Date
CA2783604A1 CA2783604A1 (en) 2011-07-14
CA2783604C true CA2783604C (en) 2018-05-01

Family

ID=44152004

Family Applications (1)

Application Number Title Priority Date Filing Date
CA2783604A Expired - Fee Related CA2783604C (en) 2009-12-17 2010-12-16 Process for epoxidation start-up

Country Status (13)

Country Link
US (1) US8530682B2 (ja)
EP (2) EP2778157A1 (ja)
JP (1) JP5946772B2 (ja)
KR (1) KR101790254B1 (ja)
CN (1) CN102666514B (ja)
BR (1) BR112012014695A2 (ja)
CA (1) CA2783604C (ja)
IN (1) IN2012DN05178A (ja)
MX (1) MX2012007043A (ja)
MY (1) MY157612A (ja)
RU (1) RU2542978C2 (ja)
TW (1) TWI485141B (ja)
WO (1) WO2011084600A2 (ja)

Families Citing this family (32)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10532989B2 (en) 2007-05-09 2020-01-14 Shell Oil Company Epoxidation catalyst, a process for preparing the catalyst, and a process for the production of an olefin oxide, a 1,2-diol, a 1,2-diol ether, a 1,2-carbonate, or an alkanolamine
MX2012007043A (es) * 2009-12-17 2012-07-20 Scient Design Co Proceso para el arranque de epoxidacion.
US20110152073A1 (en) 2009-12-23 2011-06-23 Scientific Design Company, Inc. Epoxidation process and microstructure
US8815769B2 (en) 2011-04-11 2014-08-26 Dow Technology Investments Llc Process for conditioning a high efficiency ethylene oxide catalyst
EP2797715A4 (en) 2011-12-30 2016-04-20 Saint Gobain Ceramics SHAPED ABRASIVE PARTICLE AND METHOD OF FORMING THE SAME
WO2013106597A1 (en) 2012-01-10 2013-07-18 Saint-Gobain Ceramics & Plastics, Inc. Abrasive particles having complex shapes and methods of forming same
WO2013177446A1 (en) 2012-05-23 2013-11-28 Saint-Gobain Ceramics & Plastics, Inc. Shaped abrasive particles and methods of forming same
EP2906392A4 (en) 2012-10-15 2016-07-13 Saint Gobain Abrasives Inc GRINDING PARTICLES WITH SPECIAL FORMS AND METHOD FOR FORMING SUCH PARTICLES
CN104884443B (zh) 2012-12-31 2017-07-04 科学设计公司 用于环氧乙烷催化剂的启动方法
WO2014110194A1 (en) * 2013-01-11 2014-07-17 Scientific Design Company, Inc. Epoxidation process with post-conditioning step
PL2978566T3 (pl) 2013-03-29 2024-07-15 Saint-Gobain Abrasives, Inc. Cząstki ścierne o określonych kształtach i sposoby formowania takich cząstek
EP3087061B1 (en) * 2013-12-23 2018-04-11 Scientific Design Company Inc. Epoxidation process
US9566689B2 (en) 2013-12-31 2017-02-14 Saint-Gobain Abrasives, Inc. Abrasive article including shaped abrasive particles
US9771507B2 (en) 2014-01-31 2017-09-26 Saint-Gobain Ceramics & Plastics, Inc. Shaped abrasive particle including dopant material and method of forming same
WO2015160854A1 (en) 2014-04-14 2015-10-22 Saint-Gobain Ceramics & Plastics, Inc. Abrasive article including shaped abrasive particles
US9914864B2 (en) 2014-12-23 2018-03-13 Saint-Gobain Ceramics & Plastics, Inc. Shaped abrasive particles and method of forming same
US10196551B2 (en) 2015-03-31 2019-02-05 Saint-Gobain Abrasives, Inc. Fixed abrasive articles and methods of forming same
TWI634200B (zh) 2015-03-31 2018-09-01 聖高拜磨料有限公司 固定磨料物品及其形成方法
CA2987416A1 (en) * 2015-06-02 2016-12-08 Scientific Design Company, Inc. Porous bodies with enhanced pore architecture
CA2988012C (en) 2015-06-11 2021-06-29 Saint-Gobain Ceramics & Plastics, Inc. Abrasive article including shaped abrasive particles
EP4071224A3 (en) 2016-05-10 2023-01-04 Saint-Gobain Ceramics and Plastics, Inc. Methods of forming abrasive articles
EP3455320A4 (en) 2016-05-10 2019-11-20 Saint-Gobain Ceramics&Plastics, Inc. GRINDING PARTICLES AND METHOD FOR FORMING THEREOF
US11230653B2 (en) 2016-09-29 2022-01-25 Saint-Gobain Abrasives, Inc. Fixed abrasive articles and methods of forming same
CN110035998B (zh) 2016-12-02 2024-02-20 国际壳牌研究有限公司 调节乙烯环氧化催化剂的方法和生产环氧乙烷的相关方法
US10563105B2 (en) 2017-01-31 2020-02-18 Saint-Gobain Ceramics & Plastics, Inc. Abrasive article including shaped abrasive particles
US10865148B2 (en) 2017-06-21 2020-12-15 Saint-Gobain Ceramics & Plastics, Inc. Particulate materials and methods of forming same
US11059017B2 (en) 2017-09-15 2021-07-13 MultiPhase Solutions, Inc. Halogen selective detection gas chromatography for the on-line analysis and control of selective oxidation chemical production processes
EP3749449B1 (en) * 2018-02-07 2022-02-02 Basf Se Method for preparing a silver impregnation solution
EP4081369A4 (en) 2019-12-27 2024-04-10 Saint-Gobain Ceramics & Plastics Inc. GRINDING ARTICLES AND METHODS OF FORMING SAME
CN113121474A (zh) * 2019-12-30 2021-07-16 中国石油化工股份有限公司 乙烯环氧化银催化剂的开车方法
CN114057669B (zh) * 2020-07-29 2023-12-08 中国石油化工股份有限公司 一种乙烯环氧化恒温开车方法
CN114436998A (zh) * 2020-11-05 2022-05-06 中国石油化工股份有限公司 一种乙烯环氧化开车方法

Family Cites Families (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1170663A (en) 1967-03-22 1969-11-12 Shell Int Research Process for preparing Silver Catalysts
US3702259A (en) 1970-12-02 1972-11-07 Shell Oil Co Chemical production of metallic silver deposits
US4766105A (en) 1986-10-31 1988-08-23 Shell Oil Company Ethylene oxide catalyst and process for preparing the catalyst
US4761394A (en) 1986-10-31 1988-08-02 Shell Oil Company Ethylene oxide catalyst and process for preparing the catalyst
US5057481A (en) 1987-02-20 1991-10-15 Union Carbide Chemicals And Plastics Technology Corporation Catalyst composition for oxidation of ethylene to ethylene oxide
US4908343A (en) 1987-02-20 1990-03-13 Union Carbide Chemicals And Plastics Company Inc. Catalyst composition for oxidation of ethylene to ethylene oxide
US4874879A (en) 1988-07-25 1989-10-17 Shell Oil Company Process for starting-up an ethylene oxide reactor
EP0357293B1 (en) 1988-08-30 1996-02-28 Union Carbide Corporation Catalysts for the production of ethylene oxide and their preparation processes
US5187140A (en) 1989-10-18 1993-02-16 Union Carbide Chemicals & Plastics Technology Corporation Alkylene oxide catalysts containing high silver content
US5102848A (en) 1990-09-28 1992-04-07 Union Carbide Chemicals & Plastics Technology Corporation Catalyst composition for oxidation of ethylene to ethylene oxide
US5155242A (en) 1991-12-05 1992-10-13 Shell Oil Company Process for starting-up an ethylene oxide reactor
US5407888A (en) 1992-05-12 1995-04-18 Basf Aktiengesellschaft Silver catalyst
US5856534A (en) * 1997-12-18 1999-01-05 Arco Chemical Technology, L.P. Epoxidation process using supported silver catalysts treated with carbon dioxide
JP4042332B2 (ja) 2001-02-27 2008-02-06 三菱化学株式会社 レニウム含有触媒を用いるオレフィンオキシドの製造方法
BRPI0312010B1 (pt) * 2002-06-28 2017-11-28 Shell Internationale Research Maatschappij B.V Method for detaining an epoxidation process and a process for the epoxidation of an olefine
CN100376561C (zh) * 2002-06-28 2008-03-26 国际壳牌研究有限公司 环氧化方法的开车方法、烯烃环氧化的催化剂和方法
CN100512966C (zh) 2002-06-28 2009-07-15 国际壳牌研究有限公司 提高催化剂选择性的方法和烯烃环氧化方法
CN1860109B (zh) * 2003-09-29 2010-11-10 陶氏技术投资有限责任公司 使用气相助催化剂系统制备烯化氧的方法
US8791280B2 (en) 2005-08-10 2014-07-29 Sd Lizenzverwertungsgesellschaft Mbh & Co. Kg Process for preparation of catalyst carrier and its use in catalyst preparation
JP2010527352A (ja) * 2007-05-11 2010-08-12 ビリッグ，バリー，ジェイ． 酸化オレフィンプラントにおける高選択性触媒の開始
US7553980B2 (en) * 2007-09-26 2009-06-30 Sd Lizenzverwertungsgesellschaft Mbh & Co. Kg Process for initiating a highly selective ethylene oxide catalyst
WO2009137427A2 (en) * 2008-05-07 2009-11-12 Shell Oil Company A process for the start-up of an epoxidation process, a process for the production of ethylene oxide, a 1,2-diol, a 1,2-diol ether, a 1,2-carbonate, or an alkanolamine
MX2012007043A (es) * 2009-12-17 2012-07-20 Scient Design Co Proceso para el arranque de epoxidacion.
US20110152073A1 (en) 2009-12-23 2011-06-23 Scientific Design Company, Inc. Epoxidation process and microstructure

Also Published As

Publication number Publication date
EP2778157A1 (en) 2014-09-17
TWI485141B (zh) 2015-05-21
EP2513077A2 (en) 2012-10-24
US20110152548A1 (en) 2011-06-23
CA2783604A1 (en) 2011-07-14
MX2012007043A (es) 2012-07-20
BR112012014695A2 (pt) 2015-09-15
KR20120106809A (ko) 2012-09-26
CN102666514A (zh) 2012-09-12
IN2012DN05178A (ja) 2015-10-23
TW201136906A (en) 2011-11-01
RU2012130065A (ru) 2014-01-27
JP5946772B2 (ja) 2016-07-06
WO2011084600A3 (en) 2011-11-17
WO2011084600A2 (en) 2011-07-14
US8530682B2 (en) 2013-09-10
KR101790254B1 (ko) 2017-10-26
EP2513077A4 (en) 2013-05-22
RU2542978C2 (ru) 2015-02-27
EP2513077B1 (en) 2014-06-11
CN102666514B (zh) 2015-11-25
JP2013514387A (ja) 2013-04-25
MY157612A (en) 2016-06-30

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